基质分散固相萃取-高效液相色谱-串联质谱法测定鱼肉中吡喹酮和克螨特

鱼肉样品（2.0g）按基质固相分散萃取法与10mL乙腈以6 000r.min-1转速匀浆1min,随即与4g无水硫酸镁和1.5g氯化钠混合,并以5 000r.min-1转速离心3min,移取上清液1mL,与N-丙基乙二胺和C18粉末各50mg混匀,以10 000r.min-1转速离心3min。取上清液0.5mL与0.5...     

A calibration method for optical trap force by use of electrokinetic phenomena

An experimental method for calibration of optical trap force upon cells by use of electrokinetic phenomena is demonstrated. An electronkinetic sample chamber system (ESCS) is designed instead of a common sample chamber and a costly automatism stage, thus the experimental setup is simpler and cheaper. Experiments indicate that the range of the trap force measured by this method is piconewton and sub-piconewton, which makes it fit for study on non-damage interaction between light and biological particles with optical tweezers especially. Since this method is relevant to particle electric charge, by applying an alternating electric field, the new method may overcome the problem of correcting drag force and allow us to measure simultaneously optical trap stiffness and particle electric charge.     

Ba-La-Cu-O体系的金属-半导体转变和超导电性

测量了名义组分为 BaxLa_(5-x)Cu_5O_(5(3-y))(x=0,0.25,0.5,1.0,1.25,1.5; y>0)的系列样品电阻-温度关系。发现:对x=0的二元氧化物,其电子输运呈典型的半导体特征;随着Ba的掺入以及含Ba量的增加,系统经历了半导体-半金属-金属(超导体)转变,并且其超导临界温度Tc也单调地升高。根据Mattheiss及Freeman等人的能带计算结果,在电声子强耦合的框架里对上述现象作了定性的解释。本文作者认为:二价Ba的掺入抑制了晶格的不稳定性,稳定了超导相。     

晶型碳酸稀土的形成及其影响因素

用碳酸氢铵沉淀法从风化淋积型稀土矿硫酸铵渗浸液中回收稀土、得到了晶型碳酸稀土。研究了时间、温度、浓度等各种影响因素,对晶型碳酸稀土进行了化学分析以及X射线衍射、扫描电镜、红外光谱、差热、热量分析,取得了较为理想的结果。     

混沌群作用

§ 1　ＩｎｔｒｏｄｕｃｔｉｏｎＴｈｉｓｐａｐｅｒｉｓｔｈｅｓｅｑｕｅｌｔｏ[1 ,2 ].Ｃａｉｒｎｓｅｔａｌ.[1] ｉｎｔｒｏｄｕｃｅｄｔｈｅｎｏｔｉｏｎｏｆａｃｈａｏｔｉｃｇｒｏｕｐａｃｔｉｏｎａｓａｇｅｎｅｒａｌｉｚａｔｉｏｎｏｆｃｈａｏｔｉｃｄｙｎａｍｉｃａｌｓｙｓｔｅｍｓ(ｓｅｅｄｅｆｉｎｉｔｉｏｎｂｅｌｏｗ) .Ｔｈｅｙｓｈｏｗｅｄｔｈａｔｔｈｅｃｉｒｃｌｅｄｏｅｓｎｏｔａｄｍｉｔａｃｈａｏｔｉｃａｃｔｉｏｎｏｆａｎｙｇｒｏｕｐ ,ａｎｄｃｏｎｓｔｒｕｃｔｅｄａｃｈａｏｔｉｃａｃｔｉｏｎｏｆＧ =Ｚ×…     

高能碰撞多粒子产生的分形结构的Monte Carlo研究

高能碰撞多粒子产生的末态粒子系统的涨落,有可能成为研究多粒子动力学的突破口.如何消去系统的统计涨落是其中最重要的课题.本文采用一个简单模型,通过Monte Carlo模拟,研究了统计涨落对分形结构的影响,找到一种定性地消去系统的统计涨落的方法.     

裂变统计理论存在的问题

一、引言 现有的裂变统计理论作了如下的假定:裂变过程是准静态的,因此不同裂变方式的相对几率决定于过程的最后阶段,正比于断裂一瞬间碎片量子态密度的乘积。经过计算之后,裂变断裂道的数目 N(A_L,A_H)∝e~(2~(aE))~1/2 (1)也就是说,不同方式的裂变几率主要决定于二碎片的能级密度参数之和a=a_L十a_H,及内部激发能之和E=E_L+E_H。足码L,H分别表示轻、重碎片,A为质量数。     

Large payload quantum steganography based on cavity quantum electrodynamics

A large payload quantum steganography protocol based on cavity quantum electrodynamics (QED) is presented in this paper, which effectively uses the evolutionary law of atoms in cavity QED. The protocol builds up a hidden channel to transmit secret messages using entanglement swapping between one GHZ state and one Bell state in cavity QED together with the Hadamard operation. The quantum steganography protocol is insensitive to cavity decay and the thermal field. The capacity, imperceptibility and security against eavesdropping are analyzed in detail in the protocol. It turns out that the protocol not only has good imperceptibility but also possesses good security against eavesdropping. In addition, its capacity for a hidden channel achieves five bits, larger than most of the previous quantum steganography protocols.     

双功能镧系化合物:合成、结构、磁性和荧光性质

利用N-succinopyridine（HL）配体,成功合成了2个同构型镧系化合物[Ln（HL）₂（H₂O）₄]Cl₃（Ln=Pr（1）,Eu（2））并对其进行了结构表征。1和2均由羧酸配体双桥联金属离子形成1D链结构,再通过氢键进一步相互连接构成了3D超分子结构。变温磁化率测试表明1中Pr（Ⅲ）离子之间存在反铁磁相互作用,而在2中,Eu（Ⅲ）离子之间则表现出弱铁磁相互作用。固态发光测试观察到2可以发出很强的红光,但由于Pr（Ⅲ）离子的能隙较大,未观察到1的特征峰。