A Novel Octanuclear Molecular Loop Formed by Linkage of Oxo-centered Triruthenium Cluster Units

A novel dimeric complex [Ru3^111,111,11(μ3-O)(μ-CH3COO)(CO)]2(μ-dppf)(μ-odppf) (dppf=1, 1‘-bis(diphenylphosphio)ferrocene, odppf = 1, 1‘-bis(oxodiphenylphosphoranyl)ferrocene) (1) of oxo-centered triruthenium-aectate cluster units was synthesized and characterized by X-ray crystallography. Compound 1 exhibits a cyclic structure formed by linkages of two triruthenium cluster units Ru3^111,111,11(μ3-O)(μ-CH3COO)6(CO) through dppf and odppf ligands, respectively. The diameter of the molecular loop is ca. 1.0 rim.     

关于有限群极大子群的强θ-完备

本文定义了有限群极大子群的强θ-完备这一概念．通过研究极大子群的强θ-完备对群结构的影响,给出了有限群可解性,超可解性,幂零性的一些新刻画,所得结果改进了以往的定理．     

The Microwave-assisted Preparation and X-Ray Structure of 3-Bromocarbazole-N-Acetic Acid

Carbazole and its derivatives have attracted the attention due to its photophysical and photochemical properties as well as biological activities1. So far considerable amounts of carbazole derivatives were prepared to probe the nature of electronic states. Among these carbazole derivatives, carbazole-9-carboxylic acids were important intermediates because the carboxylic group is an active function group for further transformation into other functions. The molecular packing modes of carboxylic …     

激光照射人血液荧光光谱变化的研究

采用OMA Ⅲ微弱信号检测系统研究了人血液荧光光谱在激光照射下的变化情况。结果表明 :在6 32 8nmHe Ne激光诱导下 ,不同血液在 6 70 ,730 ,981nm附近出现三个荧光峰 ;荧光强度在一定范围内与照射激光功率呈线性变化关系 ;随着激光照射时间的增加 ,三个峰位上的荧光强度下降 ,8min后趋于隐定值 ;在激光照射过程中 ,三个峰位出现不同数值的移动。     

Heisenberg自旋链系统的初边值问题

本文研究Heisenberg自旋链系统的非齐次初边值问题光滑解的存在性与唯一性.运用有限差分法与精细的先验估计,对具有Gilbert阻尼的Heisenberg自旋链系统进行了研究.     

火焰原子吸收法快速测定土壤中钙和镁

本文报道在燃烧头偏转的情况下，研究了火焰原子吸收法测定高浓度钙镁时的干扰及消除，拟定了在大量共存离子存在下直接测定土壤消煮液中高浓度钙镁的方法。本法简单、快速。     

激光血管外照射治疗可行性研究

为探讨激光血管外照射治疗的可行性,测试了人活体血管外照射以及模拟血管内照射的光能流率分布情况。研究表明,激光血管内、外照射的总光能流率的平均值分别为10.81W/cm²与1.11W/cm²,两者相差一个数量级。为获得血管内照射相应的光能流率,建议采用20mW632.8nmHe-Ne激光;垂直入射于人皮肤外表:尽可能选择血管暴露的病人或较为暴露的血管;选择被照射血管直径为6mm左右。本实验结果,特别是在人活体血管内探测到的实验数据,将有益于光在人体组织内传播特性的研究。     

CCD相机象移的补偿

本文对CCD相机由象移造成的图象退化进行了分析,并对图象的恢复机理进行了探讨,提出了相应的象移补偿方法,给出了相应的算法及程序.     

The approximate Jordan forms of operators on Σ_e~1 type Banach spaces

This paper studies the structure of operators on Σ1e type Banach spaces.It solves the problem of the small compact perturbations of operators with connected spectra.Namely,it shows that every operator with a connected spectrum on separable Σ1e type Banach spaces is a small compact perturbation of a strongly irreducible operator.Based on this result,this paper establishes the approximate Jordan forms of operators on Σ1e type Banach spaces with Schauder bases.