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排序方式: 共有134条查询结果,搜索用时 15 毫秒
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Qingsong xu Jianguo Tang Yao Wang Jixian Liu Zhen Huang Linjun Huang Aihua Li YuanWang Laurence A. Belfiore 《Particuology》2013,11(6):748-752
Conductive carbon nanotubes (CNTs) or alternatively polyaniline (PANI) nano-blocks was introduced into aqueous solutions of polyvinyl alcohol (PVA) and copper (II) salt, to assist the reduction of copper (II) ions and the anchoring of the resulting copper nanoparticles onto the conductive blocks. The mixture solutions of nano-blocks, copper (lI) salts and PVA were spin-coated onto the cathode surface, forming swollen cathode films (SCFs). The copper (II) ions in the film assembled onto the surfaces of the conductive blocks and were then reduced under an appropriate voltage. It is important that the copper nanoparticles grew only on the surfaces of the conductive blocks. PVA which acted as the matrix of the composites played a role in stabilizing the resulting copper nanoparticles. Morphologies of these polymeric composite films were studied by various characterization methods. Moreover, the mechanism of migration of copper (II) ions, the formation of these polymeric composites, and the overall procedure were investigated in detail. 相似文献
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Kun‐ze Du Jin Li Lanhui Wang Jia Hao Xue‐jing Yang Xiu‐mei Gao Yan‐xu Chang 《Journal of separation science》2020,43(4):799-807
Hydrosoluble trehalose lipid (a biosurfactant) was employed for the first time as a green extraction solution to extract the main antioxidant compounds (geniposidic acid, chlorogenic acid, caffeic acid, and rutin) from functional plant tea (Eucommia ulmoides leaves). Single‐factor tests and response surface methodology were employed to optimize the extraction conditions for ultrasound‐assisted micellar extraction combined with ultra‐high‐performance liquid chromatography in succession. A Box‐Behnken design (three‐level, three‐factorial) was used to determine the effects of extraction solvent concentration (1–5 mg/mL), extraction solvent volume (5–15 mL), and extraction time (20–40 min) at a uniform ultrasonic power and temperature. In consequence, the best analyte extraction yields could be attained when the trehalose lipid solution concentration was prepared at 3 mg/mL, the trehalose lipid solution volume was 10 mL and the extraction time was set to 35 min. In addition, the recoveries of the antioxidants from Eucommia ulmoides leaves analyzed by this analytical method ranged from 98.2 to 102%. These results indicated that biosurfactant‐enhanced ultrasound‐assisted micellar extraction coupled with a simple ultra‐high‐performance liquid chromatography method could be effectively applied in the extraction and analysis of antioxidants from Eucommia ulmoides leaf samples. 相似文献
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高温偶极子发射换能器是200℃高温多极子阵列声波测井仪器研发需要攻克的主要核心关键技术问题之一。针对这一问题,该文从材料选型和工艺改良两个方面开展技术攻关,研发了耐温达200℃偶极子发射换能器,样机耐温性能测试表明其能够在200℃下连续工作12 h而不损坏,声性能测试样机最大发射电压响应为124 dB,具有与现用换能器相当的辐射性能,样机尺寸及工作频率与现用换能器几乎完全一致,可以方便地对现用仪器进行升级。目前搭载该样机的仪器已经通过孤古8实验井测试,并在新疆顺北油田现场近9000 m井下取得高质量数据,达到设计目的。该文为开展更高温换能器研发提供了详细的研究思路。 相似文献
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针对产品开发过程中某柴油车型发动机油底壳怠速时“呜呜”异响问题,通过噪声与振动的测试及仿真分析,对油底壳异响原因进行分析。结果表明,怠速时机油泵的工作激励频率与油底壳模态频率耦合,形成“呜呜”声,并通过油底壳表面辐射出来。进一步实验研究表明,随着机油温度的升高,机油泵功率、工作激励幅值会逐步减小,异响逐步减小。同时实验研究表明,机油量对油底壳模态频率有影响,油底壳内机油加注量越多,油底壳模态频率越低,油底壳表面振动幅值及异响均逐步减小。针对该异响问题,明确该发动机机油加注上限及下限时油底壳对应频率范围后,通过优化怠速转速,提高油底壳模态频率等使机油泵激励频率与油底壳模态频率避频,解决了该异响问题。 相似文献
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Xu xu 《应用数学和力学(英文版)》2009,30(3)
Based on curve fitting of coefficients of three component forces of the Messina Straits Bridge, and the previously proposed semi-analytical expressions of flutter deriva-tives of flexible structure, the change of flutter derivatives of slender bridge cross-section with respect to its aerodynamic center, rotational speed and angle variation is studied using a parametric method. The calculated results are compared with the measured ones, and expressions of flutter derivatives of the Messina Straits Bridge are derived. The in-trinsic relationships existing in flutter derivatives are validated again. It is shown that the influence of the rotational speed on flutter derivatives is not negligible. Therefore, it provides an additional semi-analytical approach for analyzing flutter derivatives of the bridge with streamlined cross-section to get its aerodynamic information. 相似文献
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粉状工业炸药配方设计的数学模型 总被引:8,自引:1,他引:7
论述了含C、H、O、N、Al元素的工业炸药配方设计数学模型的建构方法 ,研究了无梯硝铵炸药、铵梯油炸药和含铝铵梯油炸药配方设计及最优化的数学模型 ,给出了上述几种粉状工业炸药配方设计及最优化数学模型的计算结果。对用理论配方所制工业炸药的爆炸性能也进行了研究 ,以证实数学模型的可靠性。 相似文献
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