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41.
混合中立型方程渐近衰退正解的存在性   总被引:1,自引:0,他引:1       下载免费PDF全文
该文利用Krasnoselskii不动点定理,讨论了一阶混合中立型微分方程[x(t)-cx(t-h)-c^*x(t+h^*)]'=p(t)x(g(t)),获得了方程在p\leq p(t)<0与0相似文献   
42.
43.
部分线性变系数模型中估计的渐进正态性   总被引:1,自引:1,他引:0  
作为部分线性模型与变系数模型的推广,部分线性变系数模型是一类应用非常广泛的模型,本文基于Profile最小二乘方法给出了模型中参数分量与非参数分量的估计,并在异方差情形下证明了这些估计的渐进正态性.  相似文献   
44.
A simple, sensitive and accurate liquid chromatographic method with UV detection was developed and validated to determine voriconazole in a new emulsion formulation. Chromatographic separation was achieved on a Diamonsil C18 column (250 × 4.6 mm I.D., 5 μm) using a mobile phase consisting of acetonitrile-water-acetic acid (40:60:0.25, v/v/v) at a flow rate of 1.0 mL min?1. The UV detection wavelength was set at 256 nm. The linear calibration curves were obtained in the concentration range of 1.00–100 μg mL?1 with the limit of quantification of 1.00 μg mL?1. The within- and between-run precisions in terms of percentage relative standard deviation were lower than 7.4 and 7.1%, respectively. The accuracy in terms of percentage relative error ranged from ?1.5 to 1.4%. This validated method was successfully applied to the determination of the content of voriconazole in a new emulsion formulation.  相似文献   
45.
By revisiting the preferential attachment (PA) mechanism for generating a classical scale-free network, we propose a class of novel preferential attachment similarity indices for predicting future links in evolving networks. Extensive experiments on 14 real-life networks show that these new indices can provide more accurate prediction than the traditional one. Due to the improved prediction accuracy and low computational complexity, these proposed preferential attachment indices can be helpful for providing both instructions for mining unknown links and new insights to understand the underlying mechanisms that drive the network evolution.  相似文献   
46.
Synthesis of novel water‐soluble monotosylated ethylenediamines and their application in ruthenium and iridium‐catalyzed transfer hydrogenation of aldehydes are described. Various aldehydes, including electron‐deficient and electron‐rich variants, were reduced with high conversions and chemoselectivity using sodium formate as a hydrogen source in neat water. Copyright © 2011 John Wiley & Sons, Ltd.  相似文献   
47.
A new polyethylene glycol‐supported chiral monosulfonamide was synthesized from (R,R)‐1,2‐diaminocyclohexane and shown to act as a ligand for ruthenium(II)‐catalyzed asymmetric transfer hydrogenation of aromatic ketones in neat water using sodium formate as the hydrogen source. Good enantioselectivities were obtained and the catalyst could be easily separated from the reaction mixture and reused several times. Copyright © 2011 John Wiley & Sons, Ltd.  相似文献   
48.
为了寻找高活性的含杂环的新农药, 通过2-氨基-5-(4-吡啶基)-1,3,4-噻二唑与芳酰基异氰酸酯反应, 合成了17种新的芳酰基脲, 采用红外光谱、核磁共振氢谱与元素分析证明了其结构. 初步的活性试验表明, 部分目标化合物具有良好的植物生长调节活性, 其中2c, 2e, 2f, 2i2k具有较好的细胞分裂素活性.  相似文献   
49.
通过2-氨基-5-(4-三氟甲基苯基)-1,3,4-噻二唑与芳酰基异氰酸酯反应, 合成了14种新的芳酰基脲, 它们的结构用红外光谱、核磁共振氢谱和元素分析进行了表征, 并且采用X-射线单晶衍射分析方法测定了化合物2l的结构.初步的生物活性试验表明, 部分标题化合物具有优良的植物生长调节活性.  相似文献   
50.
Mesoporous (MSU) Ce0.5Zr0.5O2 mixed oxide with a high specific surface area has been synthesized under weak acidic condition in the presence of an anionic surfactant, sodium dodecylbenzenesulfonate. The effect of the pH value on the formation of mesostructure and the thermal stability of the material has been evaluated. The products were characterized by transmission electron microscopy, powder X-ray diffraction and nitrogen adsorption-desorption measurements. The results showed that the as-prepared Ce0.5Zr0.5O2 mixed oxide possessed a specific surface area of 163.3 m^2·g^-1, which had a cubic fluorite-type structure and possessed specific surface areas of 148.4 and 62.4 m^2·g^-1 after calcination at 500 and 800 ℃ for 2 h, respectively. The material showed excellent thermal stability.  相似文献   
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