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61.
In this paper, we report electronic temperature measurement in a Rb ultracold plasma formed in a magneto-optical trap. We used the ion evaporation rate and the model presented by Comparat et al. [Mon. Not. R. Astron. Soc. 361, 1227 (2005)] to extract the electronic temperature in the plasma as a function of the energy difference between the laser photon and the ionization threshold. The obtained results are similar to those obtained in Cs; however, they do not seem to show any saturation. Comparison with other models may lead to improvements in the experiments and the theoretical models. 相似文献
62.
Atomistic simulations were performed to investigate the lattice parameters, dielectric constant, and elastic constants of Y3(GaxAl5−x)O12 (x = 1, 2, 3, 4, 5) structures. The calculated lattice parameters and elastic constants are in good agreement with those in available experimental results. The pressure dependence of all studied quantities was investigated. In general, a change in the behavior of all studied quantities is found when the Ga concentration becomes more than that of the aluminum (Al) in Y3(GaxAl5−x)O12 (x = 1, 2, 3, 4, 5) structures. 相似文献
63.
César IC Byrro RM de Santana E Silva Cardoso FF Mundim IM de Souza Teixeira L Rezende KR da Silva EP Gomes SA de Sousa VA Bonfim RR Pianetti GA 《Biomedical chromatography : BMC》2012,26(7):851-856
A rapid method for the quantification of glucosamine in human plasma using high‐performance liquid chromatography coupled to tandem mass spectrometry was developed and validated. The sample preparation includes a simple deproteinization step, using d ‐[1‐13C] glucosamine hydrochloride as an internal standard. Chromatographic separation was performed on an ACE Ciano column using isocratic elution with acetonitrile and aqueous 2 mm ammonium acetate containing 0.025% formic acid (80:20). Selected reaction monitoring was performed using the transitions m/z 180.1 → m/z 72.1 and m/z 181.0 → m/z 74.6 to quantify glucosamine and internal standard, respectively. The method was validated and proved to be linear, accurate and precise over the range 50–5000 ng/mL of glucosamine. Recovery rates higher than 90% were obtained for both glucosamine and internal standard. No matrix effect was detected in the samples. The validated method was successfully applied to a pharmacokinetic study after oral administration of a powder for oral solution formulation containing glucosamine sulfate. Copyright © 2011 John Wiley & Sons, Ltd. 相似文献
64.
Daniel Luciano Falkoski Valéria Monteze Guimarães Maíra Nicolau de Almeida Acelino Couto Alfenas Jorge Luiz Colodette Sebastião Tavares de Rezende 《Applied biochemistry and biotechnology》2012,166(6):1586-1603
The aim of this work was to evaluate the biochemical features of the white-rot fungi Pycnoporus sanguineus cellulolytic complex and its utilization to sugarcane bagasse hydrolysis. When cultivated under submerged fermentation using
corn cobs as carbon source, P. sanguineus produced high FPase, endoglucanase, β-glucosidase, xylanase, mannanase, α-galactosidase, α-arabinofuranosidase, and polygalacturonase
activities. Cellulase activities were characterized in relation to pH and temperature. β-Glucosidase and FPase activities
were higher at 55 °C, pH 4.5, and endoglucanase activity was higher at 60 °C, in a pH range of 3.5–4.0. All cellulase activities
were highly stable at 40 and 50 °C through 48 h of pre-incubation. Crude enzymatic extract from P. sanguineus was applied in a saccharification experiment using acid-treated and alkali-treated sugarcane bagasse as substrate, and the
hydrolysis yields were compared to that obtained by a commercial cellulase preparation. Reducing sugar yields of 60.4% and
64.0% were reached when alkali-treated bagasse was hydrolyzed by P. sanguineus extract and commercial cellulase, respectively. Considering the glucose production, it was observed that P. sanguineus extract and commercial cellulase ensured yields of 22.6% and 36.5%, respectively. The saccharification of acid-treated bagasse
was lower than that of alkali-treated bagasse regardless of the cellulolytic extract. The present work showed that P. sanguineus has a great potential as an enzyme producer for biomass saccharification. 相似文献
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66.
Marcos V. dos S. Rezende Paulo J.R. Montes Mário E.G. Valerio 《Journal of luminescence》2012,132(5):1106-1111
The luminescence properties of Ce3+ in BaAl2O4 are reported. The results of simultaneous measurements of XEOL and XAS in the X-ray energy range that includes the Ba LII,III-edges and Ce LIII edge are shown. The XEOL yield increases as the energy of the photons increases. The radioluminescence spectra, taken from 200 to 1100 nm, showed broad emission bands corresponding to 5d1→2F5/2, 2F7/2 transitions of Ce3+ when incorporated into two nonequivalent Ba sites. The lifetime of the light emission was also measured using the single bunch operation mode at the Brazilian National Synchrotron Laboratory (LNLS), and BaAl2O4:Ce3+ showed single exponential decay time component of about 44.3 ns. 相似文献
67.
In the investigations of antiferromagnetic (AF)/ferromagnetic (FM) bilayer samples, often distinct experimental techniques yield different values for the measured exchange anisotropy field (HE). We propose that the observed discrepancy may be accounted in part by the dependence of the unidirectional anisotropy with the value of the externally applied cooling field (h). Using a simple microscopic model for representing the AF/FM interface, which incorporates the effect of interface roughness, we show that the interface energy between the AF and FM layer indeed varies with h, as recently observed in anisotropic magnetoresistance measurements, lending support to our proposal. 相似文献
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