Auto-deposition of 210Bi and 210Po on nickel discs and their application in the analysis of natural waters

Journal of Radioanalytical and Nuclear Chemistry - This study presents a time-efficient method of analysing 210Pb, 210Bi, and 210Po in natural waters. The optimum pH (1.00), temperature...     

有界域上具有离散全纯核的Koppelman公式与-方程

D是Cn空间中具有逐块C(1)边界的有界域,该文建立了D上一个具有离散局部全纯核的 (0,q)形式的Koppelman积分公式及其相应的■-方程解的积分表示和它的内闭一致估计式.     

Studies on the properties of flow-induced oscillation and sound radiation in streamlined protuberant special cavities

I.IntroductionAsanuidpassingthroughthecavityatcertainflowrate,themediuminthemouthandthccavityisoscillatingandsoundisradiated.Noton1ystochasticturbu1encenoiscispossi-blyproducedbutsinglefrequencysoundofspecia1lydesignatedpitchisalsoproduced.Andthusthespcctrumofthcradiatedsoundisshownascontinuousspectrumandcharacteristiclinespcctrum.Inthiscascwcmaycallitflow-inducedosci1lation.Flow-inducedoscillationandsoundradiationcanbeproducedasafluid(waterorgas)passingthroughthecavitybysinkingcavityunderint…     

小间隙高放大多丝室及其放电机制

对以强猝灭气体工作的小间隙多丝室及其放电机制进行了研究,实验表明,因为工作在饱和模式区,这种室同时具有很高的气体放大和相当快的时间特性.文中探讨了放电机制,雪崩中空间电荷效应以及电离光子的产生和作用是重要的因素,而其中后一因素又受到强猝灭气体的抑制.     

矩形均匀电子束在激光介质中的能量沉积的模拟计算

本文主要论述了0.5MeV,单能垂直入射的电子束在三种不同密度的氟化氪准分子激光介质中的能量沉积。计算是采用Monte Carlo方法的MCSED程序,光轴方向采用周期性边界条件,因此能够给出平行于和垂直于电子束入射方向的沉积能量的空间分布。本文给出了在三种不同密度下的出射电子的角分布。用该程序对垂直入射的,初始能量为1MeV的电子在半无限大Al靶中的沉积能量的计算结果与ONETRAN程序的结果及实验结果的比较表明MCSED程序的计算结果是可靠的。     

Zircon SHRIMP age of Mesoarchaean meta-argilloarenaceous rock in the Anshan area and its geological significance

In order to better understand the early continental evolution of the Anshan area, one ofthe typical Precambrian distribution areas of the North China Craton, the geochronology and REEcomposition of the zircons from the meta-argillo-arenaceous rock occurred as enclave in 3.1 GaLishan trondhjemite are studied by using SHRIMP ll ion microprobe. It is indicated that the Pa-leoarchaean is a very important continental formation period in the Anshan area and 3.2 Ga can beregarded as the boundary between the Paleoarchaean and Mesoarchaean.     

Preparation and characterization of silver/TiO2 composite hollow spheres

Silver-coated poly(methyl acrylic acid) (PSA) core-shell colloid particles were prepared by an in situ chemical reduction method. Crystalline silver/titania composite hollow spheres were obtained by coating the as-prepared PSA/silver particles with an amorphous titania layer and subsequently calcining in Ar atmosphere. SEM and TEM investigation indicated that the size of the as-prepared PSA/silver and PSA/silver/TiO(2) core-shell particles and silver/titania composite hollow particles was fairly uniform and the wall thickness of the hollow spheres was in the range of 40-80 nm. UV-vis absorption spectra were recorded to investigate their optical properties.     

酚醛树脂固化过程的红外光谱分析

利用红外光谱(IR)及其变温样品池、定量分析程序对酚醛树脂固化过程中的结构变化进行了研究,它对于酚醛树脂固化过程的质量控制具有重要意义。     

一类2(1H)-喹喔啉衍生物的电子轰击质谱分析

以邻苯二胺为原料合成表征了一类喹喔啉衍生物；1-烷基-3-甲基-2（1H）-喹喔啉-2-酮（1-alkyl-3-methly-2(1H)-quinoxalin-2-one，简称AMQ，其中alky=H、CH3、Et、n-C3H5、n-C5H11、n-C16H33)。用电子轰击电离质谱（EI-MS）和核磁共振谱图（^1H-NMR)鉴定了AMQ，研究了不同取代基对这类化合物EI-MS谱图的影响，分析得到一些裂解规律。结果表明：所有样品谱图中均有芳香化合物的特征CnHn^ 系列峰m/z78，65，52，39和（或）m/z77、76、64、63、51、50、38、37。对于末取代的样品及低级烷烃取代的样品，谱图中的基峰为分子离子峰，对于取代基中碳数大于等于3的样品。谱图中的基峰不是分子离子峰，分子离子峰强度随着碳数的增加而降低。这些样品一般容易发生骨架重排，丢失一分子CO，生成1-烷基-2-甲基苯并哒唑正离子。此外，还讨论了谱图中其它的一些碎片离子峰。这对于研究和指导喹喔啉衍生物 的合成，探讨它们在药效及结构特征与生理活性的关系等方面具有重要的应用价值和理论意义。