In situ observation of NaBi(WO4)2 dendrite growth and the study on microstructure of solidification

The dendrite growth process of transparent NaBi(WO₄)₂ with small prandtl and high melting point was studied by using the in-situ observation system. According to the dynamic images and detailed information, there are two kinds of restriction effect on the dendrite growth, the competition between arms and branches and the convection in the melt. The dendrite growth rate was time dependent, and the rate of arm growth reached the maximum 5.8 mm/s in the diffusive-advective region and rapidly decreased in the diffusive-convective region. The growth rate of branch had the same change trends as the arm’s. Based on the EPMA-EDS data of solidification structure of quenched NaBi(WO₄)₂ melt, it was found that there were component differences from stoichiometric concentration in the melt near the interface during the growth process. Supported by the National Natural Science Foundation of China (Grant No. 50331040) and the Innovation Funds from Shanghai Institute of Ceramics, Chinese Academy of Sciences (Grant No. SCX0623)     

Features of the total disintegration events of heavyemulsion targets caused by 4.5A GeV/c16O

Total disintegration events produced by 4.5\,A GeV/c $^{16}$O--AgBr interactions are analysed to investigate the characteristics of secondary charged particles produced in such collisions. The multiplicity distributions of grey, black, and relativistic charged particles can be well represented by Gaussian distribution. The average multiplicity of grey particles is found to increase with the mass of projectile increasing, while that of black particles is found to decrease with the mass of projectile increasing. This result is in good agreement with the prediction of fireball model. Finally, the linear dependence between grey and black particles is observed, but there is no distinct dependence between the production of relativistic charged particles and the target excitation.     

1.54μmEr3+,Yb3+共掺玻璃激光器的速率方程及数值分析

LD抽运共掺Er,Yb玻璃激光器中的跃迁过程较复杂,针对双掺离子之间的能量传递和Er3+的多种跃迁过程,给出了详细的准三能级系统的速率方程,在合理简化后进行了数值分析,分析了Er3+掺杂浓度和介质长度、抽运光斑、输出镜透过率、谐振腔长、抽运光的椭圆度等因素对激光阈值及斜率效率的影响. 关键词： 1.54μm激光 Er3+玻璃 速率方程 数值分析     

Raman spectroscopic study of ceramic Sr2Bi4Ti5O18

Raman spectra of ceramic Sr2Bi4Ti5O18 （SBTi5） are reported to consist of four different Raman bands. Temperature-dependent spectra reveal the relationship between the lattice vibration and the material＇s structure. There appears a relatively large change in structure of the material at about 273K, The anharmonic potential of the material has a great influence on its phonon mode full width at half maximum （FWHM）, which can be expressed by a function of temperature. Theoretical fittings of the FWHMs for the two modes at around 312 cm^-1 and 464cm^-1 indicate that the latter phonon mode is more anharmonic than the former one.     

Remarks on the Scattering Result of Nonlinear Schr(o)dinger Equations

0 Introduction In this paper, we give another proof of the scattering result of the following Cauchy problem in the energy space     

A generalized existence theorem of BSDEs

In this Note, we deal with one-dimensional backward stochastic differential equations (BSDEs) where the coefficient is left-Lipschitz in y (may be discontinuous) and Lipschitz in z, but without explicit growth constraint. We prove, in this setting, an existence theorem for backward stochastic differential equations. To cite this article: G. Jia, C. R. Acad. Sci. Paris, Ser. I 342 (2006).     

流动注射化学发光抑制法测定尼群地平

基于尼群地平在碱性条件下对铁氰化钾鲁米诺化学发光体系有较强的抑制作用,联用流动注射技术建立了测定尼群地平的新方法.本法的线形范围为0.1～100.0 μg/mL,检出限0.02 μg/mL ,此法用于尼群地平片剂含量测量和药典法对照结果满意.     

改进型迈克耳孙干涉仪

采用分光梭镜代替迈克耳孙干涉仪中的分束镜和补偿板，不仅消除了杂散光斑，且简化了仪器的结构．     

Competitive influence of atactic polystyrene and supercritical carbon dioxide on the conformation of syndiotactic polystyrene

The crystallization behavior of miscible syndiotactic polystyrene (sPS) and atactic polystyrene (aPS) blends with different sPS/aPS weight ratios was investigated in supercritical CO₂ by using Fourier‐transform infrared spectroscopy, differential scanning calorimetry, and wide‐angle X‐ray diffraction. Supercritical CO₂ and aPS exhibited different effects on the conformational change of sPS and competed with each other. Increasing the content of amorphous aPS in the blends made its effect on the conformational change of sPS gradually surpass that of supercritical CO₂. Supercritical CO₂ favored the formation of the helical conformation of sPS in lower temperature range and the all trans planar conformation in higher temperature range, instead of forming the latter one only in higher temperature range in ambient atmosphere. However, increasing aPS content in the blends pushed the range for forming the helical conformation to lower temperature and made the all trans planar conformation dominant in aPS/sPS 25/75 blend after treating in supercritical CO₂ above 60 °C. The all trans planar zigzag conformation was more favorable than the helical conformation after mixing aPS in sPS in supercritical CO₂. © 2007 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 45: 1755–1764, 2007