Characterization of a 4-miktoarm star copolymer of the (PS-b-PI)3 PS type by temperature gradient interaction chromatography

Temperature gradient interaction chromatography (TGIC) was applied for the separation of a complex miktoarm star copolymer which has one polystyrene (PS) arm and three polystyrene-b-polyisoprene (PS-b-PI) diblock copolymer arms. Such miktoarm star polymers are much more difficult to characterize than branched homopolymers since the byproduct, typically polymers with missing arm(s) or coupled products, have not only different molecular weights but also different compositions. TGIC was able to fully separate the byproducts, and the composition of the molecular species corresponding to the different separated elution peaks was determined by two methods, fractionation/NMR and multiple detection (UV and RI). A reasonable agreement between the results of the two methods was obtained. By using the composition found, the corresponding molecular weights were determined by multi-angle light scattering detection. Based on the composition and the molecular weight we were able to identify the structure of the different molecular species.     

UP-conversion of terahertz radiation induced by photon drag effect

An all-optical approach to convert terahertz radiation (THz, wavelength λ₁) into infrared (IR, peak wavelength λ₂) is presented. We show that this up-conversion process is due to the photon drag effect induced by the THz radiation in intrinsic narrow-gap semiconductors followed by spatial redistribution of current carriers and band-to-band radiative recombination. The process results in non-selective high-speed (ns range rise/fall times) IR imaging of positive (conventional luminescence) and/or negative (negative luminescence) contrasts. Estimates made for an InSb pixelless converter at 300 K and moderate THz intensity (kW/cm²) show that this up-conversion process (with λ₁/λ₂>10²) can be observed with a conventional thermal imaging camera.     

利用小波变换进行海上目标识别研究

对海面舰船目标类型的识别,通常采用目视判读的方法。由于目视判读的方法不利于大面积侦察任务的快速识别,所以根据海上目标所具有的背景单一、结构复杂的特点,提出了利用小波变换所具有的多分辩率、易于消除噪声、运算方便的特点来提取舰船边缘特征,建立舰船结构特征数据库,实现舰船目标类型的自动判读。试验证明效果很好。     

一种利用Gabor小波特征的目标跟踪方法

小波特征跟踪是一种新的目标跟踪方法。这种方法利用Gabor小波提取目标的边界特征来组成特征模板,并由小波滤波器系数组成特征向量。在跟踪过程中不断优化特征模板的旋转、尺度及平移等几何变形参数,使得小波特征向量值在最小平方和的意义上与初始值相匹配,从而实现目标旋转、尺度及平移等几何变形时的自动跟踪。实验表明,该方法能够有效地跟踪飞机、车辆等目标,并且能够抵抗全局亮度的变化和局部遮挡的干扰。     

一种改进的数字散斑相关方法用于检测人的口型变化

提出了一种基于数字散斑相关测量技术的口型变化检测技术,该技术以白光数字散斑相关测量方法为基础,根据实际应用的需要,引入重心算法并进行了改进,可以实时地检测人说话时的口型变化。通过实验表明,提出的方法是一种实用的、快速、高精度的口型变化测试方法,可为今后的唇语识别技术奠定基础。     

免疫珠技术快速检测腹泻性大肠杆菌

采用表面光滑玻璃珠作为载体材料，用1：40的腹泻性大肠杆菌诊断血清进行包被。可制成免疫珠。这种免疫珠能与腹泻性大肠杆菌发生特异性结合。经乳糖蛋白胨培养液培养，然后根据其产酸产气进行判断。能在18h内完成腹泻性大肠杆菌的检测。其灵敏度为样液中含有腹泻性大肠杆菌数必须大于10CFu／mL．该法简单、快速、易操作、灵敏度高。     

A Liouville type theorem for polyharmonic elliptic systems

In this paper, we consider the polyharmonic system m(−Δ)U=Vq,m(−Δ)V=Up in RN, for m>1, N>2m, with p?1, q?1, but not both equal to 1, where m(−Δ) is the polyharmonic operator. Set α=2m(q+1)/(pq−1), β=2m(p+1)/(pq−1), for α,β∈[(N−2)/2,N−2m), we prove the nonexistence of positive solutions.     

Memory effects in gas chromatographic detection with a microwave-induced plasma

Capillary gas chromatography coupled to microwave-inducedplasma detection furnishes sensitivity adequate for trace analysis when the signal is monitored at a carbon emission line. Work performed with one of these systems at high electronic gain for the carbon signal has revealed solvent band widths in excess of four minutes; these impeded quantification of peaks eluting after the solvent. This report discusses two phenomena which could be related to the unexpected intensity of this solvent response: photomultiplier tube saturation and carbon deposits in the quartz plasma discharge tube.     

High-Throughput Screening of Ten Microcystins and Nodularins, Cyanobacterial Peptide Hepatotoxins, by Reversed-Phase Liquid Chromatography-Electrospray Ionisation Mass Spectrometry

Liquid chromatography-electrospray ionisation mass spectrometry was evaluated in the high-throughput analysis of microcystins and nodularins, cyanobacterial peptide hepatotoxins. Extracts originating from cyanobacterial strains and field material were separated on a 30 mm × 4 mm I.D. Merck Purospher STAR RP-18e column using a rapid gradient of aqueous formic acid and acetonitrile, ionised by electrospray technique and analysed on a Micromass Quattro II triple-quadrupole mass spectrometer operated in the selected ion recording (SIR) mode. The total analysis time per sample was 2.8 min corresponding to 514 samples a day. The system showed good robustness during a series of 320 repetitive injections of a field sample containing three major microcystins.