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建立了柱前衍生-高效液相法测定水中二甲基二硫代氨基甲酸钠(DTC)含量的方法。水样中的DTC和钴离子柱前衍生为稳定的络合物,用乙腈复溶解后采用C18色谱柱,以乙腈/水(60/40)为流动相等度洗脱,在257 nm波长下进行检测。结果表明,在0~100.0 mg/L范围内,DTC的质量浓度与对应的峰面积线性关系良好,方法的检出限为0.07 mg/L,DTC在水样中的平均回收率为99.3%,精密度(RSD)为2.5%。该方法准确、可靠,操作简便,可应用于快速检测水中DTC的含量。 相似文献
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设导流墩排沙漏斗清水流场的测试研究 总被引:3,自引:0,他引:3
经过多年的理论与实践研究,螺旋流排沙已被广大的水利工作者所认可.本文首次利用毕托球测速系统测试了由新疆农业大学最新推出的带导流墩排沙漏斗的三维螺旋流流场,对其时均流特性进行了分析和研究.其次,文中还分析了其对输沙过程所产生的影响,为进一步优化此类型排沙漏斗流态打下了基础 相似文献
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为进一步探讨边界效应对加筋土地基的影响,基于室内方形基础下加筋土地基大模型试验,采用ABAQUS有限元软件建立加筋土地基数值模型,主要分析了模型宽度L和加载板宽度B对加筋土地基承载性能、地基内部土体应力应变及筋材变形的影响。结果表明:无筋地基与加筋土地基极限承载力均随L/B的减小而增大,当L/B>5时,可忽略边界效应对加筋土地基的影响;当L/B<2.67时,边界效应对加筋土地基的影响最大;当L/B>4时,边界效应对无筋地基的影响可忽略不计;加筋能够显著改善地基土体的不均匀沉降和减小基础两侧土体隆起高度;竖向应力分布区域随着B的增大而增大,加筋土地基受竖向荷载的影响宽度为5B,影响深度为2.57B~4B;当L/B>5时,不同L/B工况下土体变形、应力分布及格栅变形曲线基本重合,此时加筋土地基受边界效应的影响可忽略不计。 相似文献
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“研学课堂”是教师在对学科核心素养、学业质量标准和学习初始水平进行充分研究的前提下,通过“研”中“学”、“学”中“研”,实现学习方式的优化,促进数学课堂的提质增效,以使学生理解数学本质,锻炼数学思维. 相似文献
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Irradiation hardening behaviors of tungsten-potassium alloy studied by accelerated 3-MeV W^2+ ions 下载免费PDF全文
Tungsten-potassium(WK)alloy with ultrafine/fine grains and nano-K bubbles is fabricated through spark plasma sintering(SPS)and rolling process.In this study,3-MeV W^2+ ion irradiation with a tandem accelerator is adopted to simulate the displacement damage caused by neutrons.As the depth of irradiation damage layer is limited to only 500 nm,the hardening behaviors of WK alloy and ITER(International Thermonuclear Experimental Reactor)-W under several damage levels are investigated through Bercovich tip nanoindentation test and other morphological characterizations.The indenter size effect(ISE),soft substrate effect(SSE),and damage gradient effect(DGE)are found to influence the measurement of nano-hardness.Few or no pop-ins in irradiated samples are observed while visible pop-in events take place in unirradiated metals.Extensive pile-up with different morphology features around the indentation exists in both WK and ITER-W.The WK shows a smaller hardness increment than ITER-W under the same condition of displacement damage.This study provides beneficial information for WK alloy serving as a promising plasma facing materials(PFMs)candidate. 相似文献
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采用复合电沉积和电泳沉积两步法在钛基体上制备了Co-YSZ/HAp纳米复合涂层, 与只采用电泳沉积法在钛基体上制备纳米HAp单一涂层进行了比较研究.采用场发射扫描电镜、X 射线衍射和能量散射谱对复合涂层的微观形貌, 纳米HAp外层表面形貌, 晶相, 复合涂层的断面形貌及元素组成分布进行分析研究. 通过粘结-拉伸实验测定了涂层与基体的结合强度, 结果表明, Co-YSZ/HAp 纳米复合涂层与钛基体的结合强度明显高于纳米HAp 单一涂层与钛基体的结合强度, 说明复合涂层具有更好的力学性能. 相似文献
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Theoretical and experimental analyses of recording mark microstructures in signal waveform modulation optical disc 下载免费PDF全文
In this paper,we propose a dynamic mastering process model for signal waveform modulation (SWM) optical disc.To form the ideal microstructures and solve the problems in the SWM master manufacturing process,we use this model to simulate the three-dimensional mark profiles in the SWM read-only disc.The simulated micro-patterns of recording pits and lands are employed to optimize the writing strategy and provide a quantitative basis for manufacturing the sub-pits and sub-lands.The simulation mark profiles are compared with the experimental ones,which are produced with the optimized writing strategy parameters.Comparison results demonstrate that the simulated profiles are highly consistent with the actual ones. 相似文献
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To improve the tracking servo performance, a novel signal waveform multi-level (SWML) read-only disc realized on the digital versatile disc (DVD) platform is presented. The characteristic of the differential phase detection (DPD) signal of the SWML read-only disc is analyzed both in theory and experiment. The amplitude of the DPD signal of the SWML read-only disc in an open tracking servo loop is about 2/3 of that of the DVD read-only disc. The uniformity and symmetry of the DPD signal of the SWML read-only disc are similar to those of the DVD read-only disc and better than the former multi-level run-length limited (ML-RLL) read-onlv disc. 相似文献