Surface profile inspection of a moving object by using dual-frequency Fourier transform profilometry

The 2π phase ambiguity caused by surface isolations and large height step can be solved by dual-frequency projection grating profilometry. However, in the Fourier transform profilometry (FTP) of a moving object, only one single deformed fringe pattern can be obtained. In order to introduce the dual-frequency technique into the FTP of moving object, a novel experimental system is designed to capture two fringe patterns with different frequency at the same time. A grating structure comprising two regions with different frequencies is projected upon the surface of the detected object. Two line-scan CCD cameras are used to capture the surface images encoded by the two kinds of patterns, respectively. By getting the corresponding image intensity at the same point of the object surface in the two acquired images, the dual-frequency technique is applied to extract the real phase without phase ambiguity. The surface profile of a specimen with a large height step is measured to prove the feasibility of the proposed method. The experimental results show that the proposed method can solve the 2π phase ambiguity problem successfully in the surface profile inspection of a moving object.     

The fluctuating phase error analysis in the digital grating phase-shifting profilometry

The nonlinear response of the experimental system and the saturation of fringe patterns can induce the fluctuating phase error in the projection grating phase-shifting profilometry. Two major factors of the fluctuating phase error are discussed by simulation. The fluctuating phase error caused by the nonlinear response of the system is four times the frequency of the fringe pattern when the conventional four-frame phase extracting algorithm is used. However, such error can be decreased by five-frame algorithm. On the other hand, the fluctuating phase error caused by the fringe saturation is five times the frequency of the fringe pattern by using conventional five-frame phase extracting algorithm. A novel phase recovering algorithm is used to decrease the phase error caused by the saturation. Furthermore, the applicability range of the proposed phase recovering algorithm is analyzed by simulation and experiments with different saturation degree of the fringe pattern and nonlinearity of the measurement system.     

Continuous production of (S)-1-phenylethanol by immobilized cells of Rhodotorula glutinis with a specially designed process

A specially designed process for the continuous production of a chiral alcohol by immobilized Rhodotorula glutinis was prepared and is reported. The performance of the process with immobilized cells was also investigated. The run time of the immobilized cells, the flow rates of the substrate, and tris buffer containing 4% glucose in the process were optimized. The immobilized R. glutinis biocatalyst could be used for 15 days with maximum reaction activity. Under the optimized conditions, the continuous production process was operated for 30 days and resulted in 10.8 mL (S)-1-phenylethanol [(S)-1-PE]. The process has been demonstrated on a multigram scale in 75% overall yield with a purity of >99%.     

New measurements and reanalysis of 14N elastic scattering on 10B target

The angular distributions of elastic scattering of ¹⁴N ions on ¹⁰B targets have been measured at incident beam energies of 21.0 and 24.5 MeV. Angular distributions at higher energies 38–94.0 MeV (previously measured) were also included in the analysis. All data were analyzed within the framework of the optical model and the distorted waves Born approximation method. The observed rise in cross sections at large angles was interpreted as a possible contribution of the α-cluster exchange mechanism. Spectroscopic amplitudes SA₂ and SA₄ for the configuration ¹⁴N→ ¹⁰B +α were extracted. Their average values are 0.58±0.10 and 0.81±0.12 for SA₂ and SA₄, respectively, suggesting that the exchange mechanism is a major component of the elastic scattering for this system. The energy dependence of the depths for the real and imaginary potentials was found.     

The effect of topical ethanol extract of Cotinus coggygria Scop. on cutaneous wound healing in rats

The aim of this study is to determine the cutaneous wound healing effects of the ethanol extract of Cotinus coggygria leaves in rats by excision wound model to provide scientific evidence for the traditional use of C. coggygria Scop. The levels of malondialdehyde, catalase, superoxide dismutase, glutathione and hydroxyproline were investigated in wound tissues. Histopathological examination was also performed. The hydroxyproline content of the granulation tissue and the glutathione levels were both significantly higher in the treatment group than in the control group (p < 0.05 for both); while the malondialdehyde levels were significantly lower in the treatment group (p < 0.05). These results were supported with histological results. The ethanol extract of C. coggygria Scop could be considered as an effective agent in wound healing in accordance with its traditional use.     

Profile measurement of a moving object using an improved projection grating phase-shifting profilometry

3-D profile measurement of a moving object using a novel phase-shifting technique is introduced. Digital gratings with two steps phase-shifting are projected periodically onto a measured object surface. The deformed fringe patterns are captured by a frame CCD camera within a short exposure time. By synchronizing the projector and the CCD camera accurately, there is an overlapping part which is the same part of the object among three neighbouring frames. The length of an overlapping part can be controlled as one third of a frame length. Hence the intensity values at the same surface point modulated by three neighbouring gratings can be obtained, and its phase value can be computed by an improved phase-extracting algorithm. The profile of a specimen is detected by the proposed method. Experimental results demonstrate that this method is effective for the profile measurement of a moving object.     

Surface profile measurement of moving objects by using an improved π phase-shifting Fourier transform profilometry

The π phase-shifting Fourier transform technique is introduced into the surface profile measurement of moving objects. A digital grating comprising two regions, which have a π phase shifting is projected onto the object. Two line-scan CCD cameras are used to capture two deformed fringe patterns with π phase shifting at the same time. As the object is moving, each point at the object surface can be captured twice. The digital correlation method is used to calibrate the experimental system. The zero-order component can be eliminated by subtracting intensities of the same surface point in two captured images. And then the phase can be extracted by Fourier transform without the disturbance of zero-order component. Experimental results demonstrate that this method is feasible for the moving surface profile detection and the measurable slope of height variation can be extended.     

A novel approach for highly proton conductive electrolyte membranes with improved methanol barrier properties: Layer-by-Layer assembly of salt containing polyelectrolytes

A series of highly proton conductive electrolyte membranes with improved methanol barrier properties are prepared from polyallylamine hydrochloride (PAH) and polystyrene sulfonic acid (PSS) including salt by Layer-by-Layer (LbL) method. The effects of added salt type (NaCl, MgCl₂) and salt concentration (1.0 M, 0.1 M) on proton conductivity (σ) and methanol barrier properties of the LbL self-assembled composite membranes are discussed in terms of controlled layer thickness and charge density. Furthermore, the influences of ion type in the multilayered composite membranes are studied in conjunction with physicochemical and thermal properties.The deposition of the self-assembly of PAH/PSS film on Nafion is followed by UV–Vis spectroscopy and it is observed that the polyelectrolyte layers growth on both sides of Nafion membrane regularly. (PAH/PSS)₅–Na⁺ and (PAH/PSS)₅–H⁺ with 1.0 M NaCl exhibits 49.6 and 27.8% reduction in lower methanol permittivity in comparison with the pristine Nafion^®117, respectively, while the proton conductivities are 12.97 and 74.69 mS cm⁻¹. Promisingly, it is found that the membrane selectivity values (Φ) of all multilayered membranes in H⁺ form are much higher than that of salt form (Na⁺ and Mg²⁺) and perfluorosulfonated ionomers reported in the literature. Also, we find out that the use of polyelectrolytes with high charge density causes a further improvement in proton conductivity and methanol barrier properties simultaneously. These encouraging results indicate that upon a suitable choice of LbL deposition conditions, composite membranes exhibiting both high proton conductivity and improved methanol barrier properties can be tailored for fuel cells.     

Improving amplitude-modulated signals by re-scaled and twice sampling vibrational resonance methods

Quantum chemical calculations have been employed to study the molecular effects produced by \(\hbox {Cr}_{2}\hbox {O}_{3}/\hbox {SnO}_{2}\) optimised structure. The theoretical parameters of the transparent conducting metal oxides were calculated using DFT / B3LYP / LANL2DZ method. The optimised bond parameters such as bond lengths, bond angles and dihedral angles were calculated using the same theory. The non-linear optical property of the title compound was calculated using first-order hyperpolarisability calculation. The calculated HOMO–LUMO analysis explains the charge transfer interaction between the molecule. In addition, MEP and Mulliken atomic charges were also calculated and analysed.     

The structure of N-(1H-benzo[d]imidazol-2-ylmethyl)-N-(2,6-dichlorophenyl)amine

The N-(1H-benzo[d]imidazol-2-ylmethyl)-N-(2,6-dichlorophenyl)amine, C₁₄H₁₁N₃Cl₂, M _r = 292.17, crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 10.707(2), b = 9.615(2), c = 25.944(6) Å. The benzimidazole ring system is planar and makes a dihedral angle of 77.8(1)° with the phenyl ring. The structure is stabilized by an N–H···N hydrogen bond.