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1.
Summary Using a saturated non-boiling hydrocarbon mixture, the influence of two parameters on the results of field ionization mass spectrometry (FI-MS) measurements was studied: (a) the potential difference between the FI emitter and the counterelectrode; (b) the emitter temperature.Variation of the potential difference had only a minor effect on the average molecular mass measured and had no evident effect on the relative ring number distribution in the sample. In contrast, when the emitter temperature was increased, higher average molecular masses were recorded. Moreover, the average molecular masses shifted to higher ring numbers. In order to control the relationship between the described influences during mixture analysis, measuring instructions have been developed that enable the quantitative analysis of unknown saturated samples. However, average molecular mass of the mixture must be known.
Entwicklung einer quantitativen FI-MS-Methode zur Charakterisierung von gesättigten hoch- und nichtsiedenden Kohlenwasserstoffgemischen相似文献
2.
3.
J. B. Lewis E. L. Baldeschwieler L. D. Tabern E. F. Shelberg D. Hillis S. Cromer I. F. Bingham S. Givaudon M. Aubert M. R. Moutte A. Andant P. Lambert J. Lecomte J. Tausz H. Wolf B. Gordon W. Dachnow I. Perrier M. Lobunetz M. O. Chaikin C. Engler D. Holde 《Analytical and bioanalytical chemistry》1940,119(7-8):307-310
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5.
Phenomena accompanying electrochemical doping of solid fullerene films with potassium were studied by sputter ion depth profiling
(XPS and SIMS). The potassium distribution was determined, and artifacts associated with possible damage of the layer composition
caused by ion impact were investigated and discussed. To compare the charge transfer while reductive doping is taking place
at fullerene/solution interface with doping from gas phase, model layers were prepared and doped by potassium under UHV conditions.
It was found that sputtering by Ar+ primary ions yields both accurate information on the alkaline metal distribution and on its concentration. Sputtering by
O+ ions led to an enrichment of potassium, apparently due to the reactivity of oxygen with the fullerene matrix. It is shown
that the reductive doping starts at the fullerene/solution interface. The concentration of potassium in the doped films was
found to be lower than expected from the charge transferred during the electrochemical reduction. Other phase transformations
such as hydrogenation are discussed.
Received March 4, 2002; accepted July 26, 2002 相似文献
6.
K. Wolf 《Archive of Applied Mechanics (Ingenieur Archiv)》1941,12(4):259-264
Ohne Zusammenfassung 相似文献
7.
Eckhard Steffen 《Discrete Mathematics》2004,280(1-3):191-214
Cubic bridgeless graphs with chromatic index four are called uncolorable. We introduce parameters measuring the uncolorability of those graphs and relate them to each other. For k=2,3, let ck be the maximum size of a k-colorable subgraph of a cubic graph G=(V,E). We consider r3=|E|−c3 and
. We show that on one side r3 and r2 bound each other, but on the other side that the difference between them can be arbitrarily large. We also compare them to the oddness ω of G, the smallest possible number of odd circuits in a 2-factor of G. We construct cyclically 5-edge connected cubic graphs where r3 and ω are arbitrarily far apart, and show that for each 1c<2 there is a cubic graph such that ωcr3. For k=2,3, let ζk denote the largest fraction of edges that can be k-colored. We give best possible bounds for these parameters, and relate them to each other. 相似文献
8.
Francis J. Vasko John A. McNamara Dennis D. Newhart Floyd E. Wolf 《The Journal of the Operational Research Society》1994,45(11):1285-1292
The optimum assignment of structural steel shapes to rail cars is an important logistical problem in the steel industry. In this paper, we discuss an application at Bethlehem Steel that not only involves weight and dimensional constraints, but also customer unloading constraints. The formulation is a generalized bin packing problem which is solved by modifying and extending the first fit decreasing algorithm. The solution algorithm, SOLID (for Structural Optimal Loading IDentification), has been used extensively for one of Bethlehem's high tonnage customers providing very good practical (implementable) results that achieve the desired goals. Bethlehem has enhanced this approach for use with other customers. 相似文献
9.
Christian Wolf 《Journal of statistical physics》2006,122(6):1111-1138
In this paper we introduce the notion of generalized physical and SRB measures. These measures naturally generalize classical
physical and SRB measures to measures which are supported on invariant sets that are not necessarily attractors. We then perform
a detailed case study of these measures for hyperbolic Hènon maps. For this class of systems we are able to develop a complete
theory about the existence, uniqueness, finiteness, and properties of these natural measures. Moreover, we derive a classification
for the existence of a measure of full dimension. We also consider general hyperbolic surface diffeomorphisms and discuss
possible extensions of, as well as the differences to, the results for Hènon maps. Finally, we study the regular dependence
of the dimension of the generalized physical/SRB measure on the diffeomorphism. For the proofs we apply various techniques
from smooth ergodic theory including the thermodynamic formalism.
2000
Mathematics Subject Classification. Primary: 37C45, 37D20, 37D35, Secondary: 37A35, 37E30 相似文献
10.
A. Thomasson S. Geffroy E. Frejafon D. Weidauer R. Fabian Y. Godet M. Nominé T. Ménard P. Rairoux D. Moeller J.P. Wolf 《Applied physics. B, Lasers and optics》2002,74(4-5):453-459
Continuous mapping of an ozone episode in Paris in June 1999 has been performed using a differential absorption lidar system.
The 2D ozone concentration vertical maps recorded over 33 h at the Champ de Mars are compiled in a video clip that gives access
to local photochemical dynamics with unprecedented precision. The lidar data are compared over the whole period with point
monitors located at 0-, 50-, and 300-m altitudes on the Eiffel Tower. Very good agreement is found when spatial resolution,
acquisition time, and required concentration accuracy are optimized. Sensitivity to these parameters for successful intercomparison
in urban areas is discussed.
Received: 11 February 2002 / Published online: 14 March 2002 相似文献