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61.
Matthew Wallace Andre Zamith Cardoso Dr. William J. Frith Dr. Jonathan A. Iggo Dr. Dave J. Adams 《Chemistry (Weinheim an der Bergstrasse, Germany)》2014,20(50):16484-16487
The magnetic‐field‐induced alignment of the fibrillar structures present in an aqueous solution of a dipeptide gelator, and the subsequent retention of this alignment upon transformation to a hydrogel upon the addition of CaCl2 or upon a reduction in solution pH is reported. Utilising the switchable nature of the magnetic field coupled with the slow diffusion of CaCl2, it is possible to precisely control the extent of anisotropy across a hydrogel, something that is generally very difficult to do using alternative methods. The approach is readily extended to other compounds that form viscous solutions at high pH. It is expected that this work will greatly expand the utility of such low‐molecular‐weight gelators (LMWG) in areas where alignment is key. 相似文献
62.
Maryam Khaleel Andrew J. Wagner Prof. K. Andre Mkhoyan Prof. Michael Tsapatsis 《Angewandte Chemie (International ed. in English)》2014,53(36):9456-9461
A structural study of a hierarchical zeolite X, which is similar to the one first synthesized by Inayat et al., 12 was performed using transmission electron microscopy imaging and diffraction. Evidence is provided, by comparison to simulations, that this material is an intergrowth of FAU and EMT and a conceptual model is presented for the growth of the FAU material with a small fraction of EMT in an atypical morphology of assembled sheets with well‐defined intersection angles. 相似文献
63.
Macromolecule Loading into Spherical,Elliptical, Star‐Like and Cubic Calcium Carbonate Carriers 下载免费PDF全文
Dr. Bogdan V. Parakhonskiy Dr. Alexey M. Yashchenok Dr. Senem Donatan Dr. Dmitry V. Volodkin Dr. Francesco Tessarolo Prof. Renzo Antolini Prof. Helmuth Möhwald Prof. Andre G. Skirtach 《Chemphyschem》2014,15(13):2817-2822
We fabricated calcium carbonate particles with spherical, elliptical, star‐like and cubical morphologies by varying relative salt concentrations and adding ethylene glycol as a solvent to slow down the rate of particle formation. The loading capacity of particles of different isotropic (spherical and cubical) and anisotropic (elliptical and star‐like) geometries is investigated, and the surface area of such carriers is analysed. Potential applications of such drug delivery carriers are highlighted. 相似文献
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B. I. Reznikov S. V. Bobashev B. G. Zhukov R. O. Kurakin S. A. Ponyaev S. I. Rozov 《Technical Physics》2014,59(4):499-502
The concept of an effective erosion coefficient, which takes into account the capture and entrainment in motion (by accelerated plasma) of only part of the erosion mass lost by rail accelerator electrodes, is introduced to describe the plasma acceleration dynamics in the channel of an electromagnetic rail accelerator. This parameter is determined from a comparison of the experimental and calculated plasma velocities at the stage of velocity saturation. The plasma velocity is calculated using a model that takes into account the pressure force of a shock-compressed gas and the deceleration force that appears during the capture of the erosion mass by a plasma piston. The ratio of the captured mass to the mass lost by the electrodes is found to depend on the current; for copper, this ratio is 1/4–2/3. The effective erosion coefficient is 0.6–0.7 mg/C at a current of ~40 kA. 相似文献
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S. V. Bobashev Yu. P. Golovachov N. P. Mende P. A. Popov B. I. Reznikov V. A. Sakharov A. A. Schmidt A. S. Chernyshev S. Z. Sapozhnikov V. Yu. Mityakov A. V. Mityakov 《Technical Physics》2008,53(12):1634-1635
The surface temperature of a model body of revolution placed in a pulsed supersonic nitrogen flow is measured with the help of a gradient heat flux sensor. From the measured temperature, a heat flux toward the surface of the body is determined. The steady flow of a viscous transcalent gas about the body is numerically calculated. The results of the numerical calculation and measuring data are in good agreement. 相似文献
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J.A. Pinston W. Mampe R. Roussille K. Schreckenbach D. Heck H.G. Börner H.R. Koch S. Andre D. Barneoud 《Nuclear Physics A》1979,321(1):25-44
Gamma and electron spectra following thermal neutron capture on 99Tc have been studied with a bent-crystal spectrometer, Ge(Li) and Si(Li) detectors and a magnetic spectrometer. Prompt and delayed γ-γ coincidences with Ge(Li) detectors have been performed. A level scheme is proposed for 100Tc comprising 21 excited states up to 640 keV. The binding energy of the last neutron in 100Tc was deduced. For most levels, spin and parity values were assigned. Two isometric transitions of respective half-lives 10.2 and 4.6 μs have been identified using the 100Mo(d, 2n)100Tc reaction with a pulsed beam of deuterons. From the comparison of the present (n, γ) study and the collaborative study of the 99Tc(d, p) reaction, several members of the multiplets , , and have been identified. 相似文献