α，ω-二羧基-甲基丙烯酸丁酯低聚物的合成及MS分析

利用传统自由基聚合法，在四氢呋喃溶液中自由基引发聚合甲基丙烯酸丁酯单体而得到ω-羧基-甲基丙烯酸丁酯低聚物(CTBMA)(分子量在1500左右)；利用CTBMA末端酯基的反应特性，在二氧六环／水／KOH混合溶液中皂化CTBMA，使之转化为α，ω-羧基甲基丙烯酸丁酯低聚物(di-CTBMA)；研究了溶剂的类别、反应时间等反应条件对皂化产物结构的影响；利用MALDI-TOF-MS及LSIMS对皂化各阶段产物进行了分析监测．实验表明，在适当的皂化条件下，CTBMA皂化时主要为末端酯基转化为羧基，相应得到的产物di-CTMBA具有很好的结构特性，其官能团度(functionality)接近2．     

Formation of Supersonic Zones and Local Separation Zones in Transonic Steady-State Flow Past Surface Roughness in the Free Interaction Regime

Within the framework of free interaction theory numerical methods are used to investigate the occurrence of supersonic zones with shocks in the outer inviscid region for flow past roughness in the lower viscous sublayer, with and without the formation of local separation zones.     

Quantitative vibration amplitude measurement with time-averaged digital speckle pattern interferometry

A new method of using time-averaged digital speckle pattern interferometry for the quantitative measurement of vibration amplitude was developed. Signal processing techniques especially the Hilbert transformation for quantitative evaluation of the Bessel fringes obtained in time-averaged digital speckle pattern interferometry were explored. The quadrature signal after Hilbert transformation is equivalent to a 90° phase-shifted interferogram for a monotonically increasing or decreasing phase function. An algorithm was developed for Bessel fringe contrast enhancement and phase extraction. The techniques were tested numerically and experimentally. Sub-fringe quantification of the time-averaged vibration fringes is realised with the proposed method. Compared with the commonly used phase shift method which requires a minimum of two images for image processing, this method requires only one fringe pattern for data extraction.     

自由电子激光振荡器的二维数值模拟

在柱二维坐标系中,用数值计算方法求解了摇摆器内电子模拟方程组、光场方程组和无源区(不含摇摆器区)经非自适应方法变换后的无源旁轴波动方程并设计了相应的程序R_2D。用该程序计算的数值结果表明,在有源条件下二维数值模拟结果与高斯光束近似下的数值模拟结果符合较好;取完全相同的计算条件R-2D程序与洛斯阿拉莫斯实验室(LANL)的FELEX程序的计算结果符合较好;初步认为LANL实验数据的物理图象合理,数值结果基本可信;最后给出北京自由电子激光器(BFEL)的一些物理数据。     

Infraglottic aspect of canine vocal fold vibration: Effect of increase of mean airflow rate and lengthening of vocal fold

The mucosal upheaval (MU), where the mucosal wave starts and propagates upward, appears only when the vocal fold vibrates. The location of the MU histologically and the effect of changes in mean air flow rate (MFR) and vocal fold length on occurrence of the MU were studied in twelve excised canine larynges. The lower surface of the vocal fold was marked to serve as a landmark for subsequent study. Cricothyroid approximation was performed to lengthen the vocal fold. After taking high-speed pictures or recording stroboscopic images from the tracheal side, a small cut wound was made at the mark. This wound served to compare the position of the MU with the histologically identified location of the mark. The larynx was then sectioned in the frontal plane. Before lengthening the vocal fold, the MU occurred on the area where the lamina propria became thinner and where the muscular layer neared the epithelial layer. After lengthening the vocal fold, the MU actually shifted medially compared with its original position. The subglottic area surrounded by the bilateral MUs became longer and thinner. Whether or not complete glottal closure during a vibratory cycle was achieved did not alter these findings. In contrast, with a fixed vocal fold length the MU appeared more laterally as MFR increased, but, based on the relation with the mark, its location on the vocal fold did not change from its original position before increase of MFR.     

自由电子激光的医学应用

自由电子激光这种新型光源非常适合于医学应用。通过对医用自由电子激光器的简要介绍,探讨了自由电子激光与人体组织的相互作用及其在医学上的应用前景。     

Viscosity solution theory of a class of nonlinear degenerate parabolic equations II. Lipschitz continuity of free boundary

In [1] we construct a unique bounded Hölder continuous viscosity solution for the nonlinear PDEs with the evolutionp-Laplacian equation and its anisotropic version as typical examples. In this part, we investigate the Lipschitz continuity of the free boundary of viscosity solution and its asymptotic spherical symmetricity, however, this result does not include the anisotropic case.This research is supported by the National Natural Sciences Foundation of China.     

Mittlere Schwingungsamplituden von OTeF 5 −

Summary Mean amplitudes of vibration for OTeF ₅ ^– have been calculated from known spectroscopic and structural data in a wide temperature range. The results are briefly discussed in comparison with those of related species.

     

After-Effects of Electrolytically diffused hydrogen in the second-order elastic coefficient of poynting’s effect in nickel and steel

Summary If hydrogen is diffused electrolytically in a metal, it subsequently escapes out if the metal is left to itself. However this hydrogen-treated metal does not totally regain the original magnitudes of its various physical properties,e. g., thermo e.m.f., electrical resistivity, elastic modulii etc. This effect has also been observed in the second-order elastic effect (the Poynting effect) in nickel and two varieties of steel. Measurements were carried out first before hydrogen diffusion. The samples were electrolytically diffused with hydrogen and the left to themselves for a few days and the measurements were repeated. The changed values of the coefficient of Poynting effect are discussed in terms of the dislocations created by in-and out-going hydrogen. Now retired     

Quantitative evaluation of two-dimensional dynamic deformations using digital holography

An optical system for the parallel evaluation of in- and out-of-plane dynamical deformations will be described. A double pulse laser with pulse separation in the microsecond range is used for the investigations. Two separate interferograms of an object under test, in its undeformed and deformed state, are recorded in a few microseconds. The object is illuminated from two different directions and imaged onto a CCD sensor. This produces two sensitivity vectors. The reference beams have different directions in order to produce two directional spatial carriers. The Fourier method is used for quantitative evaluation, and the measurements along different sensitivity vectors are separated in the Fourier domain. The phases of the two interferograms are obtained from the complex amplitudes and the two dimensional deformation is calculated from the phases. Experimental results are presented.