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951.
The qualitative composition of the lipids, the triacylglyceride content, and the fatty acid composition of the septa of the fruit of Persian walnutJuglans regia have been determined. The phenol fraction is represented in the form of phenolic carboxylic acids, phenolic aldehydes, catechins, proanthocyanidins, and oligomeric and polymeric phenolic compounds, including lignin. Polysaccharides are represented mainly in the form of xylan and glucan.Scientific Research Institute of Horticulture, Viticulture, and Wine-Making of the Georgian Academy of Agricultural Sciences, 6 Gelovani pr., Tbilisi 380015. Translated from Khimiya Prirodnykh Soedinenii, No. 2, pp. 161–164, March–April, 1998. 相似文献
952.
聚氯乙烯—丁腈橡胶—氯丁橡胶三元共混物的研究 总被引:1,自引:0,他引:1
测定了聚氯乙烯(PVC)-丁脯橡胶(NBR-29)-氯丁橡胶(CR)三元共混物的冲击性能和应力-应变行为,用动态力分析、扫描电和透射电镜研究了共混物的相容性和形态结构。结果表明,NBR-29对PVC,CR有良好的增容作用,三元共混物是部分相容的二相体系,具有良好的抗冲击性能。 相似文献
953.
本文应用双层点电荷配位场(DSPF)模型计算了Yb~(3+):Cs_2NaYbCl_6和Yb~(3+):Cs_2NaYbBr_6的能级,分析了二体系中Yb~(3+)与Cl~-、Br~-的成键。 相似文献
954.
M. S. El-Shahawi A. Z. Abu Zuhri S. M. Al-Daheri 《Fresenius' Journal of Analytical Chemistry》1994,350(12):674-677
A simple and convenient extractive spectrophotometric method for the determination of ruthenium has been developed. It is based on the oxidation of the different ruthenium (II, III or IV) species to perruthenate with potassium periodate at pH 7.8. The perruthenate is then extracted with benzyltributylammonium chloride in chloroform followed by direct spectrophotometric measurements at 342 and 380 nm. The optimum concentration range was found to be 0.1–5 mg l–1, the standard deviation ±2.1%. The method has been successfully applied to the determination of ruthenium in organoruthenium compounds. 相似文献
955.
Z. Valentová P. Vaňura E. Makrlík 《Journal of Radioanalytical and Nuclear Chemistry》1997,224(1-2):45-48
Extraction of85Sr by a nitrobenzene solution of bis-1,2-dicarbollylcobaltate in the presence of 15-crown-5 (15C5, L) has been investigated. The equilibrium data and the typical maxima concerning the dependencies of the Sr distribution ratios on the analytical concentration of 15C5 in the system under study can be explained assuming that the HL+, HL2
+ and SrL2
2+ species are extracted into the nitrobenzene phase. The values of the corresponding extraction and stability constants of the extracted species in nitrobenzene saturated with water have been determined. 相似文献
956.
由2-氰-5-氟-3H-4-嘧啶酮和取代苯酚钠在常压下反应,合成了7个未见文献报道的2-芳氧基-5-氟-3H-4-嘧啶酮化合物,产率70 ̄87%,结构经IR、^1H NMR和MS证实。 相似文献
957.
毛细管电泳安培法检测中的在柱场放大效应 总被引:5,自引:1,他引:5
本文首次报道用安培电化学检测器探讨毛细管电泳分离的场放大进样效应,分析了系统峰的形成以及场放大进样对电泳分离检测的影响。采用25μm内径毛细管电泳分离,对去甲肾上腺素(NE)和儿茶酚(CAT)分别可达0.4nmol/L和1.5nmol/L的浓度检测限,有效提高了毛细管电泳安培法检测的灵敏度。 相似文献
958.
This paper reports the separation and determination of V(V), Nb(V) and Ta(V) by RP-HPLC using 5-Br-PADAP as a precolumn derivatizing reagent. On C(18) column, the three metal chelates can be separated on a baseline in 9 min with the mobile phase of methanol-water (59:41, v/v) containing tartaric acid (0.2%) and acetate buffer (pH 3.5, 10 mM). The detection limits of V(V), Nb(V) and Ta(V) are 0.13 ppb, 0.22 ppb and 1.79 ppb, respectively when S/N is 3. This method is simple and rapid, and has been used in mineral analysis with satisfactory results. 相似文献
959.
The structural change from the porphyrin free base to monoacid and diacid by successive protonation has been studied by the IR, visible and NMR spectroscopy. The results have indicated that the cation and anion of the porphyrin diacid are strongly associated through H-bonding. The far IR spectra show especially marked differences in the free base, monoacid, and diacid due to the changes of the inner core of the porphyrin ring. 相似文献
960.
First-principles molecular dynamics simulations are carried out to study the structures, dynamics, and electronic properties of liquid Al88Si12 in the temperature ranging from 898 to 1298 K. The temperature dependence of static structure factors, pair correlation functions, and electronic density-of-states are investigated. The structural properties obtained from the simulations are in good agreement with the x-ray diffraction experimental results. 相似文献