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通过配方及烧成工艺的改变,得到两种不同显微结构的高铝陶瓷材料,其一为晶粒大小均匀,边界清晰,晶粒堆砌结构;其二为晶粒大小不一,晶粒边界不清,甚至晶粒被包裹在玻璃相中,形成玻璃相堆积结构.测定了材料的抗折强度、体积电阻率、抗击穿强度、比重、金属化层抗张强度和气密性.分析了两种显微结构的成因及不同微观结构对陶瓷材料性能和金属化层性能的影响.实验证明:采用微粉氧化铝配料,利于获得金属化性能优良的细晶结构的高铝陶瓷材料;用粗粉氧化铝配料,并加人复合的添加剂,也可以获得细小晶粒堆砌结构的高铝陶瓷材料,这类结构高铝陶瓷材料的金属化层性能好. 相似文献
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Small-angle neutron scattering study on the stability of oxide nanoparticles in long-term thermally aged 9Cr-oxide dispersion strengthened steel 下载免费PDF全文
Peng-Lin Gao 《中国物理 B》2022,31(5):56102-056102
A 9Cr-oxide dispersion strengthened (ODS) steel was thermally aged at 873 K for up to 5000 h. The size distribution and chemical composition of the dispersed oxide nanoparticles were analyzed by small-angle neutron scattering under a magnetic field. Combined with transmission electron microscopy, Vickers micro-hardness tests and electron backscattered diffraction measurements, all the results showed that the thermal treatment had little or no effect on the size distributions and volume fractions of the oxide nanoparticles in the ferromagnetic matrix, which suggested excellent thermal stability of the 9Cr-ODS steel. 相似文献
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本文研究了在大气中用燃烧火焰法沉积出的金刚石的结晶形态。结果发现,所沉积出的金刚石除了同体和十四面体单晶外,还有尖晶石型、伪五角型、二十面体型及球型等多重孪晶颗粒(MTPS),并与实验模型进行了对比观察。所有MTPS大多是以{111}面为孪晶面。在{111}面上还有大量层错和显微孪晶。本文还对产生上述晶体形貌的原因进行了理论分析。 相似文献
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