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β-环糊精功能化聚丙烯腈纳米纤维的制备及对亚甲基蓝的吸附性能 总被引:1,自引:0,他引:1
以N,N-二甲基甲酰胺(DMF)为溶剂,利用静电纺丝法制备了聚丙烯腈(PAN)/β-环糊精(β-CD)纳米纤维.通过场发射扫描电镜、红外光谱和粉末XRD对纳米纤维进行了表征,并检测了纺丝溶液的电导率和黏度.结果表明,β-CD的添加量可以改善纳米纤维的形貌,固定在纤维上的β-CD保留了空腔结构,为其在纳米纤维中发挥超分子... 相似文献
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利用同步辐射光电子能谱(SRPES)和X射线光电子能谱(XPS)技术,系统研究了室温下Fe/ZnO界面形成过程中Fe薄膜与氧结尾的ZnO(000 1 )衬底之间的相互作用,结果显示初始沉积的Fe明显被表面氧氧化为Fe2+离子,在Fe覆盖度为0—3 nm的范围内,分别观察到与界面电荷传输、化学反应以及薄膜磁性相关的三个有意义的临界厚度,这一结果将有助于基于Fe/ZnO界面的相关器件的设计和研发. 相似文献
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椭球形整流罩产生较大的空气阻力,限制了精确制导武器的作战性能。以减小空气阻力为主要目标,针对二次曲面共形光学整流罩进行研究,设计综合性能较为完善的整流罩面型。应用计算流体力学方法,计算了共形整流罩的空气阻力系数,建立了共形整流罩空气阻力评价函数。基于光线追迹理论,以不同目标视场下的平均波前误差作为像质评价指标,构建了共形整流罩像质评价函数。以雷达散射理论为基础,计算了整流罩的雷达散射截面积,给出了共形整流罩雷达散射特性评价函数。结合空气阻力、光学成像质量和雷达散射特性,建立了二次曲面共形整流罩综合性能评价函数,确立了长径比为1.5的抛物线型整流罩具有较好的综合性能。相比椭球形整流罩,该抛物线形整流罩减少了约1/3的空气阻力。 相似文献
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Detection of Fe 3d electronic states in valence band and magnetic properties of Fe-doped ZnO film 下载免费PDF全文
Fe-doped ZnO film has been grown by laser molecular beam epitaxy (L-MBE) and structurally characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM), all of which reveal the high quality of the film. No secondary phase was detected. Resonant photoemission spectroscopy (RPES) with photon energies around the Fe 2p-3d absorption edge is performed to detect the electronic structure in the valence band. A strong resonant effect at a photon energy of 710 eV is observed. Fe3+ is the only valence state of Fe ions in the film and the Fe 3d electronic states are concentrated at binding energies of about 3.8 eV and 7 eV~ 8 eV. There are no electronic states related to Fe near the Fermi level. Magnetic measurements reveal a typical superparamagnetic property at room temperature. The absence of electronic states related to Fe near the Fermi level and the high quality of the film, with few defects, provide little support to ferromagnetism. 相似文献