PQ/PMMA光致聚合物的偏光全息特性研究

对于体全息来说,存储材料的体积与所能存储的信息容量有关。采用热致聚合方法制备了厚度分别为0.5mm、1.0mm、1.5mm、2.0mm的菲醌掺杂的聚甲基丙烯酸甲酯(PQ/PMMA)光致聚合物材料。探测并分析了材料样品对不同波长的光吸收特性以及不同厚度材料的全息性能。实验结果表明,厚度的变化对材料的光致双折射值影响较小,而对衍射效率的影响较大。     

对于金属丝在准直激光照射下形成环形光的研究

准直激光照射下的金属丝,会在垂直于金属丝方向的光屏上出现环形光。本文采用在金属丝表面包裹碳颗粒的方法,分离反射光和衍射光,研究光路的组成。接着探究金属丝的半径和粗糙程度对环形光的影响。并在此基础上,测量环形光光强分布规律,结合几何光学和夫琅禾费衍射进行解释。光源也是潜在的影响因素,本文探究了不同波长激光对环形光的影响。     

衍射光栅实验中平行光正入射条件的讨论

针对光栅衍射实验中如何保证平行光正入射光栅表面这一难点,总结出一种在实验教学简单可行、易于学生理解的操作方法。这种实验方法,既包含了分光计调节的基本要求,又能让学生比较容易掌握和理解光栅的衍射理论,提高了实验效率。     

Hydrothermal Synthesis and Crystal Structure of One 3D Coordination Polymer of Nickle （II） Achieved from 5-Iodo-isophthalic Acid Ligand

A new coordination polymer [Ni（L）（m-bix）（H2O）]n （1, H2L = 5-iodo-isophthalic acid, m-bix=1,3-bis（imidazol-1-ylmethyl）-benzene） has been synthesized by the hydrothermal method and characterized by IR, elemental analysis, powder XRD and single-crystal X-ray analysis. The crystal is of triclinic, space group Pī with a = 9.1638（3）, b = 10.2319（3）, c = 13.2463（4） ？, α = 80.1710（10）, β = 83.671（2）, γ = 70.3790（10）o,C22H19NiIN4O5, Mr = 605.02, V = 1150.85（6） ？3, Dc = 1.746 g/cm3, F（000） = 600, μ = 2.225 mm-1, S = 1.045 and Z = 2. The final R = 0.0388 and wR = 0.1257 for 5089 observed reflections with I 〉 2σ（I）. In the title complex, the M and P layers are arranged alternately to give a double-layer structure by the symmetry related hydrogen bonds, and these double-layers are further joined together to achieve a 2D supramolecular architecture through I···π interaction involving iodine atoms and imidazole rings. The thermal stability of the title complex was studied by thermal gravimetric （TG） and differential thermal analysis （DTA）.     

前缀码与极大前缀码的一种新刻画

在语言图Γ(X*)概念的基础上,用新引入的语言竹竿l(X*)和语言竹竿集L(X*)的概念形象地刻画了前缀码与极大前缀码:A是前缀码l(X*)∈L(X*),S_l_((X*))∩A或为单点集或为Φ;A是极大前缀码l(X*)∈L(X*),i)S_(l(X*))∩A或为单点集或为Φ.ii)S_(l(X*))∩A=Φ■u∈S_(l(X*)),■a∈A,ω∈X~+使a=uw.     

线缆系统电磁脉冲效应测量系统研制和试验

分析了实验室瞬态X射线产生的系统电磁脉冲(SGEMP)效应测试所面临的技术问题,提出了解决方法、措施以及实验室模拟瞬态X射线的SGEMP模拟试验方法。通过电子屏蔽、电磁屏蔽、光电隔离、信号对称提取等特殊技术处理,解决了SGEMP效应模拟试验方法和测量系统抗X射线、抗电磁辐射等技术问题,并在大型瞬态X射线模拟源上,测出了瞬态X射线辐照时金属腔内线缆的SGEMP效应波形及幅值。     

一维势阱与扩展X射线吸收精细结构

介绍了一维势阱的一个应用实例.     

一个数学问题的探究

文[1]最后提出了一个待解决的数学问题:过∠MON(∠MON=θ,θ为定值,且θ∈(0,π))内一定点P做直线l分别交射线OM、ON于A、B两点(A、B异于顶点O),求|OA|+|OB|-|AB|的取值范围.     

能量色散型X射线荧光光谱法测定聚合物材料中镉和铅含量

提出了能量色散型X射线荧光光谱测定聚合物材料中镉和铅的测试分析方法及制样技巧。按照仪器分析条件测定同时含有镉和铅的6块不同浓度级别的标准物质来建立校准工作曲线,其线性范围分别在250ug·g-1、1100ug·g-1以内。镉和铅的方法检出限依次为4.7ug·g-1、4.1ug·g-1。该方法应用于测定欧洲标准物质ERM-EC680和ERM-EC681k,其镉和铅的实际测定值与标准物质证书的标称值相符,测定实际样品中的镉和铅的回收率介于90~110%。该方法测定标准物质和实际样品中镉和铅的精密度均小于10%。     

Energy spectrum of multi-radiation of X-rays in a low energy Mather-type plasma focus device

The multi-radiation of X-rays was investigated with special attention to their energy spectrum in a Mather-type plasma focus device （operated with argon gas）. The analysis is based on the effect of anomalous resistances. To study the energy spectrum, a four-channel diode X-ray spectrometer was used along with a special set of filters. The filters were suitable for detection of medium range X-rays as well as hard X-rays with energy exceeding 30 keV. The results indicate that the anomalous resistivity effect during the post pinch phase may cause multi-radiation of X-rays with a total duration of 300 ± 50 ns. The significant contribution of Cu-Kα was due to the medium range X-rays, nonetheless, hard X-rays with energies greater than 15 keV also participate in the process. The total emitted X-ray energy in the forms of Cu-K and Cu-K/3 was around 0.14 ± 0.02 （J/Sr） and 0.04 ±0.01 （J/Sr）, respectively. The total energy of the emitted hard X-ray （〉 15 keV） was around 0.12± 0.02 （J/Sr）.