排序方式: 共有27条查询结果,搜索用时 55 毫秒
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主要基于紫外可见(UV-Vis)漫反射光谱首次对比研究了经过热处理、有机或无机染料改色或钴-60产生的γ射线辐照三种不同处理工艺对同为珍珠质的淡水与海水珍珠及贝壳珍珠层的漫反射光谱的影响机制。结果表明:(1)在不同颜色、淡海水属性的珍珠与贝壳珍珠层的UV-Vis反射光谱的紫外区皆存在约280 nm 处的吸收峰,上述吸收峰位归属于珍珠层中自身存在的有机质所致,而非珍珠的致色色素。(2)以上三种不同的处理工艺对上述280 nm处的吸收峰位存在一致的影响行为,即随着不同的处理工艺强度的增大,处理样品对应的反射谱图中约280 nm处吸收峰的强度逐渐降低直至消失。与此同时,珍珠的反射谱图中紫外区的反射主波长的反射强度也随之减弱,且反射主波长的峰位向可见光区发生显著红移。研究工作可为珍珠及珍珠的优化处理的鉴定筛选及其珍珠颜色的形成属性判定提供检测依据与理论支撑。 相似文献
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The characterization of dielectric materials in space environment requires to understand and predict their electric behaviour, taking into account ionisation, and ageing effect (through electron or UV radiation, thermal cycling, …)For this purpose, new methods have been developed for the characterisation and qualification of space materials and satellite structure. These studies led initially to the development of dedicated facilities for the simulation of representative irradiation conditions. This work is focused on a new non-disturbing technique for the measurement of charge distribution within space irradiated polymers. This technique named PEA (Pulsed Electro-Acoustic) has been implemented in the irradiation facility for in-situ and real time measurement during irradiation and relaxation of polymer materials. Implementation and validation of this technique are presented and discussed in this paper. 相似文献
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Prof. Dr. Guobing Yan 《Chemistry (Weinheim an der Bergstrasse, Germany)》2022,28(29):e202200231
Hydrodefluorination (HDF) is a very important fundamental transformation for conversion of the C−F bond into the C−H bond in organic synthesis. In the past decade, much progress has been achieved with HDF through the utility of low-valent metals, transition-metal complexes and main-group Lewis acids. Recently, novel methods have been introduced for this purpose through photo- and electrochemical pathways, which are of great significance, due to their considerable environmental and economical advantages. This Review highlights the HDF of fluorinated organic compounds (FOCs) through photo- and electrochemical strategies, along with mechanistic insights. 相似文献
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研究采用视频分析法,利用NVivo软件,以东芝杯教学技能创新大赛的化学组选手为对象,从教学理念、教学情境、实验设计和教学手段等4个维度,评价卓越职前化学教师课堂教学的创新能力。结果发现:教学理念新颖,但具体落实尚有不足;情境创设生动,但主题与学生的联系不够紧密;实验设计别致,但在水平上还有提升空间;教学技术手段先进,但还需要深度融合。研究为创新型卓越化学教师的培养提供了启示。 相似文献
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15波长输出的布里渊掺铒光纤激光器 总被引:8,自引:3,他引:5
多波长布里渊掺铒光纤激光器是一种新型的多波长光纤激光器,其原理是利用受激布里渊增益和掺铒光纤的线性增益,可以在常温下得到波长间隔约为0.08nm(~10GHz)的多波长输出。报道的布里渊掺铒光纤激光器,在布里渊抽运功率为1.7mW、980nm抽运功率为300mW的情况下得到稳定的15个波长(间隔~10GHz)的输出,这种激光器用作光传感器、光谱分析仪以及密集波分复用系统的光源。实验发现,输出波长的个数随着980nm抽运功率的增大而增加。另外,布里渊掺铒光纤激光器的信号功率主要来自于掺铒光纤的增益,而布里渊增益对它的影响不大。 相似文献
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??We study the linear quadratic optimal stochastic control problem which is jointly driven by Brownian motion and L\'{e}vy processes. We prove that the new affine stochastic differential adjoint equation exists an inverse process by applying the profound section theorem. Applying for the Bellman's principle of quasilinearization and a monotone iterative convergence method, we prove the existence and uniqueness of the solution of the backward Riccati differential equation. Finally, we prove that the optimal feedback control exists, and the value function is composed of the initial value of the solution of the related backward Riccati differential equation and the related adjoint equation. 相似文献
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《Current Applied Physics》2018,18(11):1403-1409
In the present study, the SrMoO4:Eu3+ phosphors has been synthesized through hydro-thermal co-precipitation method, and single factor and orthogonal experiment method was adopted to find optimal synthesis condition. It is interesting to note that hydro-thermal temperature is a prominent effect on the luminescent intensity of SrMoO4:Eu3+ red phosphor, followed by co-precipitation temperature, calcining time, and the doping amount of Eu3+. The optimal synthesis conditions were obtained: hydro-thermal temperature is 145 °C, co-precipitation temperature is 35 °C, the calcining time is 2.5 h, and the doping amount of activator Eu3+ is 25%. Subsequently, the crystalline particle size, phase composition and morphology of the synthesized phosphors were evaluated by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The results show that these phosphors possess a scheelite-type tetragonal structure, and the particle size is about 0.2 μm. Spectroscopic investigations of the synthesized phosphors are carried out with the help of photo-luminescence excitation and emission analysis. The studies reveal that SrMoO4: Eu3+ phosphor efficiently convert radiation of 394 nm–592 and 616 nm for red light, and the luminescence intensity of SrMoO4:Eu3+ phosphors is improved. SrMoO4:Eu3+ phosphors may be a potential application for enhancing the efficiency of white LEDs. 相似文献