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1.
《Arabian Journal of Chemistry》2022,15(7):103933
In this study, a fingerprint-activity relationship modeling between chemical fingerprints and antirheumatic activity was established, and multivariate statistical analysis was used to evaluate the quality of Taxilli Herba (TH) from different hosts. Characteristic fingerprints of 20 batches of TH samples were generated by high-performance liquid chromatography coupled with triple quadrupole-time of flight tandem mass spectrometry (HPLC-Triple TOF-MS/MS), and the similarity analysis was calculated based on thirteen common characteristic peaks by hierarchical clustering analysis (HCA). Subsequently, nine efficacy markers were discovered by combining fingerprints and antirheumatic activity through grey correlation analysis (GCA) and bivariate correlation analysis (BCA). Meanwhile, the content of 5 constituents in 9 markers was determined by high-performance liquid chromatography coupled with triple quadrupole-linear ion trap tandem mass spectrometry (HPLC-QTRAP-MS/MS). The comprehensive quality of TH was assessed using multivariate statistical analysis, including principal components analysis (PCA) and technique for order preference by similarity to ideal solution (TOPSIS). The results showed that a high dose of TH extract could markedly ameliorate arthritis damage compared to other doses, with flavonoids playing an important role in the antirheumatic activity. The comprehensive quality of samples from Morus alba L. (SS) was superior to those from Liquidambar formosana Hance (FXS). The present study will demonstrate the markers associated with efficacy, and provide an applicable strategy for more comprehensive quality control and evaluation of TH. 相似文献
2.
针对Mach数8以上(Ma>8)冲压发动机地面试验能力不足问题,基于FD-21高能脉冲风洞,开展了吸气式推进试验技术探索,提升了FD-21风洞的重活塞驱动能力,获得了总压18.66 MPa、总温3 950 K、Ma=9.62、静压436.6 Pa、速度3 km/s的高焓大动压模拟流场,同时发展了高时间分辨率吸收光谱测量技术和基于重模型自由飞原理的发动机推阻测量方法.在此基础上,设计了弯曲激波压缩二元发动机,构建了燃料在线供应与喷注控制、模型悬挂与瞬态释放及相关测量一体的试验系统,在所建立的Ma=9.62风洞模拟环境中进行了集成验证试验,定量测得了有/无氢气射流与空气/氮气超声速气流作用下二元发动机的壁面压力、吸收光谱峰值吸收率、轴向力等数据,并利用纹影观测到了进气道唇口与燃烧室部位的波系特征.多次试验所得的壁面压力、峰值吸收率、轴向力随时间变化曲线均存在2 ms以上的平台,表明二元发动机建立了准定常流动.冷热态及氮气对照组对应的壁面压力分布、峰值吸收率、轴向力等数据呈现出了明显不同,且二者规律近似一致,一方面说明所建立的模拟流场、燃烧诊断技术、发动机推阻测量技术是有效的,另一方面也表明二元发动机实现了点火燃烧、获得有效热功转换,为后续相关研究奠定了良好的基础. 相似文献
3.
Miguel A. Alejo 《Journal of Differential Equations》2018,264(2):1192-1230
We show that breather solutions of the Gardner equation, a natural generalization of the KdV and mKdV equations, are stable. Through a variational approach, we characterize Gardner breathers as minimizers of a new Lyapunov functional and we study the associated spectral problem, through (i) the analysis of the spectrum of explicit linear systems (spectral stability), and controlling degenerated directions by using low regularity conservation laws. 相似文献
4.
5.
Tamar Lando 《Annals of Pure and Applied Logic》2018,169(4):277-311
Space, as we typically represent it in mathematics and physics, is composed of dimensionless, indivisible points. On an alternative, region-based approach to space, extended regions together with the relations of ‘parthood’ and ‘contact’ are taken as primitive; points are represented as mathematical abstractions from regions.Region-based theories of space have been traditionally modeled in regular closed (or regular open) algebras, in work that goes back to [5] and [21]. Recently, logics for region-based theories of space were developed in [3] and [19]. It was shown that these logics have both a nice topological and relational semantics, and that the minimal logic for contact algebras, (defined below), is complete for both.The present paper explores the question of completeness of and its extensions for individual topological spaces of interest: the real line, Cantor space, the rationals, and the infinite binary tree. A second aim is to study a different, algebraic model of logics for region-based theories of space, based on the Lebesgue measure algebra (or algebra of Borel subsets of the real line modulo sets of Lebesgue measure zero). As a model for point-free space, the algebra was first discussed in [2]. The main results of the paper are that is weakly complete for any zero-dimensional, dense-in-itself metric space (including, e.g., Cantor space and the rationals); the extension is weakly complete for the real line and the Lebesgue measure contact algebra. We also prove that the logic is weakly complete for the infinite binary tree. 相似文献
6.
The Gelfand-Levitan-Marchenko representation is used to analyze the initialboundary value problem of two-component nonlinear Schr¨odinger equation on the half-line.It has shown that the global relation can be effectively analyzed by the Gelfand-LevitanMarchenko representation. we also derive expressions for the Dirichlet-to-Neumann map to characterize the unknown boundary values. 相似文献
7.
《Journal of separation science》2018,41(6):1257-1265
Asenapine is a recent drug approved in the European Union for the treatment of bipolar disorder. An original approach has been developed for asenapine analysis in patients treated with the drug, including miniaturized microsampling procedures, separation and quantitation of drug enantiomers. An original enantioselective method based on high‐performance liquid chromatography with diode array detection was developed and applied to the determination of asenapine enantiomer levels in innovative haematic samples: four micromatrices have been tested, two based on dried matrix spots (dried blood spots and dried plasma spots) and two based on volumetric absorptive microsampling (from blood and plasma). Chiral separation was achieved on a cellulose‐tris(3,5 dimethylphenylcarbamate) column, with a mobile phase containing bicarbonate buffer and acetonitrile. The method was validated with satisfactory results of linearity and precision on all matrices that showed also a significant performance in terms of stability, feasibility and reliability, when compared to fluid plasma sampling, handling and processing. Among micromatrices, both volumetric absorptive microsampling types were superior to dried matrix spots in terms of data reproducibility and correspondence with plasma levels. The bioanalytical approach proposed herein provides for the first time a chiral high‐performance liquid chromatographic method for the determination of asenapine enantiomers, coupled to a very effective microsampling strategy. 相似文献
8.
Gangyong Lee Jae Keol Park S. Tariq Rizvi Cosmin S. Roman 《Journal of Pure and Applied Algebra》2018,222(9):2427-2455
Let V be a module with . V is called a quasi-Baer module if for each ideal J of S, for some . On the other hand, V is called a Rickart module if for each , for some . For a module N, the quasi-Baer module hull (resp., the Rickart module hull ) of N, if it exists, is the smallest quasi-Baer (resp., Rickart) overmodule, in a fixed injective hull of N. In this paper, we initiate the study of quasi-Baer and Rickart module hulls. When a ring R is semiprime and ideal intrinsic over its center, it is shown that every finitely generated projective R-module has a quasi-Baer hull. Let R be a Dedekind domain with F its field of fractions and let be any set of R-submodules of . For an R-module with , we show that has a quasi-Baer module hull if and only if is semisimple. This quasi-Baer hull is explicitly described. An example such that has no Rickart module hull is constructed. If N is a module over a Dedekind domain for which is projective and , where is the torsion submodule of N, we show that the quasi-Baer hull of N exists if and only if is semisimple. We prove that the Rickart module hull also exists for such modules N. Furthermore, we provide explicit constructions of and and show that in this situation these two hulls coincide. Among applications, it is shown that if N is a finitely generated module over a Dedekind domain, then N is quasi-Baer if and only if N is Rickart if and only if N is Baer if and only if N is semisimple or torsion-free. For a direct sum of finitely generated modules, where R is a Dedekind domain, we show that N is quasi-Baer if and only if N is Rickart if and only if N is semisimple or torsion-free. Examples exhibiting differences between the notions of a Baer hull, a quasi-Baer hull, and a Rickart hull of a module are presented. Various explicit examples illustrating our results are constructed. 相似文献
9.
《Mathematische Nachrichten》2018,291(2-3):443-491
In this paper, we propose the concepts of Caputo fractional derivatives and Caputo type Hadamard fractional derivatives for piecewise continuous functions. We obtain general solutions of four classes of impulsive fractional differential equations (Theorem 3.1–Theorem 3.4) respectively. These results are applied to converting boundary value problems for impulsive fractional differential equations to integral equations. Some comments are made on recently published papers (see Section 4). 相似文献
10.
Kousuke Kuto Tatsuki Mori Tohru Tsujikawa Shoji Yotsutani 《Journal of Differential Equations》2018,264(9):5928-5949
We consider the Neumann problem of a 1D stationary Allen–Cahn equation with nonlocal term. Our previous paper [4] obtained a local branch of asymmetric solutions which bifurcates from a point on the branch of odd-symmetric solutions. This paper derives the global behavior of the branch of asymmetric solutions, and moreover, determines the set of all solutions to the nonlocal Allen–Cahn equation. Our proof is based on a level set analysis for an integral map associated with the nonlocal term. 相似文献