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91.
采用高温固相法成功合成了一种可用于白光LED的Ca2Li2BiV3O12∶Eu3+新型红色荧光粉,使用X射线衍射仪和荧光分光光度计对合成样品进行了表征,研究了合成温度和Eu3+含量对合成样品相组成和发光性能的影响。结果表明,采用高温固相法在650~700 ℃能合成纯度较高、结晶度好的Ca2Li2BiV3O12∶Eu3+荧光粉,合成样品激发带覆盖200~400 nm,发射光谱的线状发射峰可归属于Eu3+的5D0→7FJ(J= 1, 2, 3,4)特征锐线发射,Eu3+摩尔分数为14%时荧光粉的发光强度最大。 相似文献
92.
S. Sutradhar S. PatiS. Acharya S. DasD. Das P.K. Chakrabarti 《Journal of magnetism and magnetic materials》2012,324(7):1317-1325
Nanoparticles of Zn substituted lithium ferrite (Li0.32Zn0.36Fe2.32O4) have been prepared by a sol-gel method where the ultra-sonication technique has been adopted to reduce the agglomeration effect among the nanoparticles. The samples were heat-treated at three different temperatures and the formation of the nanocrystalline phase was confirmed by X-ray diffractograms (XRD). The average particle size of each sample has been estimated from the (311) peak of the XRD pattern using the Debye-Scherrer formula and the average sizes are in the range of 10-21 nm. The average particle size, crystallographic phase, etc. of some selected samples obtained from the high-resolution transmission electron microscopy are in agreement with those estimated from the XRD patterns. Static magnetic measurements viz., hysteresis loops, field cooled and zero field cooled magnetization versus temperature curves of some samples carried out by SQUID in the temperature range of 300 to 5 K clearly indicate the presence of superparamagnetic (SPM) relaxation of the nanoparticles in the samples. The maximum magnetization of the SPM sample annealed at 500 °C is quite high (68 Am2/Kg) and the hysteresis loops are almost square shaped with very low value of coercive field at room temperature (827.8 A/m). The particle size, magneto-crystalline anisotropy, etc. have been estimated from the detailed theoretical analysis of the static magnetic data. The dynamic magnetic behavior of the samples was also investigated by observing the ac hysteresis loops and magnetization versus field curves with different time windows at room temperatures. The different soft magnetic quantities viz., coercive field, magnetization, remanance, hysteresis losses, etc. were extracted from dynamic measurements. Dynamic measurements confirmed that the samples are in their mixed state of SPM and ordered ferrimagnetic particles, which is in good agreement with the results of static magnetic measurements. Mössbauer spectra of the samples recorded at room temperature (300 K) and at different temperatures down to 20 K confirmed the presence of the SPM relaxation of the nanoparticles of the samples. 相似文献
93.
Yu-Jie WuXiao-Kun Chen Jing ZhangXiao-Jia Chen 《Journal of magnetism and magnetic materials》2012,324(7):1348-1352
Bi1−xYxFeO3 (x=0-0.2) powders were prepared to study the effect of Y substitution on their structural and magnetic properties. A structural symmetric breaking from the rhombohedral R3c to orthorhombic Pnma at around x=0.10 was identified across a ferroelectric-paraelectric phase. A parabolic dependence of the magnetization upon substitution was obtained with a maximum at the phase transition boundary and a switching behavior for x=0.20. The composition-driven magnetic structure evolution was proposed to account for the magnetic properties in Bi1−xYxFeO3. 相似文献
94.
To study the spectrum reconstruction of the 20 MV X-ray generated by the Dragon-I linear induction accelerator, the Monte Carlo method is applied to simulate the attenuations of the X-ray in the attenuators of different thicknesses and thus provide the transmission data. As is known, the spectrum estimation from transmission data is an ill-conditioned problem. The method based on iterative perturbations is employed to derive the X-ray spectra, where initial guesses are used to start the process. This algorithm takes into account not only the minimization of the differences between the measured and the calculated transmissions but also the smoothness feature of the spectrum function. In this work, various filter materials are put to use as the attenuator, and the condition for an accurate and robust solution of the X-ray spectrum calculation is demonstrated. The influences of the scattering photons within different intervals of emergence angle on the X-ray spectrum reconstruction are also analyzed. 相似文献
95.
提出了一种新型十字环型左手材料结构单元.该结构只需在介质板单侧蚀刻, 即可在二维方向上产生等效负介电常数和等效负磁导率.通过理论分析, 提出场-路结合的等效源分析法以计算等效介电常数、磁导率, 并据此对十字环型结构单元的左手特性激发机理进行了论证. 后采用Nicolson-Ross-Weir 等效参数法提取了十字环型单元阵列的相对介电常数和相对磁导率, 并通过棱镜实验对材料的负折射特性进行了验证.实验表明, 该左手材料在6.8-6.9 GHz频段具有二维入射左手特性. 此种左手材料制作工艺相对简单, 为左手材料在微波器件领域的应用提供了一种较为实用的设计方案. 相似文献
96.
中子符合计数在核材料认证和管理中有着广泛的应用.系统阐述了中子符合计数的基本原理,对“点模型”公式作了推导.利用MCNP4B程序实现了中子符合计数的数值模拟.Neutron coincidence counting is widely used in the authentication and management of nuclear material. The basic principles of coincidence counting and the derivation of "point model" formulae of "point model" are introduced in this paper. The numerical simulation of the coincidence counting is implemented by use of the MCNP4B package. 相似文献
97.
98.
本文对平面应变情况下不可压缩橡胶类材料裂纹尖端弹性场进行了有限变形分析.裂纹尖端场被分为收缩区和扩张区.借助于新的应变能函数和变形模式,推出了尖端场各区的渐近方程,得到了尖端场的完整描述.本文对奇异性作了讨论,得到了不可压缩橡胶类材料裂纹尖端应力及应变分布曲线,揭示了裂纹尖端应力应变场的特性. 相似文献
99.
M. N. M. Allam A. M. Zenkour & R. Tantawy 《advances in applied mathematics and mechanics.》2014,6(2):233-246
This paper presents an analytical solution for the interaction of electric potentials,
electric displacement, elastic deformations, and describes hygrothermal effect responses
in hollow and solid cylinders, subjected to mechanical load and electric potential. Exact
solutions for displacement, stresses and electric potentials in functionally graded
piezoelectric material are determined using the infinitesimal theory. The material properties
coefficients of the present cylinder are assumed to be graded in the radial direction by a
power law distribution. Numerical examples display the significant of influence of material
inhomogeneity. It is interesting to note that selecting a specific value of inhomogeneity
parameter can optimize the piezoelectric hollow and solid cylinders responses, which will
be of particular importance in modern engineering designs. 相似文献
100.