Implementation and experimental study on fast object modeling based on multiple structured stripes

In this paper, a practical structured light-based system for fast object modeling and reconstruction is reported. The system consists of an off-the-shelf digital projector, a video camera and a turntable. The system calibration is implemented accurately and automatically by taking a single image of an illuminated calibration template. The multiple color light stripes emitted by the projector adopt only three colors and the color can be modified easily according to the surface texture of the object. This makes the system widely applicable in many situations, and the assumption about color neutrality, which is a limitation to other similar systems, can be largely relaxed. The registration and merging algorithm is greatly simplified by employing a turntable. The validity and high accuracy of the method are demonstrated by extensive real experiments.     

Simultaneous characterization and quantification of flavonoids in Euonymus alatus (Thunb.) Siebold from different origins by HPLC-PAD–MS

A high-performance liquid chromatography coupled with photodiode array detection and electrospray ionization tandem mass spectrometry (HPLC-PAD–ESI-MS) method has been developed for the simultaneous identification and quantification of active compounds (rutin and quercetin) contained in Traditional Chinese Medicine (TCM) Euonymus alatus (Thunb.) Siebold (EAS). The herb samples from ten main origins and five medicinal portions (leaf, fruit, stem, pterygium and root) were investigated. The separation was performed on a Shim C₁₈ column at 30 °C with an isocratic elution. Methanol (A) and water (0.5% methanoic acid, v/v) (B) were used as mobile phases. The recoveries of the two compounds were 100.184% and 100.417%, respectively, and all of them showed good linearity (r² ? 0.9993) in relatively wide concentration ranges. The developed method was applied to identify and quantify the two major active compounds in the collected herb samples, and the results indicated that contents of the two compounds in EAS varied significantly from habitat to habitat. It was demonstrated that the proposed method was helpful for the quality evaluation of EAS.     

A novel and efficient one-pot four-component tandem approach for the synthesis of pyran derivatives

A series of new pyran derivatives are efficiently synthesized in a one-pot four-component tandem reaction via Suzuki coupling followed by a three-component reaction from readily available 4-bromobenzaldehyde, activated methylene compounds, and carbonyl compounds. Single crystal X-ray structure of the synthesized product is presented. The versatility and efficiency of the proposed methodology has been demonstrated in the synthesis of novel heterocyclic molecules.     

水下减阻技术研究综述

在简要回顾早期减阻研究的基础上,对现有典型水下湍流减阻技术进行了较深入地分析.重点介绍了脊状表面减阻、微气泡减阻和疏水/超疏水表面减阻的研究现状.分别从实验研究和理论研究两方面对其进行了阐述,并着重强调了各自的减阻机理. 此外,还简要介绍了柔顺壁面减阻、壁面振动减阻等其它减阻技术.展望了水下减阻技术今后的研究重点及其应用前景.      

A Novel One‐pot Synthesis of Biaryl Derivatives by Sequential Strategies via Suzuki Coupling/Knoevenagel Condensation in Aqueous Medium at Room Temperature

A novel one‐pot synthesis of biaryl derivatives has been developed starting from bromobenzaldehyde and phenylboronic acid in the presence of activated methylene compounds via sequential Suzuki coupling/Knoevenagel condensation in aqueous isopropanol medium at room temperature. Significantly, this strategy afforded a straightforward and efficient approach to construct original biaryls in which a new carbon double bond bound to activated moieties such as nitrile, ester and amide is formed from three simple substrates in a one‐pot procedure. Moreover, a wide scope of substrates could effectively participate in the process affording the target products in moderate to excellent yields.     

Synthesis of dendrimers terminated by DABCO ligands and applications of its palladium nanoparticles for catalyzing Suzuki–Miyaura and Mizoroki–Heck couplings

A new kind of silica‐supported third‐generation dendrimers capped by 1,4‐diaza‐bicyclo[2.2.2]octane (DABCO) group‐stabilized palladium(0) nanoparticles, and their enhanced catalytic activity in Suzuki–Miyaura and Mizoroki–Heck reactions in excellent yield under mild conditions, was reported. The resulting silica‐supported dendrimer‐stabilized palladium(0) nanoparticles with a particle size of 10–20 nm were prepared in situ by treatment with PdCl₂ and hydrazine in ethanol at 60 °C for 24 h. The catalyst as prepared was characterized by FT‐IR, X‐ray diffraction, thermal analysis, elementary analysis (EA), scanning electron microscopy and transmission electron microscopy. Recycling experiments showed that the catalyst could be easily recovered by simple filtration and reused for up to five cycles without losing its activity. Copyright © 2012 John Wiley & Sons, Ltd.     

Spalding公式在脊状表面湍壁摩擦力测量中的应用

在低速风洞中来流速度一定的情况下使用IFA300恒温热线风速仪测量了光滑表面和两种不同尺寸的脊状表面湍流边界层平均速度分布剖面,并验证了试验段湍流发展的充分性;通过应用Spalding壁面公式使用最小二乘法精准拟合了实验测量的边界层内层速度分布曲线,得到了湍流边界层壁面摩擦速度并进一步求得湍流壁面摩擦应力,较准确地计算出脊状表面的虚拟原点位置,并通过与对数律公式拟合结果比较分析,证实了该方法更加准确有效. 最后分别计算了3种实验模型的湍流边界层动量损失厚度. 通过对比脊状表面与光滑表面动量损失厚度和壁面摩擦应力,反映了动量损失厚度的大小与壁面摩擦应力的大小具有一致性,充分证实了脊状表面在湍流中具有一定的减阻效果.      

Self-standing rationally functionalized graphene as high-performance electrode materials for supercapacitors

Supercapacitors（SCs） have attracted much attention as one of the alternative energy devices due to their high power performance,long cycle life,and low maintenance cost.Graphene is considered as an innovative and promising material due to its large theoretical specific surface area,high electrical conductivity,good mechanical properties and chemical stability.Herein,we report an effective strategy for elaborately constructing rationally functionalized self-standing graphene（SG） obtained from giant graphene oxide（GGO） paper followed by an ultrarapid thermal-processing.This treatment results in both the exfoliation of graphene sheets and the reduction of GGO by elimination of oxygencontaining groups.The as-prepared SG electrode materials without additive and conducting agent provide an excellent combination of the electrical double layer capacitor（EDLC） and pseudocapacitor（PC） functions and exhibit superior electrochemical performance,including high specific capacitance,good rate capability and excellent cycling stability when investigated in three-electrode electrochemical cells.