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41.
A new, simple, precise, and rapid high-performance thin-layer chromatographic method was developed for the determination of 6 benzodioxanes in Piper mullesua extract: 1',3'-benzodioxole-5'-(2,4,8-triene-isobutyl nonanoate), 1',3'-benzodioxole-5'-(2,4,12-triene-isobutyl tridecanoate), fargesin, sesamin, asarinin, 1',3'-benzodioxole-5'-(2,4,8-triene-methyl nonanoate). The ingredients were separated on a precoated Silica Gel 60 F254 plate with a solvent system of toluene-acetone (92 + 8). The 6 benzodioxanes were well separated and easily identified in this chromatographic system. The separated benzodioxanes were visualized by color development with a spray reagent consisting of 1 g vanillin dissolved in 100 mL H2SO4-ethanol (5 + 95, v/v). Quantitation was performed by scanning the spots and comparing the integrated areas of compounds in samples with those of standards. Recoveries from samples spiked with known amounts of the benzodioxanes were excellent. The results were comparable with those estimated by liquid chromatography. 相似文献
42.
43.
Summary m-Phenylenedioxydiacetic acid gives a white precipitate with thorium even in the absence of an electrolyte which is quantitative up toph 4. Be2+, Mg2+, Ca2+, Zn2+, Pb2+ and Mn2+ ions are removed by single precipitation and Al3+, UO2
2+ and trivalent cerite earth ions are removed by double precipitation. Sn2+, Sn4+ and Cr3+ ions interfere.Part II: See. Z. analyt. Chem.165, 343 (1959). 相似文献
44.
C. D. Kalkar S. V. Doshi Seema Teli 《Journal of Radioanalytical and Nuclear Chemistry》1989,136(4):283-290
The oxidation of iron/II/ ions has been studied by dissolving -irradiated NaCl crystals in aqueous Fricke solution. The yield of iron/III/ ions was determined as a function of the amount of NaCl added, storage time, dose, concentration of iron/II/ ions and pH of the Fricke solution. The energy transfer parameter, , which is the ratio of G/Fe3+/ obtained by the addition of irradiated NaCl to that by direct radiolysis was evaluated. 相似文献
45.
S. K. Srivastava 《International Journal of Theoretical Physics》1995,34(1):109-125
Expressions for the time dependence of the fundamental constants are derived through dimensional reduction and one-loop quantum corrections to scalar fields. Moreover, singularity-free solutions of Einstein's field equations are obtained. Using these solutions, we discuss the time dependence of fundamental constants. It is interesting to see that the fine structure constant asymptotically approaches to 1/137,G
eff (effective four-dimensional constant) approachesG
N (Newtonian gravitational constant), and eff vanishes. Graphical representations of these results are also given for a special case. 相似文献
46.
The total and differential cross sections for the electron and positron impact excitation of hydrogen from its initially excited metastable 22S state to 32S and 32P states are reported. A distorted-wave approximation theory is used for the calculation. The angular correlation parameters, Ly and alignment angle are also reported for 22S-32P excitation. For comparison, similar first Born results are also obtained. Interesting features are noted on comparing our distorted wave results with the first Born results as well as with the other available results forn
2S andn
2P (n=2,3) excitations from the ground 12S state of hydrogen. 相似文献
47.
48.
G. S. Srivastava 《分析论及其应用》1996,12(4):96-104
The regular solutions of generalized axisymmetric potential equation
, a>−1/2 are called generalized axisymmetric potentials. In this paper, the characterizations of lower order and lower type
of entire GASP in terms of their approximation error {En} have been obtained. 相似文献
49.
50.