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1.
Acta Mathematicae Applicatae Sinica, English Series - In this paper, we investigate standing waves in discrete nonlinear Schrödinger equations with nonperiodic bounded potentials. By using the...  相似文献   
2.
Two independent field trials were conducted in Guangdong and Guangxi, South China, in 2013, to study the dissipation, residue levels, and distribution of pyraclostrobin in banana and soil under field conditions. Pyraclostrobin residues were determined through a quick and effective method of high-performance liquid chromatography. Results showed that the average recoveries ranged from 80.55% to 98.08%, with relative standard deviations of 3.18–7.81% at three different spiking levels for each different matrix. The quantification limit of the proposed method was 0.006 mg/kg for both banana and soil. The half-lives of pyraclostrobin in bananas were 9.09 days in Guangdong and 8.26 days in Guangxi, and both bananas exhibited a dissipation rate of 90% after 28 days. The half-lives of pyraclostrobin in soil were 11.61 days in Guangdong and 10.60 days in Guangxi, with a dissipation rate of 90% after 35 days. Although several positive banana samples (i.e., pyraclostrobin exceeding the maximum residue limits (MRL) were found, the terminal residues in banana pulp were not detectable. All the terminal residues in banana pulp were below the MRL of 0.02 mg/kg, set by the Chinese Ministry of Agriculture, indicating a negligible risk associated with the exposure to pyraclostrobin via the consumption of banana. The distribution of pyraclostrobin in soil was also investigated in two experimental sites. The pyraclostrobin in different layer soil was time dependent and did not vary between the two sites. The result also showed that pyraclostrobin could be easily transported from the top soil to the subsoil. However, the highest quantity ratio did not exceed 10% in the bottom layer (20–30 cm). The distribution assessment also revealed that no significant potential environment risk was induced by pyraclostrobin in bananas.  相似文献   
3.
As a nanoparticle support material, carbon nanotubes (CNTs) provide a certain potential activation of catalysis in heterogeneous catalytic organic reactions. Herein, an efficient Ag/CNT‐catalyzed synthesis of enamines via hydroamination of activated alkynes with aromatic amines has been described. This catalyst still retains catalytic activity after being recycled and reused three times. In addition, it represents a green and environmentally friendly process for preparation of enamines. Copyright © 2013 John Wiley & Sons, Ltd.  相似文献   
4.
西瓜中4种植物生长调节剂残留的分析方法研究   总被引:4,自引:0,他引:4  
建立了固相萃取/高效液相色谱法测定西瓜中24-二氯苯氧乙酸(24-D)、赤霉素(GA3)、多效唑(PP333)、6-苄氨基嘌呤(6-BA) 4种植物生长调节剂残留的方法.样品用80%甲醇溶液提取,采用Strata C18固相萃取小柱进行富集、净化,以甲醇-0.15%磷酸水溶液为流动相,梯度洗脱,经ZORBAX Ec...  相似文献   
5.
采用气相色谱-质谱法对韭菜茎和叶的石油醚、三氯甲烷、二氯甲烷、丙酮、乙酸乙酯有机溶剂提取液进行了检测.结果表明:有机溶剂提取液中有二甲基二硫、二甲基三硫、甲基甲烷硫代磺酸盐、二甲基酯硫磺酸、甲基2-丙烯基二硫及杂环等多种含硫化合物,另外还检出较复杂的3-乙烯基-1,2-二硫代杂环己-5-烯类物质.低温条件下,茎中石油醚...  相似文献   
6.
将吡啶-2,4,6-三羧酸(2,4,6-pytaH3),4-氨基-3,5-二(4-吡啶基)-1,2,4-三氮唑(4,4′-abpt)和CoCl2在不同的pH条件下发生水热反应,得到2个新的配位聚合物[Co(2,4,6-pytaH)(4,4′-abpt)(H2O)](1)和[Co1.5(2,4,6-pyta)(4,4′-abpt)(H2O)3].3.5H2O(2)。配合物1是在吡啶-2,4,6-三羧酸酸性环境下产生的,吡啶-2,4,6-三羧酸在水热条件下只脱去2个羧基上的质子变成2,4,6-pytaH2-,而配合物2是在NaOH碱性溶液下反应得到的,其中吡啶-2,4,6-三羧酸完全脱去3个羧基上的质子变成2,4,6-pyta3-。配合物1中包含一维Co-羧酸链,2中存在具有(4,4)拓扑网络的二维层。1和2中的一维链和二维层通过π-π堆积和丰富的氢键作用分别拓展成三维超分子网络。单晶结构分析表明,配合物1结晶于单斜晶系,P21/n空间群,a=0.961 30(10)nm,b=0.632 09(6)nm,c=3.372 9(4)nm,β=95.104(2)°,V=2.041 3(4)nm3,Z=4。而配合物2结晶于单斜晶系,P21/c空间群,a=1.795 2(2)nm,b=0.729 62(8)nm,c=2.078 7(2)nm,β=112.323(2)°,V=2.518 6(5)nm3,Z=4。  相似文献   
7.
This paper is concerned with the adaptive synchronization problem for a class of stochastic delayed neural networks. Based on the LaSalle invariant principle of stochastic differential delay equations and the stochastic analysis theory as well as the adaptive feedback control technique, a linear matrix inequality approach is developed to derive some novel sufficient conditions achieving complete synchronization of unidirectionally coupled stochastic delayed neural networks. In particular, the synchronization criterion considered in this paper is the globally almost surely asymptotic stability of the error dynamical system, which has seldom been applied to investigate the synchronization problem. Moreover, the delays proposed in this paper are time-varying delays and distributed delays, which have rarely been used to study the synchronization problem for coupled stochastic delayed neural networks. Therefore, the results obtained in this paper are more general and useful than those given in the previous literature. Finally, two numerical examples and their simulations are provided to demonstrate the effectiveness of the theoretical results.  相似文献   
8.
借鉴中小制造型企业(SMPEs)在线渠道预售模式,考虑市场中存在预付订金和不预付订金的顾客,并将其退货情况引入到生产商利润表达式中,构建确定性和随机性市场需求下的SMPEs产品销售利润最大化模型,推导生产商产品最优定价的解析解;对比两种销售模式的利润,得到了生产商选择不同销售策略的条件。进一步考虑预付定金的产品数量、预交定金比例、退货数量是关于价格折扣敏感的情况,采用拉格朗日乘子法对生产商产品定价及优化问题进行研究,分析求得生产商销售策略(产品定价和价格折扣)的近似最优解。最后,通过数值算例对研究结论进行了验证并给出经济学解释。  相似文献   
9.
陈创鑫  陈宗煊 《数学学报》2016,59(6):821-834
本文证明了:对具有两个Borel例外值a(∈C)和b(∈C∪{∞})的有限级超越亚纯函数,如果f(z+η)-f(z)和f(z)CM分担a,b,其中η(∈C)满足f(z+η)■f(z),那么b=∞,a=0且f(z)=ce~(c_1z),其中c,c_1为非零常数.  相似文献   
10.
李炜  陈平炎 《数学学报》2010,53(5):881-890
本文获得了B值ρ混合随机元序列的均值收敛性,Kolmogorov强大数定律以及正则和极大值矩的存在性问题,推广和改进了已有的结果.  相似文献   
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