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71.
Here, we report multiwalled carbon nanotubes (MWCNTs) functionalized with γ-cyclodextrins (γCD) as a novel electrochemical strategy for Rutin determination, showing superior performance than β-cyclodextrins (βCD) modified MWCNTs, suggesting an adequate environment for host-guest interactions. Under optimized conditions, the sensor showed a linear range of 39–975 nmol L−1 and a limit of detection of 7 nmol L−1. When tested with quercetin, catechin, and caffeine, the platform presented high selectivity with an interference response <10 %. The method was employed to quantify Rutin in spiked pharmaceutical and herbal extracts, providing recovery of 93–98.4 %. Also, HPLC-PDA confirmed the method‘s accuracy.  相似文献   
72.
Given two epimorphisms of algebras A ? B and C ? B, we consider the pullback R. We introduce a particular class of algebras, the tree oriented pullback, where there is a close relationship between the category of indecomposable modules of these algebras. This leads us to prove that if A and C are hereditary algebras, then R is a tilted algebra.  相似文献   
73.
Economic theory relates prices to quantities via ” market curves.” Typically, such curves are monotone, hence they admit functional representations. The latter invoke linear pricing of quantities so as to obtain market values. Specifically, if higher prices call forward greater supply, a convex function, bounded below by market values, represents the resulting supply curve. Likewise, if demand decreases at higher prices, a concave function, bounded above by market values, represents the attending demand curve. In short, grantedmonotonicity, market curves are described by bivariate functions, either convex or concave, appropriately bounded by linear valuations of quantities. The bounding supply (demand) function generates ask (resp. bid)valuations. Exchange and trade, as modelled here, are driven by valuation differentials, called bid-ask spreads. These disappear, and market equilibrium prevails, if all ”inverse market curves” intersect in a common price. A main issue is whether and how market agents, by themselves, may reach such equilibrium. The paper provides positive and constructive answers. As vehicle it contends with bilateral transactions.  相似文献   
74.
The distinguished econometrician Ragnar Frisch (1895–1973) also played an important role in optimization theory. In fact, he was a pioneer of interior-point methods. This note reconsiders his contribution, relating it to history and modern developments.  相似文献   
75.
This study brings together the research focused on science education through project-based learning (PBL). This learning project was carried out in a rural learning community and an attempt was made to adapt to the natural resources of the area by organizing educational outings, experimental activities, and encouraging the participation of families. The overall objective is to test the effectiveness of applying the PBL teaching methodology for learning science in a rural learning community. The methodology used has been qualitative, specifically, the participating research has been used and the information has been compiled in a field notebook. The results show that the didactic proposal had good results; showing that, in conclusion, science teaching today should be inclined toward more innovative educational methodologies such as PBL.  相似文献   
76.
This paper presents an application of the UTA method for building utility functions for the evaluation criteria defined by the Staff Evaluation Commission (CAD) of the Rio de Janeiro Federal University (UFRJ). Every year, the CAD-UFRJ gives the staff evaluation results for each Postgraduate Engineering Programme. However, the method used to generate the staff evaluation is assumed unknown. Trying to find the CAD-UFRJ preference structure, the evaluation results supplied by CAD-UFRJ are used to apply the UTA method. Some additional information obtained from the CAD-UFRJ data is incorporated in the optimal solutions analysis.  相似文献   
77.
78.
We compute constrained equilibria satisfying an optimality condition. Important examples include convex programming, saddle problems, noncooperative games, and variational inequalities. Under a monotonicity hypothesis we show that equilibrium solutions can be found via iterative convex minimization. In the main algorithm each stage of computation requires two proximal steps, possibly using Bregman functions. One step serves to predict the next point; the other helps to correct the new prediction. To enhance practical applicability we tolerate numerical errors. Research supported partly by the Norwegian Research Council, project: Quantec 111039/401.  相似文献   
79.
Noise is one of the most highly found physical contaminants in the construction sector. The most negative effects caused by noise exposure are related to the hearing system and may produce professional deafness or even permanent deafness. As these effects have a very important influence on people’s health and well-being, it is necessary to assess the noise exposure and to develop mechanisms for studying and proposing preventive solutions.This work has studied the noise levels which the workers of the construction sector are exposed to. A number of representative measurements have been carried out using a sound level meter and a dosimeter to collect data from workers devoted to different tasks in the construction process. Analysis of the most important levels and indexes have been done with those data, and afterwards, they have been compared with the limits imposed by the different current regulations.  相似文献   
80.
A peatland in Pinheiro, Diamantina City, Minas Gerais State - Brazil, was sampled at different depths of two profiles with diverse vegetation coverings (grassland field and bush) in order to collect materials that might reflect changes in the chemical states of iron over the peat formation coming from original minerals such as hematitic phyllite surrounding the boggy pedon. Samples collected were chemically, structurally and magnetically characterized. The results show that both series of peats are composed of organic matter and minerals such as quartz, kaolinite, gibbsite, rutile and muscovite. Deeper layers present only quartz. Mössbauer spectroscopy shows that iron is present in both electron states, Fe2+ and Fe3+, under both vegetations, each valence appearing in the spectra in the form of a discrete doublet. No hyperfine magnetic splitting was observed in any spectrum at room temperature. The Mössbauer subspectral area of Fe2+ tended to increase from the upper to deeper layers. Magnetic measurements reveal that the magnetic response of the surface samples is the highest, displaying a sharp decrease below 15 cm and that the magnetic signal is a superposition of (super)paramagnetic and ferrimagnetic contributions. Samples from the grassland field also show a diamagnetic component for the deeper layers.  相似文献   
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