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991.
Marian Vâjâitu 《Algebras and Representation Theory》2013,16(6):1611-1620
Given a prime number p and K a compact subset of ? p , the topological completion of the algebraic closure of the field of p-adic numbers, we are interested in integral representations for a class of Krasner analytic functions defined on ${\mathbb{P}}^1({\mathbb{C}}_p)\setminus K$ with values in ${\mathbb{P}}^1({\mathbb{C}}_p)$ . We apply these results to study the behavior of Krasner analytic functions around singular points. 相似文献
992.
Victor Alexandru Nicolae Popescu Marian Vâjâitu Alexandru Zaharescu 《Algebras and Representation Theory》2013,16(3):895-904
Given a prime number p and a compact subset X of the topological completion ? p of the algebraic closure of the field of p-adic numbers, we study the set of zeros of Krasner analytic functions defined on ?1(? p ) \ X with values in ? p . 相似文献
993.
RM Maria TB Moraes CJ Magon T Venâncio WF Altei AD Andricopulo LA Colnago 《The Analyst》2012,137(19):4546-4551
Proton nuclear magnetic resonance ((1)H NMR) spectroscopy for detection of biochemical changes in biological samples is a successful technique. However, the achieved NMR resolution is not sufficiently high when the analysis is performed with intact cells. To improve spectral resolution, high resolution magic angle spinning (HR-MAS) is used and the broad signals are separated by a T(2) filter based on the CPMG pulse sequence. Additionally, HR-MAS experiments with a T(2) filter are preceded by a water suppression procedure. The goal of this work is to demonstrate that the experimental procedures of water suppression and T(2) or diffusing filters are unnecessary steps when the filter diagonalization method (FDM) is used to process the time domain HR-MAS signals. Manipulation of the FDM results, represented as a tabular list of peak positions, widths, amplitudes and phases, allows the removal of water signals without the disturbing overlapping or nearby signals. Additionally, the FDM can also be used for phase correction and noise suppression, and to discriminate between sharp and broad lines. Results demonstrate the applicability of the FDM post-acquisition processing to obtain high quality HR-MAS spectra of heterogeneous biological materials. 相似文献
994.
Dual feasible functions have been used to compute fast lower bounds and valid inequalities for integer linear problems. In this paper, we analyze the worst-case performance of the lower bounds provided by some of the best functions proposed in the literature. We describe some worst-case examples for these functions, and we report on new results concerning the best parameter choice for one of these functions. 相似文献
995.
Sanches-Silva A Ribeiro T Albuquerque TG Paseiro P Sendón R de Quirós AB López-Cervantes J Sánchez-Machado DI Valdez HS Angulo I Aurrekoetxea GP Costa HS 《Journal of separation science》2012,35(5-6):633-640
Chitosan, a multiple applications molecule, was isolated from shrimp by-products by fermentation. The amount of chitosan in the solid fraction of the fermented extract was measured after its conversion in the respective glucosamine units. The procedure includes an acid hydrolysis (110 °C, 4 h with HCl 8 M) and a derivatization with 9-fluorenylmethyl chloroformate (Fmoc-Cl). Ultra-high-pressure liquid chromatography method was developed and optimized. Excellent peaks resolution was achieved in just 10 min. The method was evaluated in what concerns to validation parameters such as linearity, repeatability, quantification limit, and recovery. Migration tests of films prepared with chitosan were carried out in two simulants: ultrapure water and ethanol 95% (v/v). 相似文献
996.
The retention behavior for a series of biogenic amines and related sympathomimetic drugs has been investigated in reversed-phase thin-layer chromatography using RP-2, RP-8, RP-18W, and Diol stationary phase and mixtures of phosphate buffer (pH = 7.10) and methanol in different proportions as mobile phases. Several methodologies like arithmetic mean of experimental retention values, extrapolation to zero methanol concentration procedure and principal component analysis were applied to retention data values (R(M)) in order to determine relevant parameters (mean of R(M) - mR(M), R(M0), and scores corresponding to the first principal component - PC1/R(M) respectively) encoding information on the lipophilic behavior of compounds. High similarities in lipophilicity behavior of investigated amines were highlighted by mR(M) and PC1/R(M) lipophilicity indices for all of the studied stationary phases. The experimental results were compared with some computed lipophilicity parameters expressed as distribution coefficients at working pH (logD), partition coefficients (logP(N), logP(I), and diff(logP(N-I))) concerning both neutral and fully protonated species and difference between both species, and also with various lipophilicity values (logP) generated by different commonly used software. Significant correlations were observed between the experimental lipophilicity indices mR(M) respectively PC1/R(M) and diff(logP(N-I) ) values in all cases. 相似文献
997.
Claudianor O. Alves Marco A. S. Souto Marcelo Montenegro 《Calculus of Variations and Partial Differential Equations》2012,43(3-4):537-554
In the present paper, we establish the existence of Ground State Solutions for some class of Elliptic problems with Critical Growth in ${\mathbb{R}^{N}}$ for N ≥ 2. Our results complete the study made in Berestycki and Lions (Arch Rat Mech Anal 82:313–346, 1983) and Berestycki, Gallou?t and Kavian (C R Acad Sci Paris Ser I Math 297:307–310, 1984), in the sense that, in those papers only the subcritical growth was considered. 相似文献
998.
K. De S. Das A. Roy V.S. Amaral S. Majumder S. Giri P.K. Mahapatra 《Physica B: Condensed Matter》2012,407(13):2442-2446
The magnetic and electrical transport properties of La0.9Mn0.9M0.1O3 (M=Mn, Zn and Ti) were investigated. The temperature and magnetic field dependence of electrical resistivity (ρ) and dc magnetization were studied. All the compounds are found in rhombohedral structure. The excess oxygen in all three compounds was detected through iodometric titration. A modification in resistivity is observed when M=Mn is replaced by M=Zn and Ti. The high temperature resistivity above TC follow variable range hopping model for both Zn and Ti compounds. For Zn doping, the observation of large field-cool effect and decrease in resistivity at room temperature and is assumed to be due to the implant of Mn4+ in Mn3+ matrix, which favor Mn3+/Mn4+ double exchange. The ferromagnetic behavior below TC for the compound with M=Ti is correlated to the excess oxygen in it, which implants Mn4+ and thus incorporates ferromagnetic interactions. The substitutions lead to a reduction of Tc and magnetization. 相似文献
999.
Cavalcanti MG Filho FC Mendonça AM Duarte GR Barbosa CC De Castro CM Alves LC Brayner FA 《Micron (Oxford, England : 1993)》2012,43(2-3):285-291
Biomphalaria glabrata and Biomphalaria straminea have been identified as intermediate hosts for Schistosoma mansoni. Several studies have found two cell types in the hemolymph of B. glabrata (hyalinocytes and granulocytes). However, there are no studies describing the hemocytes of B. straminea. With the aim of further describing the hemocyte subsets in B. glabrata and B. straminea, we conducted a detailed study using optical microscopy and transmission electron microscopy. Based on the morphological characteristics of the cells, we identified the same types of hemocytes in two species of molluscs, namely: blast-like cells, granulocytes, type I hyalinocytes, type II hyalinocytes and type III hyalinocytes. Blast-like cells had a spherical profile with a central nucleus filling almost the whole cell. Granulocytes were characterized by presenting variable numbers of granules. Type I hyalinocytes were the most abundant cell type and displayed various cytoplasmic projections. Type II and type III hyalinocytes had never previously been reported. They were few in number and were characterized by having an eccentric nucleus. From these results, it is concluded that there are five types of cells in the hemolymph of B. glabrata and B. straminea. Further studies are now needed to identify the role of these hemocytes in the immune response of these snails. 相似文献
1000.
da Cunha FM Caetano FH Wanderley-Teixeira V Torres JB Teixeira AA Alves LC 《Micron (Oxford, England : 1993)》2012,43(2-3):245-250
The toxic effects of Bt proteins from the body of the prey/host to predators and parasitoids have been investigated as a route of impact on non-target insects of Bt crops. This research aimed to analyze ultrastructural changes and histochemistry in digestive cells of the middle region of the midgut of Podisus nigrispinus fed, since its second instar, with Spodoptera frugiperda reared on Bt cotton variety Acala90 B, which expresses the toxin Cry 1Ac, and its non-Bt isoline Acala 90. Fragments of the midgut of P. nigrispinus were analyzed by electron microscopy. For the histochemical analysis, Bromophenol Blue, Periodic Acid Schiff von Kossa, Alcian Blue pH 2.5 and Sudan Black were used. The Cry1Ac toxin of Bt cotton ingested by S. frugiperda promotes a disorganization in the perimicrovillar matrix of P. nigrispinus (third trophic level), thus generating ultrastructural changes in the digestive cells, as elongation of microvilli, presence of spherocrystals and granules of different electron densities, in addition to altering the distribution pattern of glycogen, lipids and calcium of these cells in the median region of the midgut. Thus, we conclude that species moderately susceptible to Cry1Ac toxin, such as S. frugiperda, can acquire this toxin and expose it to P. nigrispinus, which can interfere with your ability to predation. 相似文献