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Karger-Kocsis J. Shang P. P. Moskala E. J. 《Journal of Thermal Analysis and Calorimetry》1999,55(1):21-28
The tensile loading-induced necking in notched specimens of an amorphous copolyester (aCOP) was studied by modulated differential
scanning calorimetry (MDSC). It was shown that necking occurred by cold drawing since the enthalpy of cold crystallization
and that of the subsequent melting agreed fairly with each other. Increasing deformation in the necking zone and increasing
deformation rate of the specimens shifted the onset of cold crystallization toward lower temperatures and yielded a slightly
higher glass transition temperature (Tg). This was attributed to the molecular orientation caused by mechanical loading. The finding that the melting contained a
non-reversing part was considered as appearance of possible microcrystallinity. The Tg range was strongly influenced by the deformation rate and reflects the thermomechanical history of the samples accordingly.
This revised version was published online in August 2006 with corrections to the Cover Date. 相似文献
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R. N. Haward 《Journal of Polymer Science.Polymer Physics》1995,33(10):1481-1494
The Gaussian expression for the isothermal tensile deformation of thermoplastics including the proposed strain hardening constant Gp, has been combined with the Eyring flow equation to provide a new relation describing the rate of strain of a thermoplastic in terms of the true stress and the extension ratio under isothermal conditions. In conventional mechanical tests this model can be used to quantify the tendency to strain localization, to predict the natural draw ratio and the inversion point where the true engineering stress passes through a minimum. The latter is expected to correlate with the value of the extension ratio where crazes do not propagate under tension. The equation is most easily demonstrated in constant load experiments where they agree well with published work. However, for a more precise evaluation of the theory the constant Gp should be measured separately and the calculated results compared with other tests on the same material. Where necking occurs it is possible to use a simplified plug flow model to calculate neck profiles. These show that no special assumptions are required to account for necking which results directly from the interaction of geometric thinning and strain hardening, even where true strain softening is absent. The procedure makes it possible to illustrate the way in which the form of the neck can be affected by the rate of extension or in a constant load experiment by the applied load. ©1995 John Wiley & Sons, Inc. 相似文献
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On the plastic deformation of bulk syndiotactic polypropylene 总被引:1,自引:0,他引:1
The plastic deformation of syndiotactic polypropylene (sPP) bulk samples has been investigated. A structural comparison of
the initial states before and after plastic deformation by necking is carried out by X-ray diffraction observations. Independent
of the initial states (amorphous, semi-crystalline with different crystal phases), only the planar all-trans crystal form of sPP is present in the deformed samples after necking. Form these results, molecular mechanisms of the plastic
deformation in the neck zone of semi-crystalline polymers will be discussed.
Received: 11 February 1997 Accepted: 15 August 1997 相似文献
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Dhammaraj Rokade Lal B. Azad Suparna Poddar Satyendra Mishra Harshawardhan V. Pol 《Journal of Macromolecular Science: Physics》2017,56(4):213-233
The research described was concerned with the effect of layered-silicate-based organically modified nanoclay fillers on controlling the extent of necking in a polymer melt extrusion film casting (EFC) process. We show that a linear polythylene resin (such as a linear low-density polyethylene—LLDPE) filled with a very low percentage of well-dispersed (or intercalated) nanoclay displays an enhanced resistance to the necking phenomenon. In general, melt-compounded nanoclay-filled LLDPE resin formulations displayed a higher final film width (less necking), thus a lower final film thickness (greater draw down for the same draw ratio), and cooled down faster when compared to the base LLDPE resin. Incorporation of nanoclay filler in the mainly linear chain LLDPE resin led to significant modification of the melt rheological properties that, in turn, affected the melt processability of these formulations. Primarily, the intercalated nanoclay-filled LLDPE formulations displayed the presence of strain-hardening in unaxial extensional rheology. Additionally, the presence of well-dispersed nanoclay in the LLDPE resin led to a display of prominent extrudate swell indicating the presence of melt elasticity in such formulations. The presence of melt elasticity, as shown by shear rheology and strain-hardening, observed by uniaxial extensional rheology, contributed to the LLDPE nanoclay formulations displaying an enhanced resistance to necking for these films. It can be concluded that linear chain polymers susceptible to necking in an EFC process can be made more resistant to such necking by using nanoclay fillers at very low levels of loading. 相似文献
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The tensile and compression tests were performed on zinc single crystals oriented for slip in the basal slip system. During the first stage of the stress–strain curve, the localized necking was typical of strain localization in the tensile specimens. Single or multiple necks were formed along the specimen length. The range of temperatures and the strain rates for single necking of the sample was determined. The formation of such necking depends on strain hardening characteristics and can be predicted by the Considère criterion. On the other hand, propagation of the necked area along the sample length was not predictable by this criterion. Localized sliding and specimen kinking was indicative of the strain localization observed for different specimens compressed under the same conditions, i.e. temperature and strain rate. A decrease in the compression force and in the cross-sectional area with anvil displacements produced localized sliding. On the other hand, a continuous increase in the compression force was representative of tests leading to specimen kinking. 相似文献
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This paper presents the application of Moire interferometry in measuring the displacement and strain field at notch-tip and
crack-tip before and after crack propagation. The experiment is carried out using a three point bending beam with a notch.
TheN
x andN
y fringe patterns representing displacement field, and the ΔN
x/Δx and ΔN
γ/Δγ fringe patterns representing the strain field are obtained. The sensitivity of the measured displacement is 0.417 μm per
fringe order. The displacement and strain distribution along the sectionx=0 have been worked out according toN
x andN
γ fringe patterns.
The project supported by Chinese Academy of Sciences and National Natural Science Foundation of China 相似文献
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Tang C.Y. Fan Jianping Tsui C.P. 《Acta Mechanica Solida Sinica》2006,19(2):174-180
This paper presents the application of anisotropic damage theory to the study of forming limit diagram of A12024T3 aluminum alloy sheet. In the prediction of limiting strains of the aluminum sheet structure, a finite element cell model has been constructed. The cell model consists of two phases, the aluminum alloy matrix and the intermetallic cluster. The material behavior of the aluminum alloy matrix is described with a fully coupled elasto-plastic damage constitutive equation. The intermetallic cluster is assumed to be elastic and brittle. By varying the stretching ratio, the limiting strains of the sheet under biaxial stretching have been predicted by using the necking criterion proposed. The prediction is in good agreement with the experimental findings. Moreover, the finite element cell model can provide information for understanding the microscopic damage mechanism of the aluminum alloy. Over-estimation of the limit strains may result if the effect of material damage is ignored in the sheet metal forming study. 相似文献