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The synthesis of coumarins by hydroxyalkylation of phenols with ethyl acetoacetate (via Pechmann reaction) is attempted using magnetically separable and reusable CuFe2O4 nanoparticles in water.
[Supplementary materials are available for this article. Go to the publisher's online edition of Synthetic Communications ® for the following free supplemental resource(s): Full experimental and spectral details.] 相似文献
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Simeon Hubrich Meysam Joulaian Paolo Di Stolfo Andreas Schröder Alexander Düster 《PAMM》2016,16(1):201-202
The finite cell method is based on a fictitious domain approach, providing a simple and fast mesh generation of structures with complex geometries. However, this simplification leads to intersected cells where the standard Gauss quadrature does not perform well. To perform the numerical integration of these cells, we use the moment fitting approach that generates an individual quadrature rule for every broken cell. In this paper, we will perform a non-linear optimization approach to find the optimal position and number of the integration points. The findings show that the proposed method leads to efficient quadrature rules that require less integration points than other existing integration methods. (© 2016 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
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Robabeh Baharfar Seyed Meysam BaghbanianSeyed Mohammad Vahdat 《Tetrahedron letters》2011,52(45):6018-6020
The reactive 1:1 zwitterionic intermediate, formed by the addition of isocyanides to dialkyl acetylenedicarboxylates, was trapped by thiouracils to yield a ketenimine intermediate, which cyclized and then rearranged to afford pyrimido[2,1-b][1,3]thiazines in good yields. 相似文献
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Behnam Vahdani S. Meysam Mousavi Reza Tavakkoli-Moghaddam 《Applied Mathematical Modelling》2011,35(9):4257-4269
The aim of this paper is to present a novel fuzzy modified technique of order preference by a similarity to ideal solution (TOPSIS) method by a group of experts, which can select the best alternative by considering both conflicting quantitative and qualitative evaluation criteria in real-life applications. The proposed method satisfies the condition of being the closest to the fuzzy positive ideal solution and also being the farthest from the fuzzy negative ideal solution with multi-judges and multi-criteria. The performance rating values of alternatives versus conflicting criteria as well as the weights of criteria are described by linguistic variables and are transformed into triangular fuzzy numbers. Then a new collective index is introduced to discriminate among alternatives in the evaluation process with respect to subjective judgment and objective information. This paper shows that the proposed fuzzy modified TOPSIS method is a suitable decision making tool for the manufacturing decisions with two examples for the robot selection and rapid prototyping process selection. 相似文献
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Numerical Algorithms - This paper provides a numerical method for solving a class of Itô stochastic delay differential equations (SDDEs). The method’s novelty is its use of the spectral... 相似文献
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We present a novel numerical scheme for the valuation of options under a well‐known jump‐diffusion model. European option pricing for such a case satisfies a 1 + 2 partial integro‐differential equation (PIDE) including a double integral term, which is nonlocal. The proposed approach relies on nonuniform meshes with a focus on the discontinuous and degenerate areas of the model and applying quadratically convergent finite difference (FD) discretizations via the method of lines (MOL). A condition for observing the time stability of the fully discretized problem is given. Also, we report results of numerical experiments. 相似文献
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F. Soleymani D.K.R. Babajee Taher Lotfi 《Journal of the Egyptian Mathematical Society》2013,21(3):346-353
An optimal method is developed for approximating the multiple zeros of a nonlinear function, when the multiplicity is known. Analysis of convergence for the proposed technique is studied to reveal the fourth-order convergence. We further investigate the dynamics of such multiple zero finders by using basins of attraction and their corresponding fractals in the complex plane. A fourth-order method will also be presented, when the multiplicity m is not known. Numerical comparisons will be made to support the underlying theory of this paper. 相似文献
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Structural Chemistry - The [4+2] cycloaddition reaction of 1,3-dimethylindole and ortho-quinone methide (obtained from tautomerization of 2,6-dimethylquinone under basic conditions), experimentally... 相似文献
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In the present work, an innovative leach proof nanocatalyst based on dendritic fibrous nanosilica (DFNS) modified with ionic liquid loaded Fe3O4 NPs and CuI salts was designed and applied for the rapid synthesis of imidazo[1,2‐a]pyridines from the reaction of phenyl acetylene, 2‐aminopyridine, and aldehydes in aqueous medium. The structure of the synthesized nanocatalyst was studied by field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), Fourier transform infrared (FT‐IR), flame atomic absorption spectroscopy (FAAS), energy‐dispersive X‐ray (EDX), and X‐ray diffraction (XRD), vapor–liquid–solid (VLS), and adsorption/desorption analysis (Brunauer–Emmett–Teller [BET] equation) instrumental techniques. CuI/Fe3O4NPs@IL‐KCC‐1 with high surface area (225 m2 g?1) and porous structure not only exhibited excellent catalytic activity in aqueous media but also, with its good stability, simply recovered by an external magnet and recycled for eight cycles without significant loss in its intrinsic activity. Higher catalytic activity of CuI/Fe3O4NPs@IL‐KCC‐1 is due to exceptional dendritic fibrous structure of KCC‐1 and the ionic liquid groups that perform as strong anchors to the loaded magnetic nanoparticles (MNPs) and avoid leaching them from the pore of the nanocatalyst. Green reaction media, shorter reaction times, higher yields (71–97%), easy workup, and no need to use the chromatographic column are the advantages of the reported synthetic method. 相似文献