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Yan YangMeng Gao Liu-Ming WuCong Deng Dong-Xue ZhangYang Gao Yan-Ping ZhuAn-Xin Wu 《Tetrahedron》2011,67(29):5142-5149
The convergent and linear domino reactions have been first integrated, for the first time, to provide an efficient synthesis of indole-furan conjugates from indoles, methyl ketones, and 1,3-dicarbonyl compounds. 相似文献
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Zaixiang Lou Hongxin WangSong Zhu Ming ZhangYang Gao Chaoyang MaZhouping Wang 《Journal of chromatography. A》2010,1217(16):2441-2446
The simultaneous ultrasonic and microwave assisted extraction (UMAE) technique was first employed to obtain phenolics. The effects of UMAE variables including extraction time, microwave power, and solvent to solid radio on the yield of phenolics were investigated. The optimized conditions were as follows: solvent to solid ratio was 20:1 (ml/g), extraction time was 30 s, microwave power was 500 W and two times of extraction. Moreover, the phenolic yield of UMAE was higher than that by maceration, indicating a significant reduction of extraction time and an improvement of efficiency. The phenomenon is related to the strong disruption of leaf tissue structure by microwave induced expansion and ultrasonic shaking, which had been observed with the scanning electron microscopy. The phenolic compositions of the extract was then identified by ultra performance liquid chromatography tandem mass spectrometry (UPLC–MS/MS), 10 compounds had been characterized, providing a more complete identification of phenolic compounds in burdock leaves than previously reported. The occurrence of benzoic acid and p-coumaric acid is reported for the first time. This study suggests that UMAE is a good alternative for the extraction of phenolics, with a great potential for industrial application. Also, UMAE provides a new sample preparation technique for characterization of the phenolic compounds from plants. 相似文献
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Liyan ZhangYang Yang Shuyuan MaWanju Luo Yulong Liu Ke Zhu 《Physica B: Condensed Matter》2012,407(3):494-499
Influence of magnetic annealing at 823 K up to 10 T (T) on the phonon behaviors of nanocrystalline BiFeO3 was investigated by Raman spectroscopy. The frequencies of fundamental Raman modes increase obviously with increasing annealing magnetic field, and the intensity of the 1260 cm−1 two-phonon mode decreases. The pronounced anomalies of Raman phonon modes under magnetic annealing are attributed to the change of the spin-phonon coupling due to the modulation of spiral spin order. Furthermore, the temperature dependence of Raman peak positions, for the two prominent modes (147 and 176 cm−1), show no notable anomaly around TN except the sample annealed under 10 T magnetic field; meanwhile, in this sample, another obvious phonon anomaly occurs at ∼150 K (another magnetic phase transition point), which indicate that stronger magnetic annealing with 10 T intensely enhances the spin-phonon coupling, and possibly increases magnetoelectric coupling of nanocrystalline BiFeO3 due to severely modulation of spiral spin order. 相似文献
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