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扇贝脂肪的提取和分析 总被引:5,自引:2,他引:3
以快速脂肪提取法取代素氏提取法,提取扇贝脂肪仅需45min,提取率98.8%。利用40m×0.35mmi.d.PEG-20M玻璃毛细管柱分离测定扇贝脂肪中脂肪酸。分离出46个峰,结合气相色谱/质谱(GC/MS),鉴定出36个峰,占脂肪区总量的99.4%,其中饱和脂肪酸占32%,不饱和脂肪酸占67.4%。 相似文献
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毛细管气相色谱法分析虾蛄肉中的脂肪酸 总被引:2,自引:0,他引:2
以快速脂肪提取器分别提取雄、雌虾蛄肉中脂肪,利用50m×0.35mmi.d.PEG-20M玻璃毛细管柱分离测定了雄、雌虾蛄肉中的脂肪酸,结合气相色谱/质谱法,鉴定出45个峰,分别占脂肪酸总量的99.2%和98.0%,其中不饱和脂肪酸分别为74.7%和71.5%。 相似文献
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银杏叶中脂肪酸的GC-MS分析研究 总被引:3,自引:0,他引:3
银杏叶用石油醚提取,经皂化、酯交换法处理,用GC-MS对其脂肪酸化学成分进行了分析和鉴定。经DB-1柱分离出39个峰,鉴定了其中的34种化合物,占总含量的94.37%。其中饱和脂肪酸占31.64%;不饱和脂肪酸占34.23%;烷基酚占14.07%;其它部分占14.43%。 相似文献
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人工养殖对虾与野生对虾脂肪酸的组成分析和测定 总被引:8,自引:0,他引:8
用脂肪快速提取器对人工养殖对虾与野生对虾脂进行了提取和测定。脂肪甲酯化后,采用60m*0.32mmi.d.交联PEG-20M石英毛细管柱,FID检测器,对脂肪酸进行了分析。 相似文献
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稠李果、茎、叶、皮及树干挥发油化学成分的分析 总被引:10,自引:0,他引:10
采用气相色谱.质谱联用技术,对稠李果、茎、叶、皮及树干挥发油进行了成分分析。首次从稠李果、茎、叶、皮及树干分别鉴定出了29、31、35、29和21种化合物,已鉴定挥发油成分占总挥发油含量分别为98.14%、96.96%、94.34%、99.16%及96.73%。5个部位中挥发油化学组成各有异同,但其主要成分均是苯甲酸和苯甲醛。皮中苯甲酸相对含量高达64.43%,因苯甲酸具有防腐作用,故认为稠李木材是天然的防腐木材。本研究结果为稠李的综合开发利用提供理论依据。 相似文献
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顶空气相色谱法测定香水中的甲醇 总被引:20,自引:0,他引:20
In this paper. headspace GC was used to determine methanol in perfume. Separation was performed on a GDX-201 column. 2m×3mm i.d. at 150℃. The characteristics of this method are sensitive. accurate and with less interference. This new method can be used for determination of methanol in cosmetics. 相似文献
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气相-质谱法测定孜然芹挥发油的化学成分 总被引:13,自引:0,他引:13
采用水蒸气蒸馏法从孜然芹中提取挥发性成分,并用气相 质谱法(GC MS)联机分析,共分离出60余峰,鉴定出了49种物质,用面积归一法确定了相对含量。在所分离出的化合物中,碳氢化合物16种,烃类含氧衍生物32种。主要成分为枯茗醛和藏花醛,它们分别占测得组分的32 26%和26 49%。另有9种含量在1%以上的物质,主要是萜类中的单萜、倍半萜和芳香族醛、酮醚类物质。低含量组分主要为萜烯类的醇、醛、酮、酯和部分芳香族化合物。在气相分析中,选择了合适的条件,采用中等极性的DB 210柱,对孜然芹挥发油中的中等极性和非极性成分有较好的分离效果。 相似文献
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本文研究了一种结核分枝杆菌细胞单糖的毛细管气相色谱分析方法。测定了11种(株)标准分枝杆菌,2株人工培养耐药株及11株临床分枝杆菌菌株的细胞单糖成分。实验结果表明,分枝杆菌细胞单糖的分析,不仅可以对分枝杆菌进行鉴定,而且可以提供与分枝杆菌的毒力和耐药性有关的特征色谱峰。 相似文献
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Ridha El Mokni Siwar Majdoub Ikbal Chaieb Ibrahim Jlassi Rajesh K. Joshi Saoussen Hammami 《Biomedical chromatography : BMC》2019,33(10)
The present study was conducted to investigate for the first time the chemical composition and insecticidal and antimicrobial properties of Phlomis floccosa D. Don. essential oil isolated by hydro‐distillation of its aerial parts. Qualitative and quantitative analyses of the essential oil on the basis of gas chromatography and mass spectrometry (GC/FID and GC/MS) revealed the presence of 59 organic volatiles representing 86.9% of the total constituents. The major compounds were germacrene‐D (19.7%) followed by β‐caryophyllene (15.5%), caryophyllene oxide (8.3%), hexadecenoic acid (7.9%) and carvacrol (6.1%). The broth microdilution method was conducted to test the antimicrobial activity of the essential oil against five pathogens: Escherichia coli, Pseudomonas aeruginosa, Salmonella enterica, Staphylococcus aureus, Bacillus subtilis and the yeast Candida albicans. The oil of P. floccosa D. Don. shows promising activity against the Gram‐positive bacteria S. aureus and B. subtilis and the yeast C. albicans (minimum inhibitory concentration = 625 μg.mL?1). The effectiveness of the essential oil was assessed on both Tribolium confusum and Sitophilus zeamais pest insects and it was more pronounced against T. confusum, showing a moderate mortality of 47.5%. 相似文献
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Characteristics of Carbon Isotopes of Alkane Components and Identification Marks of Biogenic Gases in China 总被引:3,自引:0,他引:3
The carbon isotope composition of alkane component in biogenic gases of China has the following characteristics:with the increase of carbon number of the alkane molecules in biogenic gases, (i) the distribution range of the δ13C values and their main frequency sections become narrower, and both the heaviest and the lightest δ13C boundary values shift to their heavier end; (ii) the δ13C values of ethane and propane in biogenic gases present a positive linear relationship and (iii) the values of δ13C1, δ13C2 and δ13C3 tend to become heavier with the increase of heavy alkane component (C2+3) in biogenic gases. The authors studied the relationship between the δ13C values and the amount of heavy alkane components in biogenic gases (δ13C1 -C2+3(%). δ13C2 -C2+3(%) ,δ13C3-C2+3(%) for the first time and set up the interrelated regression equations between δ13C and C2+3 content (C2+3%), and advance that δ13C1< -55‰ and C2+3<0. 5% are two fine marks for identification of biogenic gases of China. δ13C 相似文献
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珠兰花香味成份的分离和鉴定 总被引:1,自引:0,他引:1
用石油醚回流蒸馏法抽取新鲜珠兰花的挥发性香味成份,经旋转蒸发器浓缩,通过气相色谱质谱联用仪鉴定出60余种组份,包括脂肪烃,芳香烃,醚,醇,醛酮,羧酸和脂等,主要组分是4-羟基-β-紫罗酮(20%)表茉莉酮酸甲脂(6%)和茉莉酮酸甲脂(4%)。 相似文献