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91.
An analytical result is not considered to be complete without a statement of the measurement uncertainty associated with
it. Evaluation of measurement uncertainty is therefore an essential part of every determination. In the present study the
measurement uncertainty of the result of determination of selenium in the reference material Seronorm Trace Elements Serum
was studied. The combination of a digestion procedure using sulfuric acid, V2O5 in H2SO4 and hydrogen peroxide and the continuous flow approach of hydride generation atomic fluorescence spectrometry (HG-AFS) detection
was used for selenium determination. The total uncertainty budget was calculated with the help of the GUM Workbench program,
in which computations follow the rules of the ’ISO guide to the expression of uncertainty in measurement’. The major sources
of uncertainty were found to be due to the recovery of the procedure, measurement of peak heights and the purity of Na2SeO3. A selenium mass fraction of 77.1±4.8 ng/g (with a coverage factor of 2.1, 95% probability) was determined, which is comparable
with the recommended value of 80 ng/g.
Received: 13 September 2002 Accepted: 23 December 2002
Acknowledgements We would like to thank Tinkara Buˇcar, B.Sc. for useful discussions and the IAEA Vienna, for financial support of the project
11553/RO.
Presented at CERMM-3, Central European Reference Materials and Measurements Conference: The function of reference materials
in the measurement process, May 30–June 1, 2002, Rogaška Slatina, Slovenia
Correspondence to V. Stibilj 相似文献
92.
Michael Szydlo 《Journal of Number Theory》2004,104(1):75-99
Kodaira and Néron classified and described the geometry of the special fibers of the Néron model of an elliptic curve defined over a discrete valuation ring with a perfect residue field. Tate described an algorithm to determine the special fiber type by manipulating the Weierstrass equation. In the case of non-perfect residue fields, we discover new fiber types which are not on the Kodaira-Néron list. We describe these new types and extend Tate's algorithm to deal with all discrete valuation rings. Specifically, we show how to translate a Weierstrass equation into a form where the reduction type may be easily determined. Having determined the special fiber type, we construct the regular model of the curve with explicit blow-up calculations. We also provide tables that serve as a simple reference for the algorithm and which succinctly summarize the results. 相似文献
93.
We propose a minimum mean absolute error linear interpolator (MMAELI), based on theL
1 approach. A linear functional of the observed time series due to non-normal innovations is derived. The solution equation
for the coefficients of this linear functional is established in terms of the innovation series. It is found that information
implied in the innovation series is useful for the interpolation of missing values. The MMAELIs of the AR(1) model with innovations
following mixed normal andt distributions are studied in detail. The MMAELI also approximates the minimum mean squared error linear interpolator (MMSELI)
well in mean squared error but outperforms the MMSELI in mean absolute error. An application to a real series is presented.
Extensions to the general ARMA model and other time series models are discussed.
This research was supported by a CityU Research Grant and Natural Science Foundation of China. 相似文献
94.
A fourth‐order compact finite difference scheme on the nine‐point 2D stencil is formulated for solving the steady‐state Navier–Stokes/Boussinesq equations for two‐dimensional, incompressible fluid flow and heat transfer using the stream function–vorticity formulation. The main feature of the new fourth‐order compact scheme is that it allows point‐successive overrelaxation (SOR) or point‐successive underrelaxation iteration for all Rayleigh numbers Ra of physical interest and all Prandtl numbers Pr attempted. Numerical solutions are obtained for the model problem of natural convection in a square cavity with benchmark solutions and compared with some of the accurate results available in the literature. Copyright © 2003 John Wiley & Sons, Ltd. 相似文献
95.
The wreath product of finite association schemes is a natural generalization of the notion of the wreath product of finite permutation groups. We determine all irreducible representations (the Jacobson radical) of a wreath product of two finite association schemes over an algebraically closed field in terms of the irreducible representations (Jacobson radicals) of the two factors involved. 相似文献
96.
Dielectric elastomer actuators (DEAs) have received considerable attention recently due to large voltage-induced strains, which can be over 100%. Previously, a large deformation quasi-static model that describes the out-of-plane deformations of clamped diaphragms was derived. The numerical model results compare well with quasi-static experimental results for the same configuration. With relevance to dynamic applications, the time-varying response of initially planar dielectric elastomer membranes configured for out-of-plane deformations has not been reported until now. In this paper, an experimental investigation and analysis of the dynamic response of a dielectric elastomer membrane is reported. The experiments were conducted with prestretched DEAs fabricated from 0.5 mm thick polyacrylate films and carbon grease electrodes. The experiments covered the electromechanical spectrum by investigating membrane response due to (i) a time-varying voltage input and (ii) a time-varying pressure input, resulting in a combined electromechanical loading state in both cases. For the time-varying voltage experiments, the membrane had a prestretch of three and was passively inflated to various predetermined states, and then actuated. The pole strains incurred during the inflation were as high as 25.6%, corresponding to slightly less than a hemispherical state. On actuation, the membrane would inflate further, causing a maximum additional strain of 9.5%. For the time-varying pressure experiments, the prestretched membrane was inflated and deflated mechanically while a constant voltage was applied. The membrane was cycled between various predetermined inflation states, the largest of which was nearly hemispherical, which with an applied constant voltage of 3 kV corresponded to a maximum polar strain of 28%. The results from these experiments reveal that the response of the membrane is a departure from the classical dynamic response of continuum membrane structures. The dynamic response of the membrane is that of a damped system with specific deformation shapes reminiscent of the classical membrane mode shapes but without same-phase oscillation, that is to say all parts of the system do not pass through the equilibrium configuration at the same time. Of particular interest is the ability to excite these deformations through a varying electrical load at constant mechanical pressure. 相似文献
97.
The synthesis and optical properties of tetrahedral fluorescent compounds comprising of tetraphenylmethane as the core and oligothiophenes as the chromophoric arms, and their water-soluble poly(ethylene glycol)-linked polymers are reported. 相似文献
98.
99.
Johan van Benthem 《Logica Universalis》2007,1(1):125-138
We prove new Lindstr?m theorems for the basic modal propositional language, and for some related fragments of first-order
logic. We find difficulties with such results for modal languages without a finite-depth property, high-lighting the difference
between abstract model theory for fragments and for extensions of first-order logic. In addition we discuss new connections
with interpolation properties, and the modal invariance theorem.
Mathematics Subject Classification (2000): Primary 03B45; Secondary 03C95 相似文献
100.
本文从速率方程出发,讨论了类锂铝复合等离子体的激发态结构,衰减常数,反转率和小信号增益等表征介质增益特性的物理量以及它们随电子温度,电子密度和光子逃逸几率的变化。找到了进行类锂铝离子通过复合机制产生X光激光设计应创造的等离子体状态目标区域。还讨论了这些物理量随原子序数变化的定标律。 相似文献