小花棘豆中黄酮甙的2D-NMR研究

利用2D-NMR并结合其它理化方法研究了从豆科植物小花棘豆中分得的一种黄酮甙:山奈酚-3-O-芸香糖甙的化学结构;该成分系首次从棘豆属植物中分得。     

含杂质无格点基底表面分枝状凝聚体的计算机模拟

根据含杂质熔融玻璃表面金原子凝聚的实验规律，在原子团簇具有随机的线扩散步长和刚性 转动角度的特征条件下，建立了含杂质无格点基底表面的各向异性团簇-团簇凝聚模型，对 团簇的无规扩散、刚性转动以及凝聚全过程进行了计算机模拟，系统地研究了基底表面无规 分布的杂质区域对分枝状凝聚体诸多特性的影响，所得结果与实验事实相符合. 关键词： 薄膜生长 Monte Carlo模拟 分形     

玻色─爱因斯坦关联半径和源半径对实验窗口的依赖及它们的差异

研究了160A GeVPb+Pb反应中π源的玻色─爱因斯坦关联半径和源半径(均方根半径)的关系,以及它们对实验窗口的依赖. 模型冗源由URASiMA生成器产生. 研究表明关联半径和源半径不仅数值不等,而且变化行为也不同.     

THE TRANSFORMATION FUNCTION Φ AND THE CONDITION NEEDED FOR KUR SPACE HAVING THE FIXED POINT

In the last several years some progress has been made in the study of the properties ofthe extent of Banach space:In 1979 for example.when Suillivan discussed a relatedcharacterization of real L~P(X)space.he used uniform behavior of all two-dimensionalsubspace and defined this concept of a KUR space.In 1980 Huff used the concept of a NUCspace when he discussed the property of generalizing uniform convexity which was definedin terms of sequence.And in 1980 Yu Xin-tai stated,certainly and proved that the KURspace is equal to the NUC space.However,the following quite interesting questions raised respectively by Suillivan andHuff merit attention:Does every super-reflexive space have the fixed point property?The purpose of this paper is to study the characterization of transformationfunction and relationships between transformation function and the two questions above.     

高等职业教育高在何处

通过论述高等职业教育的办学特色，从高、中职学历教育两方面阐述高等教育的标尺和高等职业技能的科技文化含量，为高等职业教育提供参考。     

一种电化学调制光谱用电解池

电化学调制光谱,又称电反射谱,是近年来发展起来的现场光学测量新技术。其实验方法是:研究电极受到小幅度交流信号的激励,其反射率发生相应的交变响应,采用锁相技术,测     

Preparation and Photocatalytic Properties of Ti1-xZrxO2 Solid Solution

A series of Ti1-xZrxO2 materials were synthesized through a multistep sol-gel process. The structural characteristics were investigated using X-ray diffraction （XRD）, X-ray photoelectron spectroscopy （XPS） and Raman measurements. The experimental results showed that a solid solution could be obtained at low Zr/（Ti＋Zr） molar ratios （x ≤0.319）. Raman measurements exhibited that the presence of zirconium in the solid solutions greatly retarded the amorphous-anatase and anatase-rutile transitions. The diffuse reflectance UV-Vis spectra revealed that the bandgap of the solid solution was enlarged gradually with the increment of incorporated zirconium content. The Ti1-xZrxO2 solid solutions exhibited higher photocatalytic activity than pure TiO2 for the degradation of 4-chlorophenol aqueous solution.     

无载体离子有机共沉淀分离-石墨炉原子吸收光谱法测定海水中铜铅铬镍

以吡咯烷二硫代氨基甲酸铵(APDC)氧化物作为共沉淀剂,建立了无载体离子有机共沉淀分离、石墨炉原子吸收光谱法测定海水中铜、铅、铬、镍的方法。考察了海水样品pH、共沉淀剂APDC和氧化剂H_2O_2的用量、陈化时间等因素对共沉淀分离效果的影响,优化了实验条件。结果证明,在p H4~5的海水样品中,加入4 m L 30 g/L APDC,1 m L H_2O_2,静置60 min,待测元素能与海水基体很好的分离。铜和铬含量在0~20μg/L范围内呈良好的线性关系,线性相关系数R0.999;镍含量在0~30μg/L,铅含量在0~40μg/L范围内呈良好的线性关系,线性相关系数R0.998;检出限分别为0.31,0.30,0.20,0.25μg/L,方法精密度好,加标回收率为88.8%~101.4%。方法可用于海水样品中铅、铜、镍、铬的常规检测。     

甲基橙—溴化十六烷基三甲胺三元络合物分光光度法测定微量铜（Ⅱ）

本介绍了甲基橙与铜在ＰＨ３．８时与溴化十六烷基三甲胺形成三元胶束络合物增溶于聚乙烯醇体系中，其表观摩尔吸系数ε５８０为２．９５×１０＾６Ｌ．ｍｏｎ＾－１．ｃｍ＾－１，铜（Ⅱ）浓度在０．１－０．６μｇ／２５ｍＬ范围内与吸光度成线性关系。用此法分析人中铜含量，结果满意。