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71.
A. Basillais R. Benzerga H. Sanchez E. Le Menn C. Boulmer-Leborgne J. Perrière 《Applied Physics A: Materials Science & Processing》2005,80(4):851-859
The pulsed-laser-deposition (PLD) method is particularly well suited for the growth of oxide thin films, but in the case of other compounds, such as nitrides, PLD presents some limitations which are mainly due to the low reactivity of nitrogen in comparison with oxygen. A possible way to overcome this problem is to increase the reactivity of the constituent species, via plasma assisted-pulsed-laser deposition. A plasma is coupled to the ablation chamber, in order to increase the density of reactive atomic species, which can be further incorporated in the growing film. This approach is described in this paper as well as the nature, energy, and concentration of the atomic and molecular species in the plasma as determined by various plasma diagnostics. These results are correlated to the growth of thin films in the particular case of the aluminum nitride compound. The composition and structure of the films are studied as a function of the growth conditions, and the positive effects of the additional discharge are evidenced on the film purity and properties. The fundamental problem with the PLD technique, especially with metallic targets, is the production of unwanted droplets that significantly worsen the properties of the films. To eliminate these droplets, a thin film has been grown with an experimental setup using two targets and crossed laser beams which gave positive results. PACS 81.15.Fg; 52.80.Pi; 77.84.Bw 相似文献
72.
Ewald G Nörtershäuser W Dax A Götte S Kirchner R Kluge HJ Kühl T Sanchez R Wojtaszek A Bushaw BA Drake GW Yan ZC Zimmermann C 《Physical review letters》2004,93(11):113002
The 2s-->3s transition of (6,7,8,9)Li was studied by high-resolution laser spectroscopy using two-photon Doppler-free excitation and resonance-ionization detection. Hyperfine structure splittings and isotope shifts were determined with precision at the 100 kHz level. Combined with recent theoretical work, the changes in the nuclear-charge radii of (8,9)Li were determined. These are now the lightest short-lived isotopes for which the charge radii have been measured. It is found that the charge radii monotonically decrease with increasing neutron number from 6Li to 9Li. 相似文献
73.
U.?Pal J.F.?Sanchez Ramirez H.B.?Liu A.?Medina J.A.?AscencioEmail author 《Applied Physics A: Materials Science & Processing》2004,79(1):79-84
The synthesis of bimetallic nanoparticles has become so important in recent times due to its multi-faceted applications. The structure of the synthesised particles influences directly their properties. In this paper, we report the synthesis of Au/Cu nanoparticles by a simultaneous reduction method, considering three different molar concentrations (AuCu, AuCu3 and Au3Cu) of the components. In order to determine the size and structure of the obtained clusters, the particles were examined by optical spectroscopy, transmission electron microscopy and high-resolution transmission electron microscopy. One of the major factors, the minimum bimetal formation energy, was calculated by an embedded-atom method. The relation between the Au/Cu proportions has been demonstrated to affect the size of the particles and the corresponding structures. From the basic structural analysis it is found that the particles were fcc-like, multiple twin or multiple defect particles for the different Au/Cu concentrations. The smallest particles were identified for the Au/Cu sample with 50% of each, and the most crystalline structures were also obtained in the same sample. PACS 61.46.+w; 61.16.-d; 31.15.Qg 相似文献
74.
S-Alkyl dithioformates, generated by a cycloreversion process, react as 1,3-dipolarophiles with beta-lactam-based azomethine ylids to provide, after (net) elimination of MeSH, C(2)-unsubstituted penems. The overall cycloreversion/cycloaddition sequence was accelerated by microwave irradiation. [reaction: see text] 相似文献
75.
M.?AriasEmail author J.?Campos A.?M.?Robles-Pérez L.?Sanchez 《Calculus of Variations and Partial Differential Equations》2004,21(3):319-334
We study the existence of fast and heteroclinic solutions of an ODE that arises in connection with travelling wave solutions of Fisher-Kolmogorovs equation. They are obtained by solving a minimum or constrained minimum problem. A variational characterization of the minimum speed for which heteroclinic solutions exist is obtained.Received: 14 November 2003, Accepted: 29 January 2004, Published online: 2 April 2004M. Arias: Supported by MCYT, Acción Integrada HP2000-0039, SpainJ. Campos: Supported by MCYT, BFM2002-01308 and Acción Integrada HP2000-0039, SpainA.M. Robles-Pérez: Supported by Acção Integrada E-15/01 and Fundaçâo para a Ciência e a Tecnologia, Portugal 相似文献
76.
Phase noise characterization of a 10-W Yb fiber amplifier is presented, and we demonstrate phase locking of two fiber amplifiers with near-perfect fringe contrast at power levels of as much as 10 W per fiber. Coherent beam combining is maintained during the turn-on transient as well as in thermal steady-state operation. 相似文献
77.
Various organic moieties are homogeneously introduced in high quantities into mesostructured porous silica films through a general co-condensation process, which influences the self-assembly mechanism, depending on the physico-chemical properties of each function. 相似文献
78.
Wavelength beam combining of five ytterbium fiber lasers is demonstrated in a master-oscillator power-amplifier configuration at combined powers up to 6 W. The combined beam profile has an M2 value of 1.14, which is equal to that of an individual fiber. Beam steering in one dimension over 140 resolvable spots is also demonstrated. 相似文献
79.
B. Ortaç A. Hideur M. Brunel T. Chartier M. Salhi H. Leblond F. Sanchez 《Applied physics. B, Lasers and optics》2003,77(6-7):589-594
The properties of an ytterbium-doped double-clad fiber laser, passively mode-locked by nonlinear polarization rotation are investigated in this work. Cartographies of mode-locking regime versus halfwave plates orientations are presented for several values of the total cavity dispersion and for different pump powers. Bistability between the continuous and the mode-locking regimes is pointed out. The effect of the total group velocity dispersion is described with a master mode-locking equation. PACS 42.55.Wd; 42.65.Re 相似文献
80.
J.A. Hodges P. Bonville A. Forget J.P. Sanchez P. Vulliet M. Rams K. Królas 《The European Physical Journal B - Condensed Matter and Complex Systems》2003,33(2):173-181
Using 170Yb and 155Gd M?ssbauer measurements down to ∼ 0.03 K, we have examined the semiconducting pyrochlore Yb2Mo2O7 where the Mo intra-sublattice interaction is anti-ferromagnetic and the metallic pyrochlore Gd2Mo2O7 where this interaction is ferromagnetic. Additional information was obtained from susceptibility, magnetisation and 172Yb perturbed angular correlation measurements. The microscopic measurements evidence lattice disorder which is important in
Yb2Mo2O7 and modest in Gd2Mo2O7. Magnetic irreversibilities occur at 17 K in Yb2Mo2O7 and at 75 K in Gd2Mo2O7 and below these temperatures the rare earths carry magnetic moments which are induced through couplings with the Mo sublattice.
In Gd2Mo2O7, we observe the steady state Gd hyperfine populations at 0.027 K are out of thermal equilibrium, indicating that Gd and Mo
spin fluctuations persist at very low temperatures. Frustration is thus operative in this essentially isotropic pyrochlore
where the dominant Mo intra-sublattice interaction is ferromagnetic.
Received 13 January 2003 Published online 4 June 2003
RID="a"
ID="a"e-mail: hodges@drecam.saclay.cea.fr 相似文献