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排序方式: 共有425条查询结果,搜索用时 46 毫秒
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2.
林孝贵 《数学的实践与认识》2014,(7)
我国出口外贸企业将来收到外汇货款又要借款用于生产,企业面临很大人民币汇率利率双重风险,因此迫切需要解决其风险管理问题。可以使用目前市场上交易的人民币外汇远期、外汇期货和利率远期等衍生工具,分别对这两项风险进行独立管理和同步管理。导出策略的回报、风险和效率等统计指标,比较评价这两种风险管理策略的优良性。得到同步管理比独立管理更加优越的结论,企业可以使用同步管理策略更有效地规避所面临的双重风险。 相似文献
3.
M.R.Haddadi 《分析论及其应用》2014,(4):399-404
In this paper, we give some result on the simultaneous proximinal subset and simultaneous Chebyshev in the uniformly convex Banach space. Also we give relation between fixed point theory and simultaneous proximity. 相似文献
4.
胶束毛细管电泳法同时分离四环素与青霉素类药物的研究 总被引:2,自引:0,他引:2
采用胶束毛细管电泳(MEKC),建立了四环素(TCs)和青霉素(PENs)两类7种药物同时分离的方法。考察了MEKC中缓冲液类型、离子浓度和pH值,以及表面活性剂(SDS)浓度、分离电压、温度等参数的影响。利用L16(45)正交试验,确立了最佳的电泳条件:缓冲液为40 mmol/L磷酸二氢钾-20 mmol/L硼砂,添加65 mmol/L SDS,pH 7.9,分离电压28 kV,分离温度28℃,紫外检测波长分别为350 nm和200nm。结果表明:7种药物在25 min内得到完全分离。在1.56~50 mg/L范围内呈良好的线性关系,相关系数(r2)为0.997 9~0.999 9,峰面积的相对标准偏差(n=6)为4.1%~7.3%;迁移时间的相对标准偏差(n=6)为0.33%~0.67%。在2.0,5.0,10.0 mg/kg的加标水平下,7种药物的回收率为83.6%~93.3%,相对标准偏差(n=6)为4.7%~7.6%。该法快速、简便、准确,具有较高的灵敏度,已应用于合肥市及周边地区水塘和湖水中7种药物的快速分离检测。 相似文献
5.
Photonic crystals are nanomaterials with unique structural coloration, and they have been used in multiple analyses, gene function analyses, and nanoarray biosensors. Here, we used agarose hydrogel microcarriers with characteristic reflection peak codes to improve the biocompatibility of the material and the efficiency of detection, which may be helpful for further clinical applications. The paper has two parts: condition optimization and product application. Goat antihuman immune globulin G, human immune globulin G, and fluorescein isothiocyanate-labeled goat antihuman immune globulin G are commonly used materials in double-antibody sandwich techniques, which are used for optimization in the application of advanced composite materials. Goat antihuman immune globulin G was immobilized on the surfaces of photonic crystal hydrogel beads through chemical bonding. When the target immune globulin G was captured, the fluorescence-labeled antibody could combine with photonic crystal hydrogel beads. The reaction conditions were optimized using the gray-scale value of fluorescent intensities. Photonic crystal hydrogel beads with different reflection spectra were coated with purified platelet glycoprotein IIb/IIIa and glycoprotein Ib/IX. A total of 64 clinical samples including sera from patients with immune thrombocytopenia (n?=?32) and healthy human sera (n?=?32) were tested using photonic crystal hydrogel beads and monoclonal antibody immobilization of platelet antigen (MAIPA). Photonic crystal hydrogel bead array reaction conditions were established for multiple analysis, showing similar sensitivity and specificity with MAIPA in testing different platelet antibodies and shortening the analysis time. The features of these composite materials make them suitable for potential applications in clinical screening assays. 相似文献
6.
针对Wollaston棱镜和Savart偏光镜(SP)组合的差分成像光谱系统存在光线溢出和无法改变系统光程等问题,设计了一种新型双通道差分偏振干涉成像系统.此系统不仅可获取正交偏振图像,还可以通过调整Savart偏光镜的厚度来改变系统光程.介绍了该系统的结构、理论原理,并利用琼斯矩阵推导出四束偏振光线的复振幅及其相干光干涉强度表达式.分析了宽视场Savart偏光镜(WSP)和可调光程的Savart偏光镜(MSP)的分束特性,得出WSP相较于SP具有更好的剪切能力和WSP可优化系统光路的结论.获得了不同楔形结构角下MSP的光程差、横向剪切量随楔形移动量的变化曲线.通过实验验证,获取了不同剪切量下的干涉图像和复色光下平行、垂直分量的空间图像,进而获得了总的强度图像和差分强度图像.得出差分强度图像相较于偏振强度图像具有较高对比度的结论.研究结果对双通道成像光谱系统的性能优化具有一定的参考意义. 相似文献
7.
《Journal of separation science》2018,41(2):440-448
The chromatographic separation of several isomeric anilines is a challenging issue. Herein, a simple method for the simultaneous determination of four groups of isomeric primary aromatic amines, including chloroanilines, methylanilines, methoxylanilines, and dimethylanilines, was presented. In this method, all of the 15 primary aromatic amines were easily transformed into the corresponding imine derivative by treatment with benzaldehyde under mild conditions. The formed isomeric imine derivatives were completely separated on a commercial capillary gas chromatography column. The effects of several derivatization parameters were investigated and optimized. Linearity in the optimized method ranged from 0.050 to 50 μg/mL with the squared correlation coefficients (R2) between 0.9981 and 0.9999. Reasonable reproducibility was obtained, with the intraday relative standard deviation (N = 5) ranging from 0.89 to 4.57% and interday relative standard deviation ranging from 2.26 to 7.69% at the concentration of 5.0 μg/mL. The developed method has been successfully applied to determine these isomeric aromatic amines in real samples. 相似文献
8.
Simultaneous determination of caffeic acid and its major pharmacologically active metabolites in rat plasma by LC‐MS/MS and its application in pharmacokinetic study 下载免费PDF全文
Xiangyang Wang Wei Li Xiaohui Ma Yang Chu Shuming Li Jiahua Guo Yumeng Jia Shuiping Zhou Yonghong Zhu Changxiao Liu 《Biomedical chromatography : BMC》2015,29(4):552-559
A simple, sensitive and selective high‐performance liquid chromatography electrospray ionization tandem mass spectrometry (LC‐MS/MS) method was developed for simultaneous determination and pharmacokinetic study of caffeic acid (CA) and its active metabolites. The separation with isocratic elution used a mobile phase composed of methanol and water (containing 0.1% formic acid) at a flow rate of 0.2 mL/min. The detection of target compounds was done in selected reaction monitoring (SRM) mode. The SRM detection was operated in the negative electrospray ionization mode using the transitions m/z 179 ([M ? H]?) → 135 for CA, m/z 193 ([M ? H]?) → 134.8 for ferulic acid and isoferulic acid and m/z 153 ([M ? H]?) → 108 for protocatechuic acid. The method was linear for all analytes over the investigated range with all correlation coefficients 0.9931. The lower limits of quantification were 5.0 ng/mL for analytes. The intra‐ and inter‐day precisions (relative standard deviation) were <5.86 and <6.52%, and accuracy (relative error) was between ?5.95 and 0.35% (n = 6). The developed method was applied to study the pharmacokinetics of CA and its major active metabolites in rat plasma after oral and intravenous administration of CA. Copyright © 2014 John Wiley & Sons, Ltd. 相似文献
9.
J. Engel L. Blanchet B. Bloemen L.P. van den Heuvel U.H.F. Engelke R.A. Wevers L.M.C. Buydens 《Analytica chimica acta》2015
Many advanced metabolomics experiments currently lead to data where a large number of response variables were measured while one or several factors were changed. Often the number of response variables vastly exceeds the sample size and well-established techniques such as multivariate analysis of variance (MANOVA) cannot be used to analyze the data. 相似文献
10.
经辉 《中国无机分析化学》2015,5(3):34-40
建立了X射线荧光光谱法测定矿石样品中铀、钍含量的快速分析方法。采用高压粉末制样法,对不同含量的放射性样品的压片压力、粒径、含水率、用量等处理条件到进行单因素实验。在400 MPa压力下压制,克服了低压制样的弊端,制备的样片表面光滑、致密,大幅改善了制样重现性,有效地减少了部分基体效应,铀校准曲线的标准偏差从0.053%降到0.0071%,钍校准曲线的标准偏差从0.062%降到0.0057%。经国家一级标准物质验证,表明方法准确、可靠,能满足样品中铀、钍含量日常分析要求。 相似文献