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21.
Yalu Ma Xiaofei Ma Yun Tian Xue Qin Hongling Gao Huaji Liu Fanli Lu Xiaodong Wang Xingyao Wang Danfeng Li Jianhui Wang 《大学化学》2020,35(8):48-53
将课程思政应用到"无机化学和化学分析"教学中,更好发挥其价值引领作用。开展课程思政建设,应做到守正与创新。本文以价值引领为切入点,介绍如何将思想政治教育有机融入课程内容设置和课堂讲授等环节,力求培养学生的家国情怀、国际视野、法治意识、生态意识、工程伦理、人文关怀等科学素养,深入践行立德树人,提高本科教学质量。 相似文献
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Quality by design: A systematic and rapid liquid chromatography and mass spectrometry method for eprosartan mesylate and its related impurities using a superficially porous particle column 下载免费PDF全文
Pradipbhai D. Kalariya Murali V. N. Kumar Talluri Vinay D. Gaitonde Prashant S. Devrukhakar Ragampeta Srinivas 《Journal of separation science》2014,37(16):2160-2171
The present work describes the systematic development of a robust, precise, and rapid reversed‐phase liquid chromatography method for the simultaneous determination of eprosartan mesylate and its six impurities using quality‐by‐design principles. The method was developed in two phases, screening and optimization. During the screening phase, the most suitable stationary phase, organic modifier, and pH were identified. The optimization was performed for secondary influential parameters—column temperature, gradient time, and flow rate using eight experiments—to examine multifactorial effects of parameters on the critical resolution and generated design space representing the robust region. A verification experiment was performed within the working design space and the model was found to be accurate. This study also describes other operating features of the column packed with superficially porous particles that allow very fast separations at pressures available in most liquid chromatography instruments. Successful chromatographic separation was achieved in less than 7 min using a fused‐core C18 (100 mm × 2.1 mm, 2.6 μm) column with linear gradient elution of 10 mM ammonium formate (pH 3.0) and acetonitrile as the mobile phase. The method was validated for specificity, linearity, accuracy, precision, and robustness in compliance with the International Conference on Harmonization Q2 (R1) guidelines. The impurities were identified by liquid chromatography with mass spectrometry. 相似文献
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Static headspace‐multicapillary column with gas chromatography coupled to ion mobility spectrometry as a simple approach for the discrimination of crude and processed traditional Chinese medicines 下载免费PDF全文
Gang Cao Qiyang Shou Qinglin Li Jianping Jiang Xiaocheng Chen 《Journal of separation science》2014,37(21):3090-3093
The processing procedure can alter the nature and chemical transformation of traditional Chinese medicine to accommodate different clinical dispensing and preparation requirements. In this study, static headspace‐multicapillary column with gas chromatography coupled to ion mobility spectrometry was developed for the rapid and sensitive discrimination of crude and processed traditional Chinese medicine. Using Radix Paeoniae Alba as a traditional Chinese medicine model, the combined power of this approach was illustrated by classifying the crude and processed Radix Paeoniae Alba samples into two main categories. The contents of the main components in Radix Paeoniae Alba varied significantly. The established method could promote the use of ion mobility spectrometry in intrinsic quality control and differentiation of herbal medicines from other processed products or preparations. 相似文献
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Lívia Riberti Rodrigues Diogo Noin de Oliveira Mônica Siqueira Ferreira Rodrigo Ramos Catharino 《Analytica chimica acta》2014
The analysis of impurities and degradation products in pharmaceutical preparations are usually performed by chromatographic techniques such as high-performance liquid chromatography (HPLC). This approach demands extensive analysis time, mostly due to extraction and separation phases. These steps must be carried out in samples in order to adapt them to the requirements of the analytical method of choice. In the present contribution, matrix-assisted laser desorption/ionization mass spectrometry imaging (MALDI-MSI) was employed to quantify an important degradation product in atorvastatin calcium 80 mg tablets: the atorvastatin lactone. Through the standard of the impurity, it was possible to perform quantitative analysis directly on the drug tablet, using a quick and novel approach, suitable for quality control processes in the pharmaceutical industry. 相似文献
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In this paper, the various Optical Burst Switching (OBS) reservation schemes have been examined in order to reduce data loss caused by either channel scheduling or resources. A novel multi-service OBS edge node with synchronized bandwidth reservation mechanism (SRM) has been proposed, which enables high-speed network transport nodes to dynamically reserve bandwidth needed for active data burst flows. The performance of the proposed mechanism is evaluated by means of NS-2 simulation. The results show that the packet delay is kept within the constraint for each traffic flow and the performance metrics such as burst loss rate, throughput and fairness are remarkably improved. 相似文献
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探讨了分光光度法测定吸收液中二氧化氮,采用盲样与已知标准样品进行比对,结果表明,该法符合质量控制要求,并对可能影响质控结果的因素进行了讨论。 相似文献
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化探样品中金含量测定的探讨 总被引:1,自引:0,他引:1
讨论了化探样品中金测定过程中的分解方法、金的富集、酸度及流速、泡塑清洗及控制等条件,严格控制各个分析环节,通过对标准样品进行分析,相对标准偏差为0.75%—3.64%,回收率为95.0%—105.0%,方法适合批量样品生产,能达到化探样品中金含量的分析要求。 相似文献