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31.
On‐line coupling of LC and ICP‐MS has been used for fractionation and detection of species of Cu, Fe, I, Se and Zn in human serum. It has been shown that anion exchange chromatography provided better separation capability (both intra‐ and inter‐element) than size‐exclusion chromatography. The mobile phases for ion exchange chromatography consisted of Tris–HNO3 buffer and ammonium salt (nitrate, acetate or formate). Formate was found to be the best mobile phase counter ion, enabling good chromatographic separation, and is acceptable for mass spectrometry too. The quantitative evaluation of element concentrations adhering to individual fractions was performed by the peak area normalization method. The repeatability of results ranged from 3 to 15% (depending on the element concentration level) and represented the main part of the result uncertainty. The accuracy of Cu and Zn fraction determinations was confirmed by comparison with the isotope dilution technique. Copyright © 2006 John Wiley & Sons, Ltd. 相似文献
32.
Received December 31, 2001 / Published online May 21, 2002 相似文献
33.
An approach to dealing with missing data, both during the design and normal operation of a neuro-fuzzy classifier is presented in this paper. Missing values are processed within a general fuzzy min–max neural network architecture utilising hyperbox fuzzy sets as input data cluster prototypes. An emphasis is put on ways of quantifying the uncertainty which missing data might have caused. This takes a form of classification procedure whose primary objective is the reduction of a number of viable alternatives rather than attempting to produce one winning class without supporting evidence. If required, the ways of selecting the most probable class among the viable alternatives found during the primary classification step, which are based on utilising the data frequency information, are also proposed. The reliability of the classification and the completeness of information is communicated by producing upper and lower classification membership values similar in essence to plausibility and belief measures to be found in the theory of evidence or possibility and necessity values to be found in the fuzzy sets theory. Similarities and differences between the proposed method and various fuzzy, neuro-fuzzy and probabilistic algorithms are also discussed. A number of simulation results for well-known data sets are provided in order to illustrate the properties and performance of the proposed approach. 相似文献
34.
The complete set of self-consistent parameters of nominally undoped LiNbO3 crystals of congruent composition that describe the electro-optic, piezoelectric, elasto-optic, elastic, and dielectric response
has been determined by numerically evaluating available measurements. The parameters were determined at room temperature and
consist of the low-frequency clamped dielectric constants εS
ij, elastic stiffness constants at constant electric field CE
ijkl, piezoelectric stress coefficients eijk, elasto-optic constants at constant electric field pE
ijkl, and clamped electro-optic coefficients rS
ijk. It is shown that the complete set is required for calculating the effective electro-optic coefficients and dielectric constants
in photorefractive applications of LiNbO3.
Received: 4 January 2002 / Revised version: 1 February 2002 / Published online: 14 March 2002 相似文献
35.
Summary The paper addresses the problem of the implementation of nonhomogeneous essential Dirichlet type boundary conditions in thep-version of the finite element method.Partially supported by the Office of Naval Research under Grant N-00014-85-K-0169Research partially supported by the Air Force Office of Scientific Research, Air Force Systems Command, USAF, under Grant Number AFOSR 85-0322 相似文献
36.
Recently published data on thep T dependence of the angular distributions of muon pairs produced in collisions of negative pions with deuterium and tungsten nuclei reveal an unexpected tendency. We show that the quantum statistical approach involving expansions in terms of coherent states leads in this case to an exact, non-perturbative result which in the lowest order approximation describes the observed trends with sufficient accuracy. In this procedure, the non-vanishing correlations between the coordinates and momenta of dimuons play a decisive role. 相似文献
37.
38.
J. Ježek 《Czechoslovak Mathematical Journal》2004,54(1):233-246
We investigate congruences in one-element extensions of algebras in the variety generated by tournaments. 相似文献
39.
J. Mlynár J. Ongena The EFDA JET Contributions I. Duran M. Hron R. Pánek V. Petržílka F. Žáček 《Czechoslovak Journal of Physics》2004,54(3):C28
JET (Joint European Torus) is the largest tokamak in the world and the only fusion facility able to operate with Tritium, the fusion fuel, and Beryllium, the ITER first wall material. JET also features the most complete remote handling equipment for invessel maintenance. As a multinational research center, JET provides logistic experience in preparing for operation of the global facility, tokamak ITER.Experiments on JET are focused on ITER-relevant studies, in particular on detailing the operational scenarios (EL My H-modes and advanced regimes), on enhancing the heating systems, on developing diagnostics for burning plasmas etc. Pioneering real-time control techniques have been implemented that maximize performance and minimize internal disturbances of JET plasmas. In helium plasmas, ion cyclotron heating (ICRH) created fast α-particles, mimicking their populations in future burning plasmas. The recent successful Trace Tritium campaign provided important new data on fuel transport. Current enhancements on JET include a new ITER-like ELM-resilient high power ICRH antenna (7 MW) and over twenty new diagnostics that will further extend the JET scientific capabilities and push the facility even closer to the ITER parameters.A special mention is given to the involvement of the fusion experts from Association EURATOM-IPP.CR, who have been actively participating in the collective use of JET facility for more than three years. 相似文献
40.
Bogdan Nita 《General Relativity and Gravitation》2003,35(10):1865-1868
Algebraically special gravitational fields are described using algebraic and differential invariants of the Weyl tensor. A type III invariant is also given and calculated for Robinson-Trautman spaces. 相似文献