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1.
采用固相膜萃取-气相色谱法测定养殖用水中乐果、甲基对硫磷和马拉硫磷等3种有机磷农药的含量。水样经C18固相萃取膜萃取后,用丙酮和二氯甲烷洗脱。用SPB-608毛细管色谱柱分离,氮磷检测器检测。3种有机磷农药的质量浓度均在0.02~1.0μg·L-1范围内与其峰面积呈线性关系,方法的检出限(3S/N)在0.0025~0.004μg·L-1之间。以空白样品为基体进行加标回收试验,回收率在93.0%~111%之间,测定值的相对标准偏差(n=5)在0.13%~5.2%之间。 相似文献
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The dynamic response of submerged and confined disk-like structures is of interest in engineering applications, such as in hydraulic turbine runners. This response is difficult to be estimated with accuracy due to the strong influence of the boundary conditions. Small radial gaps as well as short axial distances to rigid surfaces greatly modify the dynamic response because of the added mass and damping effects.In this paper, the influence of the axial nearby rigid distance on the dynamic response of a submerged disk is evaluated when the radial gap is very small. Moreover, the effects of the fluid depth and fluid viscosity on the natural frequencies and damping ratio of the submerged disk are studied. The study has been performed experimentally and numerically using structural–acoustic simulations.For the experimental investigation a test rig has been developed. It consists of a disk attached to a shaft and confined with a small radial gap inside a cylindrical container full of water. The disk can be moved up and down along the shaft to vary the axial distance to the nearby rigid surface. Piezoelectric patches are used to excite the disk and the response is measured with submersible accelerometers. Several excitation patterns can be used due to the disposition of these piezoelectric patches. For each configuration tested, the dynamic response of the structure is studied analyzing the natural frequencies and damping ratio of the disk attached to the shaft. The numerical results have been compared with the experimental results. 相似文献
4.
A nanofluid is composed of a base fluid component and nanoparticles, in which the nanoparticles are dispersed in the base fluid. The addition of nanoparticles into a base fluid can remarkably improve the thermal conductivity of the nanofluid, and such an increment of thermal conductivity can play an important role in improving the heat transfer rate of the base fluid. Further, the dynamics of non-Newtonian fluids along with nanoparticles is quite interesting with numerous industrial applications. The present predominately predictive modeling studies the flow of the viscoelastic Oldroyd-B fluid over a rotating disk in the presence of nanoparticles. A progressive amendment in the heat and concentration equations is made by exploiting the Cattaneo-Christov heat and mass flux expressions. The characteristic of the Lorentz force due to the magnetic field applied normal to the disk is studied. The Buongiorno model together with the Cattaneo-Christov theory is implemented in the Oldroyd-B nanofluid flow to investigate the heat and mass transport mechanism. This theory predicts the characteristics of the fluid thermal and solutal relaxation time on the boundary layer flow. The von K′arm′an similarity functions are utilized to convert the partial differential equations(PDEs) into ordinary differential equations(ODEs). A homotopic approach for obtaining the analytical solutions to the governing nonlinear problem is carried out. The graphical results are obtained for the velocity field, temperature, and concentration distributions. Comparisons are made for a limiting case between the numerical and analytical solutions, and the results are found in good agreement. The results reveal that the thermal and solutal relaxation time parameters diminish the temperature and concentration distributions, respectively. The axial flow decreases in the downward direction for higher values of the retardation time parameter. The impact of the thermophoresis parameter boosts the temperature distribution. 相似文献
5.
Interaction of forced and self-sustained vibrations of one disk rotor is described by nonlinear finite-degree-of-freedom dynamical system. The shaft of the rotor is supported by two journal bearings. The combination of the shooting technique and the continuation algorithm is used to study the rotor periodic vibrations. The Floquet multipliers are calculated to analyze periodic vibrations stability. The results of periodic motions analysis are shown on the frequency response. The quasi-periodic motions are investigated. These nonlinear vibrations coexist with the periodic forced vibrations. 相似文献
6.
在红外探测器的应用中,常用统计分析、算例验证等方法研究目标成像精确定位问题。鉴于上述方法难以充分阐释物理意义与揭示普遍规律,提出基于能量分布及成像特征的分析方法,针对红外探测目标成像精确定位问题,利用能量分布和数字图像中成像规律,研究像点定位及精度分析。研究了红外目标成像和数字图像特点,建立了定位模型和方法流程;分析了定位误差影响因素,实现了定位结果精度评定;最后结合典型应用实例,进行了计算验证。该方法与已有方法相比,分析过程更直观,获取了红外像点定位分析的理论依据,并给出了定位结果的精度水平:通常红外成像应用中,精度优于1/6像元;在成像较大时,精度可达1/10像元以上。该研究结论对红外探测应用中目标准确定位具有重要意义。 相似文献
7.
图的交叉数是图的一个重要参数,研究图的交叉数问题是拓扑图论中的前沿难题.确定图的交叉数是NP-难问题,因为其难度,能够确定交叉数的图类很少.通过圆盘画法途径,确定了一个特殊6点图与n个孤立点nK_1,路P_n及圈C_n的联图的交叉数分别是cr(Q+nK_1)=Z(6,n)+2[n/2],cr(Q+P_n)=Z(6,n)+2[n/2]+1及cr(Q+C_n)=Z(6,n)+2[n/2]+3. 相似文献
8.
采用中心波长为940nm的激光二极管泵浦,实现了Yb:YAG薄片的Cr4+:YAG被动调Q激光输出.Yb:YAG薄片掺杂Yb3+离子浓度为10%,厚度为500μm.理论上计算了Yb:YAG薄片在直接水冷方式与不同厚度SiC冷却方式下的温度分布.实验中采用厚度800μm的SiC冷却方式,获得了最高功率2.8 W的1 030nm连续激光输出,输出功率相比直接水冷方式提高了40%.通过Degnan理论优化了被动调Q晶体Cr4+:YAG的初始透过率和输出耦合镜,采用初始透过率为93%的Cr4+:YAG晶体和透过率为10%的输出耦合镜,在800μm SiC冷却方式下,获得了平均输出功率1.95 W、单脉冲能量1.2mJ、脉冲宽度74ns、重复频率1.6kHz的稳定调Q脉冲输出,斜效率为18.1%.光束质量因子M2x=1.622,M2y=1.616. 相似文献
9.
Making use of the fractional differential operator, we impose and study a new class of analytic functions in the unit disk (type fractional differential equation). The main object of this paper is to investigate inclusion relations, coefficient bound for this class. Moreover, we discuss some geometric properties of the fractional differential operator. 相似文献
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