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采用改进的Brust方法,用硼氢化钠还原氯金酸,并以巯基丁二酸(MSA)、氮乙酰基半光胺酸(NAC)作为包裹剂,成功制备了单分散的水溶性金纳米团簇。高分辨透射电镜(HRTEM)结果表明,增大硫醇与氯金酸的比例并增加氯金酸的初始浓度,有利于得到尺寸更小的金纳米粒子。当氯金酸的浓度(CAu)为9.3 mmol·L-1,CAu:CS为1:30时,得到了直径约为1 nm、标准偏差为0.2 nm的Au@MSA纳米团簇。结合紫外(UV)、热重(TG)和X射线光电子能谱(XPS)分析结果,可以推测出单分散金纳米簇的化学式为[Au38(MSANa)26]或[Au39(MSANa)27]。 相似文献
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We propose a concept of wavelength synchronization to ensure the stability of ultra-dense channels in an ultra-dense wavelength division multiplexing passive optical network(UDWDM-PON)transmitter.A mode-locked laser is used to provide wavelength references for users.By injection locking the semiconductor laser,the separation of the wavelength reference is realized in an optical line terminal.The downlink and uplink wavelength references are interlaced and distributed to facilitate the synchronization of uplink carriers.In the optical network unit,the uplink optical carriers are filtered by injection locking semiconductor lasers,which achieve wavelength synchronization for the uplink users.In this Letter,an adaptive wavelength synchronization transmitter for UDWDM-PON is realized with a channel spacing of 5 GHz. 相似文献
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