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991.
A facile and efficient synthetic methodology for the preparation of aza-pyrimidone and beno-pyrimidone derivatives is described, in which the triazinone ring and dihydroquinazolin-2(1H)-one was convenient constructed. The structures of all the newly synthesized compounds were characterized by mass, 1H NMR, and infrared spectroscopy. In additional, the crystal of pymetrozine was obtained to find useful information such as configuration and molecular action mechanisms. 相似文献
992.
Efficient and accurate procedure for selecting ground motions matching target response spectrum 总被引:2,自引:0,他引:2
Linear and nonlinear response history analyses have become popular in seismic design and seismic performance evaluation procedures. The accuracy of analysis results depends not only on the accurate analytic models for structures but also on the proper selection of input ground motions. The purpose of this study is to develop a computationally efficient and accurate procedure for selecting ground motions considering the target response spectrum mean and variance, and the correlations between response spectra of different periods. In this procedure, a number of response spectra are simulated equal to the number of ground motions to be selected, using a Monte Carlo simulation. Subsequently, ground motions are selected from a ground motion library to individually match the simulated response spectra, using the proposed selection procedure. This procedure is computationally efficient and accurate in selecting a ground motion that best matches a simulated response spectrum and in determining a scaling factor for the selected ground motion. In order to further improve the selection result, multiple sets of simulated response spectra are considered. The accuracy and efficiency of the proposed procedure are verified with numerical examples. 相似文献
993.
994.
Highly efficient AgNO3‐catalyzed approach to 2‐(benzo[d]azol‐2‐yl)phenols from salicylaldehydes with 2‐aminothiophenol, 2‐aminophenol and benzene‐1,2‐diamine 下载免费PDF全文
A new, convenient and efficient AgNO3‐catalyzed strategy for the preparation of 2‐(benzo[d]azol‐2‐yl)phenol derivatives in good to excellent yields (63–98%) is described. The reaction proceeds via condensation/intramolecular nucleophilic addition/oxidation process between substituted salicylaldehydes and 2‐aminothiophenol, 2‐aminophenol or benzene‐1,2‐diamine under mild reaction conditions. Notably, this reaction utilizes cheap AgNO3 as a readily available and low‐cost benign oxidant at low catalyst loadings with excellent functional group tolerance. 相似文献
995.
996.
Fang Dong Rong-Zhang Jin Jian-Quan Liu Xiang-Shan Wang 《Research on Chemical Intermediates》2017,43(11):5995-6006
997.
Inside Cover: An Extra‐Large‐Pore Zeolite with 24×8×8‐Ring Channels Using a Structure‐Directing Agent Derived from Traditional Chinese Medicine (Angew. Chem. Int. Ed. 22/2018) 下载免费PDF全文
998.
Jin Liu Xianxue Wang Han Guo Xiaokang Shi Xiaoyu Ren Guosheng Huang 《Tetrahedron》2012,68(5):1560-1565
A novel NH4OAc/CuBr(PPh3)3-induced intermolecular Pummerer-type reaction between free (NH)-indoles and dimethylsulfoxide is first reported, which offers the 3-methylthiomethyl substituted indoles conveniently and efficiently. 相似文献
999.
Da Quan Zhang Xing Jin Bin Xie Hyung Goun Joo Li Xin Gao Kang Yong Lee 《Surface and interface analysis : SIA》2012,44(1):78-83
The corrosion inhibition of ammonium heltamolybdate (AH) and calcium gluconate (CG) for AA6061 alloy in 3% NaCl solution was investigated by the electrochemical measurements. It indicates that AH inhibits the corrosion of AA6061 alloy and acts as an anodic inhibitor. Maximum inhibition efficiency reaches 74.3% at the concentration of 1 × 10?4 mol.l?1 AH. The results of the electrochemical studies reveal AH is physically adsorbed on the AA6061 alloy surface and the adsorption follows Langmuir isotherm. The combination of AH and CG enhances the inhibition efficiency to 95.9%. The enhanced inhibition is attributed to the promotion of AH adsorption by CG. The mixture of AH and CG is a mixed‐type inhibitor and renders the corrosion potential to more positive values. Copyright © 2011 John Wiley & Sons, Ltd. 相似文献
1000.