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The field emission (FE) characteristics of nano-structrued carbon films (NSCFs) are investigated. The saturation behaviour of the field emission current density found at high electric field E cannot be reasonably explained by the traditional Fowler-Nordheim (F-N) theory. A three-region E model and the curve-fitting method are utilized for discussing the FE characteristics of NSCFs. In the low, high, and middle E regions, the FE mechanism is reasonably explained by a modified F-N model, a corrected space-charge-limited-current (SCLC) model and the joint model of F-N and SCLC mechanism, respectively. Moreover, the measured FE data accord well with the results from our corrected theoretical model. 相似文献
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Chemical Synthesis and Characterization of Flaky h-BCN at High Pressure and High Temperature 下载免费PDF全文
Hexagonal boron carbonitrogen (h-BCN) compound is synthesized from a mixture of boron powder and CNH compound prepared by pyrolysis of melamine (CaH6N6) under high temperature (1400-1500℃) and high pressure (5.0-5.5 GPa). X-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy and Raman spec- troscopy are used to determine the chemical composition and bonds of the product. The results show that the product has composition of B0.18C0.64N0.16 (near BC4N) and atomic-level hybrid. X-ray diffraction analysis indicates that the powder has a hexagonal network structure. Scanning and transmission electron microscopy results suggest that h-BCN compound morphology is mainly flaky in width about 1 μm and thickness 200nm. 相似文献