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1.
Gurenkova Yu. S. Kornyakov I. V. Ostrovsky V. A. Skrylnikova M. A. Khramchikhin A. V. 《Russian Journal of General Chemistry》2020,90(7):1202-1206
Russian Journal of General Chemistry - 8-Phenyltetrazolo[5,1-b][1,3,4]thiadiazepine was obtained as a result of intermolecular cyclization of 1-amino-1H-tetrazole-5-thiol and 3-phenyl-2-propynal.... 相似文献
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V. A. Khramchikhin N. G. Didkovskii A. V. Khramchikhin A. V. Dogadina B. I. Ionin 《Russian Journal of General Chemistry》2011,81(8):1635-1639
A new approach to the synthesis of the triketones of triacylmethane series containing a (dimetoxyphosphoryl) acetyl group
was developed based on the reaction of β-diketones with dimethyl chloroacetylenephosphonate. 相似文献
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Elena B. Erkhitueva Albina V. DogadinaAndrey V. Khramchikhin Boris I. Ionin 《Tetrahedron letters》2012,53(33):4304-4308
1-Chloroacetylene-2-phosphonates react with 1H-1,2,4-triazole-3-thiols in anhydrous acetonitrile with high regioselectivity to form the fused heterocycles, 6-(dialkoxyphosphoryl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ylium chlorides 1-5. A significant difference from the previously known reactions of binucleophiles with haloacetylenes is the involvement of both acetylenic carbon atoms in the heterocycle formation. A reaction mechanism is hypothesized that assumes the formation of a sulfenium cation at the acetylene C-1 atom followed by attack of the C-2 atom by the ring N-2 atom. Compounds 1-5 easily lose one alkyl group from the dialkoxyphosphoryl fragment to form zwitterions (e.g., 6-8) which further can be transformed into inner salts 9 and 10 when heated with concentrated hydrochloric acid. 相似文献
4.
M. V. Karpov A. V. Khramchikhin I. V. Suvorova Yu. L. Piterskaya M. D. Stadnichuk 《Russian Journal of General Chemistry》2007,77(5):899-904
A method of synthesis of 2-propargylaminoethanols, perspective synthons for a one-pot synthetic technology excluding isolation of unstable prop-2-ynylideneaminoethanols is developed. A number of 2-propargylaminoethanol hydrochloride derivatives are synthesized, and their 1H and 13C NMR spectra were discussed. 相似文献
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Light-induced dibromophosphination of alkenes was studied. Dehydrobromination of the synthesized bromoalkylphosphonous dibromides gave the corresponding dibromophosphinoalkenes which were converted into alkenylphosphonous acids and their cyclic esters, benzo[1,3,2]dioxaphospholes. 相似文献
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Khramchikhin V. A. Yacobson G. V. Dogadina A. V. Khramchikhin A. V. Ionin B. I. 《Russian Journal of General Chemistry》2010,80(2):364-365
Russian Journal of General Chemistry - 相似文献
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Synthesis of 6-chlorotetrazolo[1,5-a]quinazoline and 6-chloro-4,5-dihydrotetrazolo[1,5-a]quinazoline
Skryl’nikova M. A. Khramchikhin A. V. Krivchun M. N. 《Russian Journal of General Chemistry》2017,87(4):885-886
Russian Journal of General Chemistry - Reaction of 5-aminotetrazole triethylammonium salt and 2-fluoro-6-chlorobenzaldehyde resulted in the formation of 6-chlorotetrazolo[1,5-a]quinazoline instead... 相似文献
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