铁氰化钴修饰石墨烯平面电极对过氧化氢的传感作用

利用高分子支撑法将气相沉积(CVD)石墨烯从铜基底上转移到聚对苯二甲酸乙二醇酯(PET)基底上,制备出石墨烯平面电极(GPE), 通过循环伏安法将铁氰化钴(CoHCF)纳米颗沉积到GPE上,得到铁氰化钴修饰石墨烯平面电极(CoHCF/GPE).研究表明,此电极对过氧化氢具有良好的传感作用,从而构建一种新型无酶过氧化氢传感器.此传感器在过氧化氢浓度为5.0-1200 μmol/L范围内,响应电流与浓度呈现良好的线性关系,检出限为7.1 nmol/L (S/N=3),响应时间约为2 s,具有稳定性好、抗干扰能力强、制备简单等优点.     

各向异性Hardy空间的分子特征及其应用

给定一个扩张矩阵A,得到了某些伴随于A的各向异性Hardy空间Hp(Rn)的分子特征刻画.作为其应用,还研究了与A相关的Calderón-Zygmund奇异积分算子和分数次积分算子在各向异性Hardy空间的有界性.     

Marcinkiewicz积分交换子的弱型(H1,L1)估计

§1Introductionandstatementofresult DenotebySn-1theunitsphereinRn(n≥2)equippedwiththenormalizedLebesgue measuredx′=dσ(x′).LetΩ∈L1(Sn-1)behomogeneousofdegreezeroandsatisfy∫Sn-1Ω(x′)dx′=0.(1.1)Then-dimensionalMarcinkiewiczintegralcorrespondingtotheLittlewood-Paleyg-functionintroducedbyStein[1]isdefinedbyμΩ(f)(x)=∫∞0|FΩ,t(f)(x)|2dtt31/2,where FΩ,t(f)(x)=∫|x-y|≤tΩ(x-y)|x-y|n-1f(y)dy.In1958,Stein[1]provedthatifΩ∈Lipγ(Sn-1)(0<γ≤1),thenμΩisoftype(p,p)for1相似文献   

一类带有变量核的积分算子在Herz型Hardy空间的有界性

本文研究了带有变量核的奇异积分与分数次积分算子.当核函数满足一类Dini型条件时,证明了这类算子从Herz型Hardy空间到Herz空间的有界性.     

Effects of Calcination Temperature on the Acidity and Catalytic Performances of HZSM-5 Zeolite Catalysts for the Catalytic Cracking of n-Butane

The acidic modulations of a series of HZSM-5 catalysts were successfully made by calcination at different treatment temperatures, i.e. 500, 600, 650, 700 and 800 ℃, respectively. The results indicated that the total acid amounts, their density and the amount of B-type acid of HZSM-5 catalysts rapidly decreased, while the amounts of L-type acid had almost no change and thus the ratio of L/B was obviously enhanced with the increase of calcination temperature (excluding 800 ℃). The catalytic performances of modified HZSM-5 catalysts for the cracking of n-butane were also investigated. The main properties of these catalysts were characterized by means of XRD, N2 adsorption at low temperature, NH3-TPD, FTIR of pyridine adsorption and BET surface area measurements. The results showed that HZSM-5 zeolite pretreated at 800 ℃ had very low catalytic activity for n-butane cracking. In the calcination temperature range of 500-700 ℃, the total selectivity to olefins, propylene and butene were increased with the increase of calcination temperature, while, the selectivity for arene decreased with the calcination temperature.The HZSM-5 zeolite calcined at 700 ℃ produced light olefins with high yield, at the reaction temperature of 650 ℃ the yields of total olefins and ethylene were 52.8% and 29.4%, respectively. Besides, the more important role is that high calcination temperature treatment improved the duration stability of HZSM-5zeolites. The effect of calcination temperature on the physico-chemical properties and catalytic performance of HZSM-5 for cracking of n-butane was explored. It was found that the calcination temperature had large effects on the surface area, crystallinity and acid properties of HZSM-5 catalyst, which further affected the catalytic performance for n-butane cracking.     

分数次积分算子交换子的弱型估计

通过引进一类相应于平均Luxemburg范数的分数阶极大算子并使用sharp函数的技巧,建立了分数次积分算子及其相应的极大算子与BMO函数生成的交换子的LlogL型弱型估计.     

变量核分数次积分在Hardy空间的有界性

§ 1　 Introduction and main resultsLet Sn- 1 be the unitsphere in Rn(n≥ 2 ) equipped with normalized Lebesgue measure dσ= dσ(z′) .We say that a functionΩ(x,z) defined on Rn× Rnbelongs to L∞ (Rn)× Lr(Sn- 1 )(r≥ 1 ) ,ifΩ(x,z) satisfies the following two conditions,(i) for any x,z∈Rnandλ>0 ,there hasΩ(x,λz) =Ω(x,z) ;(ii)‖Ω‖L∞(Rn)× Lr(Sn- 1) :=supx∈ Rn∫Sn- 1|Ω(x,z′) | rdσ(z′) 1 / r<∞ .For 0 <α相似文献   

关于C*-代数交换性的若干结果

本文给出了C^*-代数的交换性的一系列等价刻划,特别，证明了C^*-代数A是交换的当且仅当存在正整数n≥2使得对所有a，b∈A^ ，下面的二项式公式成立：(a b)^n=∑k=0^nCn^ka^kb^n-k。     

具有齐性核的Marcinkiewicz积分在Herz型Hardy空间的有界性

本文讨论了具有齐性核的Marcinkiewicz积分μΩ在Herz型Hardy空间的有界性,证明了μΩ是从HKqα,p(Rn)到Kqα,p(Rn)有界的.     

Marcinkiewicz积分交换子在Herz型空间中的弱型估计

用μΩ表示Marcinkiewicz积分,μΩ,b表示μΩ与函数b∈BMO(R~n)生成的交换子．本文证明了交换子μΩ,b是从Herz型Hardy空间H■_q~(n(1-(1/q)),p)(R~n)到弱Herz空间W■_q~(n(1-(1/q)),p)(R~n)有界的,其中0＜p≤1,1＜q＜∞．