93型精密控温煮解电炉介绍

93型精密控温煮解电炉,采用了大型集成化电路设计方法,对化学分析加热控温煮解过程进行数字直观显示。它集于国内外化学分析不同加热煮解类设备功能于一体,填补了化学分析由室温～600℃加热连续自动精密控温煮解技术一项空白。和分析方法密切配合,为实现化学分析质量登上准、稳、快、省全新台阶和分析技术工作效率长足发展提供了一个理想的工具。     

同步辐射X射线和中子粉末衍射及Rietveld精化（1）

把Rietveld精化方法用于处理同步辐射X射线和中子粉末衍射数据，使得粉末试样的结构研究有很大发展。本文在简要介绍两种粉末衍射术和Rietveld方法之后，用实例描述它们在结构精化、解未知结构、沸石、有关微孔材料及磁结构材料测定中的应用。     

高能质子辐射作用的分子机理——DNA空间结构微观损伤的Raman光谱特征

高能质子是空间辐射的重要类型。本文用激光Raman光谱技术,研究了高能质子(27.9 MeV)对水溶液中DNA辐射作用的分子机理。通过解析其特征Raman谱线,获得DNA空间结构微观损伤的以下信息:(1)维系双螺旋结构的碱基间氢键部分断裂;(2)4种碱基均被损伤,其中腺嘌呤环的破坏最重;(3)脱氧核糖发生了明显的变化;(4)骨架磷酸离子(PO_2~-)和磷酸二酯(PO_2)的损伤严重,并出现单、双链的断裂;(5)B型构象的数量显著减少。     

不同管电压下前瞻性心电门控双源CT诊断冠心病的比较分析

本研究探讨前瞻性心电门控双源CT低管电压在冠心病诊断中的应用价值。回顾性选取60例冠心病患者,根据管电压分为观察组(管电压80 kV)和对照组(管电压100 kV),观察两组诊断情况、图像质量等差异。观察组和对照组诊断冠状动脉狭窄的灵敏性、特异性、准确性、阳性预测值、阴性预测值、冠状动脉节段图像质量评分比较,差异无统计学意义(P>0.05)。观察组和对照组升主动脉根部、右冠状动脉开口、左冠状动脉开口管腔CT值、信噪比(SNR)和对比噪声比(CNR)比较,差异无统计学意义(P>0.05)。观察组剂量长度乘积(DLP)、容积CT剂量指数(CTDIvol)和有效辐射剂量(ED)明显低于对照组(P<0.05)。观察组心率<75次/分患者冠状动脉节段图像质量优于心率≥75次/分患者(P<0.05)。因此,前瞻性心电门控双源CT低管电压在冠心病诊断中有较好的应用价值,具有图像质量好、辐射剂量低等优点,同时心率会影响图像质量。     

Decomposition Reaction of Zn-MPA（3-Mercaptopropionic Acid） Complex Under Microwave Irradiation

The thermal decomposition of Zn-MPA complex was investigated under microwave irradiation. ZnO and ZnS nanocrystals could be obtained by decomposing Zn-MPA（3-mercaptopropionic acid） complex under different reaction conditions. It was found that both the pH value of the solution and the molar ratio of Zn2＋ and MPA can play an important role in the formation of ZnO and ZnS nanocrystals. MPA mainly acts as an S source or as a complexing agent. This study provides a new route for the controllable preparation of semiconductor nanocrystals.     

固体材料激光冷却的实验研究及其最新进展

近年来，基于反斯托克斯荧光制冷(Anti—Stokes Fluorescent Cooling)的固体材料激光冷却技术得到了快速发展。本文首先简单介绍了固体材料激光冷却的基本原理及其技术；其次，详细介绍了各种固体激光冷却的新材料、新方案和新结果及其最新实验进展；最后，就固体激光冷却技术的应用前景及其未来发展方向等问题进行了简单讨论与展望。     

Experimental characterization and correction of non-equivalence of Solar Irradiance Absolute Radiometer

We experimentally evaluate and correct the non-equivalence between electrical and radiative heating of solar irradiance absolute radiometer to compensate the systematic error of radiant power measurement at ambient pressure. A relative difference of the order of 0.08%-0.27% between electrical and radiative heating sensitivities is shown, and the resulting non-equivalence correction factor is calculated. The radiant power measurement equation is modified using the non-equivalence correction factor, a systematic deviation of 0.19% of radiant power measurement is hence eliminated.     

Energy spectrum of multi-radiation of X-rays in a low energy Mather-type plasma focus device

The multi-radiation of X-rays was investigated with special attention to their energy spectrum in a Mather-type plasma focus device （operated with argon gas）. The analysis is based on the effect of anomalous resistances. To study the energy spectrum, a four-channel diode X-ray spectrometer was used along with a special set of filters. The filters were suitable for detection of medium range X-rays as well as hard X-rays with energy exceeding 30 keV. The results indicate that the anomalous resistivity effect during the post pinch phase may cause multi-radiation of X-rays with a total duration of 300 ± 50 ns. The significant contribution of Cu-Kα was due to the medium range X-rays, nonetheless, hard X-rays with energies greater than 15 keV also participate in the process. The total emitted X-ray energy in the forms of Cu-K and Cu-K/3 was around 0.14 ± 0.02 （J/Sr） and 0.04 ±0.01 （J/Sr）, respectively. The total energy of the emitted hard X-ray （〉 15 keV） was around 0.12± 0.02 （J/Sr）.