负载金的纳米管钛酸光催化氧化一氧化碳

 用化学方法制备了负载金的纳米管钛酸(Au/H2Ti2O4(OH)2)光催化剂,并用TEM,XPS,XRD和DRS等技术对催化剂进行了表征. 结果表明,经573 K处理后,纳米管钛酸表面及管内均有零价的金颗粒存在. 与纳米管钛酸(H2Ti2O4(OH)2)相比,Au/H2Ti2O4(OH)2具有明显的CO光催化氧化活性,但在暗态时无活性. 经分析认为,暗态时Au与纳米管相互接触的周界处不活泼,故催化剂无CO催化氧化活性; 紫外光照射下,纳米管激发产生e--h+对,e-从纳米管转移到Au0上, 使纳米管和Au-在接触周界处产生相互作用,形成活性位,导致CO催化氧化反应发生.     

Approximate Noether-Type Symmetries and Conservation Laws via Partial Lagrangians for Nonlinear Wave Equation with Damping

In terms of our new exact definition of partial Lagrangian and approximate Euler-Lagrange-type equation, we investigate the nonlinear wave equation with damping via approximate Noether-type symmetry operators associated with partial Lagrangians and construct its approximate conservation laws in general form.     

Residual symmetry,interaction solutions,and conservation laws of the(2+1)-dimensional dispersive long-wave system

We explore the(2+1)-dimensional dispersive long-wave(DLW) system. From the standard truncated Painlev′e expansion, the B¨acklund transformation(BT) and residual symmetries of this system are derived. The introduction to an appropriate auxiliary dependent variable successfully localizes the residual symmetries to Lie point symmetries. In particular, it is verified that the(2+1)-dimensional DLW system is consistent Riccati expansion(CRE) solvable. If the special form of(CRE)-consistent tanh-function expansion(CTE) is taken, the soliton-cnoidal wave solutions and corresponding images can be explicitly given. Furthermore, the conservation laws of the DLW system are investigated with symmetries and Ibragimov theorem.     

二氧化钛纳米膜电极的形貌和光电化学性质

采用两种不同粒度的国产TiO2纳米材料和进口TiO2P25粉末,以涂覆法分别在导电玻璃基底上制备出TiO2纳米膜电极.通过循环伏安、瞬态光电流时间谱,结合SEM、DRS、XRD等实验手段,分析比较了三种TiO2膜电极的形貌和光电化学性质,探讨了提高和改善电极性能的途径.     

硫铁矿烧渣制备氧化铁黄和氧化铁红

对利用硫铁矿烧渣制备氧化铁黄和氧化铁红进行了研究。考察了影响硫铁矿烧渣还原、酸溶、中和、氧化等过程的各种因素。结果表明,在适宜的条件下,利用烧渣可以制备出用做颜料的氧化铁黄和氧化铁红。     

The derivative-dependent functional variable separation for the evolution equations

This paper studies variable separation of the evolution equations via the generalized conditional symmetry. To illustrate, we classify the extended nonlinear wave equation u_tt=Au,u_xu_xx+Bu,u_x,u_t which admits the derivative-dependent functional separable solutions DDFSSs). We also extend the concept of the DDFSS to cover other variable separation approaches.     

微乳液1-(2-吡啶偶氮)-2-萘酚分光光度法测定蔬菜样品中的钴

以十二烷基硫酸钠-溴代十六烷基三甲胺(SDS-CIMAB)复合微乳液为介质,对Co(Ⅱ)-1-(2-吡啶偶氮)-2-萘酚的显色反应条件进行了研究.结果表明该体系的λ_(max)=580nm,ε_(580)=3.4×10~4L·mol·cm~(-1),Co(Ⅱ)测定的线性范围为0～2.40mg/L.回收率在96%～103%之间,该法选择性好,用于蔬菜中Co(Ⅱ)含量的测定,得到了满意的结果.     

纳米CdS粒度控制的动力学效应

介绍了一种同阳离子共沉淀控制纳米CdS粒度的新方法.共沉淀的两种反应都是扩散控制，两者的反应速率存在很大差异，快速生成物CdS的纳米尺寸受到两种负离子的初始浓度比的控制.吸收光谱、X射线粉末晶体衍射谱、荧光光谱和X射线电子能谱的表征表明，共沉淀物是CdS和CdSt     

硫铁硫烧渣制备氧化铁黄和氧化铁红

对利用硫铁矿烧渣制备氧化铁黄和氧化铁红进行了研究。考察了影响硫铁矿烧渣还原、酸溶、中和、氧化等过程的各种因素。结果表明，在适宜的条件下，利用烧渣可以制备出用做颜料的氧化铁黄和氧化铁红。     

Preliminary Group Classification for One Class of Nonlinear Wave Equations

The group classification is carried out on the nonlinear wave equation utt = f（x,u, ux）uzz ＋ g（x,u,uz） by using the preliminary group classification approach. The generators of equivalence group are determined and the corresponding reduced forms are obtained. The result of the work is shown in table form.