Moessbauer Investigation of the Ferromagnetic Coupling in Copper-Iron Polycyanides

One of the Prussian blue analogs, molecular magnet Cu3^Ⅲ [Fe^Ⅲ (CN)6]2.11.6H2 O, was investigated by Moessbauer spectroscopy. It was found that transition temperature was around Tc = 18.5 K from paramagnetic phase to ferromagnetic phase. The β value of the critical exponent is around 0.338 at magnetic ordering temperature.Therefore, the ferromagnetic coupling interaction of Cu-Fe cyanide could be clearly explained by spin wave theory.     

双阱结构含时量子输运的微扰论及输运方程

利用Lewis-Riesenfeld不变量理论和与不变量有关的幺正变换方法研究了双阱结构含时量子 输运的微扰论.获得了双阱内含时薛定谔方程的精确解的完备集，在此基础上，把双阱与左 右热库的相互作用作为微挠，获得了双阱结构一阶近似下的输运方程，并在绝热近似下提供 了一种用于研究量子输运过程中几何相因子(Berry相因子)的方法. 关键词： 含时量子输运 输运方程 不变量 几何相因子     

Aligned ZnO Nanofibre Array Prepared by Vapour Transport in Air

An aligned zinc oxide nanofibre array has been fabricated by heating the mixture of ZnO, Ga2Oa, and graphite powders in atmosphere. The ZnO nanofibre showed a uniform size of about 150nm in diameter and 50μm in length. The nanofibres grew predominantly along one direction. Both x-ray diffraction (XRD) and Raman shift spectra show that the product is composed of ZnO with the typical hexagonal structure. The good crystallinity of these ZnO nanofibres has been verified by photoluminescence spectra with strong UV emission at 287nm and weak green band emission observed at room temperature. The component of the product was analysed by XRD,Raman shift spectrum, x-ray energy dispersion (EDX) and x-ray photoelectronic energy spectroscopy (XPS). The growth process and the characteristics can be interpreted by vapour-liquid-solid mechanism.     

Hα Emission Imaging during Supersonic Molecular Beam Injection by CCD Photograph

There are several fuelling methods for tokamak plasma： pellet injection （PI）, gas puffing （GP）, neutral beam injection （NBI） and supersonic molecular beam injection （SMBI） .SMBI has been created in the Southwestern Institute of Physics, China.     

用超声化学法制备有机包覆纳米银

纳米级银粉，以其纳米尺寸所赋予的独特性能，可广泛应用于催化剂材料、电池电极材料、低温材料和导电浆料，探索纳米银粉的制备方法具有重要的意义。2004年，通过超声化学法，在乙二醇介质中、以硝酸银为原料制备出了有机包覆的纳米银。产物用X射线光电子能谱仪（XPS）、透射电子显微镜（TEM）和红外光谱等进行了检测。     

The First Results of Supersonic Molecular Beam Injection in the HL-2A Tokamak

HL-2A tokamak, the first tokamak with divertor in China, has been constructed and put into operation in 2002. The main parameters are R=1.65 m, a=0.4 m, BT=2.8 T, Ip = 0. 48 MA. The divertor of HL-2A is unique, because it is characterized with a large closed divertor chamber. The device has double divertor chamber, but now it is operating with lower single null configuration to study the physics of divertor for the next step design of a divertor. Supersonic molecular beam injection （SMBI） system with LN2 cooling trap was first installed and demonstrated on the HL-2A tokamak in 2004. The first results of SMBI into HL-2A plasma are to demonstrate the function of the HL-2A divertor and to observe the cold pulse propagation during multi-pulse SMBI on HL-2A Tokamak.     

激光水下偏振特性用于目标图像探测

利用激光水下偏振特性获得偏振差分图像(PDI),并运用PDI技术,从理论和实验上对水下目标探测进行了研究.介绍了PDI基本概念和实验系统原理,然后比较分析了不同条件下普通图像与PDI在辨别目标距离及其纹理上的差别和PDI中背景偏振光的影响,得出利用目标和背景偏振光的差异区分二者,从而提高探测距离的结论,并取得了较好的效果.在此基础上提出了通过处理有关PDI偏振参量来进一步辨别目标与背景的设想.     

Polystyrene—supported Benzyl Selenide：An Effcient Reagent for Highly Stereocontrolled Synthesis of Substituted Olefins

Polystryene-supported benzly selenide has been prepared.This novel reagent was treated with LDA to produce a selenium stabilized carbanion,which reacted with alkyl halide,followed by selenoxide syn-elimination,to give substituted olefins stereospecificly.     

SJTU-1型新型医用超声设备声输出测量系统通过鉴定

2003年2月27日由国家药品监督管理局医疗器械司委托全国医用电器标准化技术委员会组织,在上海市举行了SJTU-1型医用超声设备声输出测量系统的技术成果鉴定会。由王威琪院士、冯若教授、张德俊教授为主任委员的鉴定委员会,对此项成果进行了测试和技术鉴定,认为SJTU-1型医用超声设备声输出测量系统的技术指标达到了同类系统的国际先进水平,某些功能优于国外同类系统。     

Ni（Ⅱ）—MOBTAMB—TritonX—100体系析相光度法测定痕量镍

研究了Triton X-100在浊点条件下,对Ni(Ⅱ)-2-[2′-(6′-甲氧基-苯并噻唑)偶氮]-5-二甲氨基苯甲酸(MOBTAMB)配合物的析相条件。在pH 8.6～9.5的氨-氧化铵缓冲体系中,90℃水浴加热1.5h,析相完全。配合物最大吸收峰位于658nm处,表观摩尔吸光系数为5.5×10~5。镍含量在0～3μg/30ml范围内符合比耳定律。所拟方法用于天然水中的痕量镍测定,结果满意。