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21.
P. M. Rafailov A. V. Egorysheva T. I. Milenov V. D. Volodin G. V. Avdeev R. Titorenkova V. M. Skorikov R. Petrova M. M. Gospodinov 《Applied physics. B, Lasers and optics》2010,101(1-2):185-192
Single-crystalline species of the novel compounds BaBiBO4 and CaBi2B2O7 with Pna21 structure were successfully grown by the top-seed solution growth (TSSG) method and solid-state recrystallization, respectively. X-ray diffraction methods were used to confirm the symmetry of the crystal structure and to determine unit cell parameters. Normal-mode classification and assignment were performed from the results of polarized Raman and IR absorption measurements on the obtained crystals. The high-frequency part of the vibrational spectra of both materials (580–1400 cm?1) is reminiscent of the normal modes of the isolated [BO3]3? group. The expected crystal-field induced changes in these modes from group-theoretical considerations provide important clues for the normal-mode assignment of the high-frequency spectral lines. 相似文献
22.
The thermal dehydration of CuSeO3·2 H2O, and the thermal dissociation of CuSeO3 and Ag2SeO3 are studied. The mechanism of these processes is suggested. The heats of phase transitions and the specific heats of the corresponding compounds are determined. 相似文献
23.
Investigation of Phase Equilibria in the Systems Sb2O3? SO3? H2O and Bi2O3? SO3? H2O Phase equilibria in the systems Sb2O3? SO3? H2O and Bi2O3? SO3? H2O within the concentration range of 1 up to 98.5% H2SO4 at 100°C are studied. In the system Sb2O3? SO3? H2O crystallization fields of five compounds depending on the H2SO4 concentration were determined: 5Sb2O3 · Sb2(SO4)3 · 3H2O; 7Sb2O3 · 2Sb2(SO4)3; 2Sb2O3 · Sb2(SO4)3; Sb2O3 · Sb2(SO4)3 and Sb2(SO4)3. The obtained compounds are identified by chemical and derivatographic analysis. 相似文献
24.
G. Gospodinov 《无机化学与普通化学杂志》1985,525(6):237-240
Isotherms of Solubility and Thermal Stability of the Phases in the System CdSeO4? H2SeO4? H2O at 100°C The isotherms of solubility in the system CdSeO4? H2SeO4? H2O were studied and constructed at 100°C. Existence fields of CdSeO4 · H2O and CdSeO4 were determined. The compounds are isolated in pure form and their crystallographic characteristics are calculated. The mechanism of thermal dehydration and dissociation is shown. 相似文献
25.
The temperature dependence of the molar heat capacities of the tellurites
PbTeO3, Pb2Te3O8
and Ge(TeO3)2 are determined.
By statistical manipulation of the values obtained, the parameters in the
equations for the corresponding compounds showing this dependence are determined
using the least-squares method. These equations and the standard molar entropies
are used to determine the thermodynamic functions Δ0
T
S
m
0
, ΔT
T
H
m
0 and (Φm
0+Δ0
T
H
m
0/T) for T'=298.15
K. 相似文献
26.
27.
Skumryev V Laukhin V Fina I Martí X Sánchez F Gospodinov M Fontcuberta J 《Physical review letters》2011,106(5):057206
We demonstrate that the magnetization of a ferromagnet in contact with an antiferromagnetic multiferroic (LuMnO(3)) can be speedily reversed by electric-field pulsing, and the sign of the magnetic exchange bias can switch and recover isothermally. As LuMnO(3) is not ferroelastic, our data conclusively show that this switching is not mediated by strain effects but is a unique electric-field driven decoupling of the ferroelectric and antiferromagnetic domain walls. Their distinct dynamics are essential for the observed magnetic switching. 相似文献
28.
Lubka Atanasova Ginka Baikusheva-Dimitrova Georgy Gospodinov 《Journal of Thermal Analysis and Calorimetry》2014,118(1):493-497
Tellurites of CuTeO3 and HgTeO3 are synthesized and their specific molar heat capacities are experimentally determined for the first time. The tellurites discussed in the present paper are used for preparation of optical glasses with special properties for optoelectronics, nuclear and power industries. The tellurites synthesized are prepared for chemical analysis, differential thermal analysis and X-ray analysis. The use of the tellurites studied is related to knowing their thermodynamic properties like specific molar heat capacity (C p,m), enthalpy \( \left( {\Delta_{{{\text {T}}^{\prime}}}^{\text{T}} H_{\text{m}}^{0} } \right), \) entropy \( \left( {\Delta_{{{\text {T}}^{\prime}}}^{\text{T}} S_{\text{m}}^{0} } \right) \) and Gibbs energy \( \left( { - \Delta_{{{\text {T}}^{\prime}}}^{\text{T}} G_{\text{m}}^{0} } \right) \) . The temperature dependences of their molar heat capacities are determined using the least squares method. The thermodynamic properties are calculated: entropy, enthalpy and Gibbs function. 相似文献
29.
30.