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981.
Yuanyi Cao Shaolei Wang Haiyan Mou Haiyan Xu Chifei Wu 《Journal of Crystal Growth》2010,312(10):1747-1750
Crystal growth of a hindered phenol compound, tetrakis [methylene-3-(3-5-ditert-butyl-4-hydroxy phenyl) propionyloxy] methane (trade name AO-60), was successfully recorded by optical microscopy (OM) equipped with a hot stage. The morphology of AO-60 crystals, grown at 100 °C from amorphous state, appeared in the form of tetragonal-sloped step growth. Further study using scanning electron microscopy (SEM) and atomic force microscopy (AFM) experimentally demonstrated that AO-60 crystals had a hopper-like morphology, which had occurred rarely in the condition of organic compound crystals but predominantly rather to inorganic compound crystals in the reported literatures. The morphological features observed on the crystal surfaces suggested step growth and hopper growth mechanism. Besides, a raising around the edge of the AO-60 hopper crystal was also experimentally characterized for the first time. 相似文献
982.
In this report, we describe the noncatalytic and template-free synthesis of zinc nitride (Zn3N2) novel microstructures with hollow interiors via simple nitridation reaction of zinc powder at optimum temperature of 600° C for 120 min in ammonia gas environment under atmospheric pressure. Hollow microstructures obtained were mostly of spherical shape with diameters in the range 8–35 μm and with open mouth on the surface. The growth mechanism has been proposed for the elucidation of hollow structures formation. Crystal structure and phase purity of the product were investigated by X-ray diffraction (XRD) characterization and energy dispersive X-ray spectroscopy (EDS) analysis confirmed the chemical composition of the product. Morphology of the as-prepared product was investigated using scanning electron microscopy (SEM). Ultraviolet–visible–near infrared (UV–vis–NIR) spectrophotometry was used to study the transmittance behaviour of zinc nitride microstructures and thereby an indirect optical band gap of 2.81 eV was calculated using Davis–Mott model. Room temperature photoluminescence (PL) studies exhibited two prominent peaks of the product; one very strong peak near band edge UV emission (395 nm) and other comparatively suppressed and broad peak at orange luminescence emission (670 nm). 相似文献
983.
Shuti Li Jun Su Guanghan Fan Chao Liu Jianxing Cao Yian Yin 《Journal of Crystal Growth》2010,312(21):3101-3104
We have investigated the growth of magnesium-doped GaP (GaP:Mg) layers on GaN by metalorganic chemical vapor deposition. The hole carrier concentration increased linearly from 0.8×1018 to 4.2×1018 cm−3 as the Bis(cyclopentadienyl) magnesium (Cp2Mg) mole flow rate increased from 1.2×10−7 to 3.6×10−7 mol/min. However, the hole carrier concentration decreased when the CP2Mg mole flow rate was further increased. The double crystal X-ray diffraction (DCXRD) rocking curves showed that the GaP:Mg layers were single crystalline at low CP2Mg molar flow. However, the GaP:Mg layers became polycrystalline if the CP2Mg molar flow was too high. The decrease in hole carrier concentration at high CP2Mg molar flow was due to crystal quality deterioration of the GaP layer, which also resulted in the low hole mobility of the GaP:Mg layer. 相似文献
984.
S.R. Xu Y. Hao J.C. Zhang Y.R. Cao X.W. Zhou L.A. Yang X.X. Ou K. Chen W. Mao 《Journal of Crystal Growth》2010,312(23):3521-3524
We have investigated the unintentional impurities, oxygen and carbon, in GaN films grown on c-plane, r-plane as well as m-plane sapphire by metal-organic chemical vapor deposition. The GaN layer was analyzed by secondary ion mass spectroscopy. The different trend of the incorporation of oxygen and carbon has been explained in the polar (0 0 0 1), nonpolar (1 1 2¯ 0) and semipolar (1 1 2¯ 2) GaN by a combination of the atom bonding structure and the origin direction of the impurities. Furthermore, it has been found that there is a stronger yellow luminescence (YL) in GaN with higher concentration of carbon, suggesting that C-involved defects are originally responsible for the YL. 相似文献
985.
We study the structure of invertible substitutions on three-letter alphabet. We show that there exists a finite set
of invertible substitutions such that any invertible substitution can be written as Iwσ1σ2σk, where Iw is the inner automorphism associated with w, and
for 1jk. As a consequence, M is the matrix of an invertible substitution if and only if it is a finite product of non-negative elementary matrices. 相似文献
986.
987.
In this paper,the distance-sability of nonlinear discrete system is investigated by meansof the Gauss-Seidel iteration method.Some algebric criteria of the distance-stability are ob-tained.Construction of Lyapunov function is avoided. 相似文献
988.
1引言设A是n阶非负方阵.设矩阵方程(1)AXA=A,(2)XAX=X,(3)(AX)~T= AX,(4)(XA)~T=XA,(5)AX=XA.A具有非负广义逆是指存在非负方阵X满足方程(1)~(4),并记为A~(?).A具有非负群逆是指存在非负方阵X满足方程(1),(2),(5),并记为A~#.在A~(?)存在的前提下,两者相同的充分必要条件有(a)AA~(?)=A~(?)A;(b)A~(?)=p(A),其 相似文献
989.
After more than 20 years of impressive development since the economic reforms in 1978, today western China is facing an increasing
development gap between its regions, particularly between urban and rural areas. Using the fuzzy comprehensive evaluation
model, this paper aims to demonstrate the evolution of the economic competitiveness levels base on two categories of geographical
unity in the province of Gansu located in Northwest China between 2000 and 2004. The results of fuzzy modeling are integrated
into GIS spatiotemporal analyses in order to identify the spatial variation of each significant change in terms of the regional
economic development. Our research effectively illustrates that there is a particular spatial dynamic of the economic development
from region to region. Although the cities have improved very well in their economic competitiveness, the rural areas and
minority regions still have a lot of progress to be achieved. 相似文献
990.