Experimental investigation into three-dimensional wavy liquid films under the influence of electrostatic forces

Three-dimensional interfacial waves that develop on the free surface of falling liquid films are known to intensify heat and mass transfer. In this context, the present paper studies the effect of electrostatic forces applied to a falling film of dielectric liquid on its three-dimensional nonlinear wave dynamics. Therefore, measurements of the local film thickness using a confocal chromatic imaging method were taken, and the complex wave topology was characterized through photography. The experiments show a complex interaction between the electric field and the hydrodynamics of the falling film, whereby electrostatic forces were found to both increase and decrease wave peak height in different regions of the wave. Additionally, an electrically induced breakup of the three-dimensional wave fronts, which leads to a locally doubled frequency in streamwise direction, is found. The ability to influence the wave topology demonstrated here opens the possibility to optimize heat transfer processes in falling liquid films.     

Investigations of the Marangoni effect on the regular structures in heated wavy liquid films

Formation and development of quasi-regular metastable structures within laminar-wavy falling films were studied. These structures emerge within the residual layer between large waves and could be one reason for the break up of the falling film. The temperature field of the film surface was visualised using IR-thermography. The film thickness was obtained from point measurements with the chromatic confocal imaging method and converted into a film thickness field, based on a quasi-steady assumption and IR thermography images. The thermo-capillary nature (Marangoni effect) of the regular structures was proven experimentally.     

Liquid film characterization in horizontal,annular, two-phase,gas–liquid flow using time-resolved laser-induced fluorescence

A non-intrusive optical technique was developed to provide time-resolved longitudinal and cross-sectional images of the liquid film in horizontal annular pipe flow of air and water, revealing the interfacial wave behavior. Quantitative information on the liquid film dynamics was extracted from the time-resolved images. The planar laser-induced fluorescence technique was utilized to allow for optical separation of the light emitted by the film from that scattered by the air–water interface. The visualization test section was fabricated from a tube presenting nearly the same refractive index as water, which allowed the visualization of the liquid film at regions very close to the pipe wall. Longitudinal images of the liquid film were captured using a high-frame-rate digital video camera synchronized with a high-repetition-rate laser. An image processing algorithm was developed to automatically detect the position of the air–water interface in each image frame. The thickness of the liquid film was measured at two axial stations in each processed image frame, providing time history records of the film thickness at two different positions. Wave frequency information was obtained by analyzing the time-dependent signals of film thickness for each of the two axial positions recorded. Wave velocities were measured by cross-correlating the amplitude signals from the two axial positions. For the film cross-section observations, two high-speed digital video cameras were used in a stereoscopic arrangement. Comparisons with results from different techniques available in literature indicate that the technique developed presents equivalent accuracy in measuring the liquid film properties. Time-resolved images of longitudinal and cross-section views of the film were recorded, which constitute valuable information provided by the technique implemented.     

Measurement of liquid film thickness using a laser light absorption method

A photometric technique for film thickness measurements is described in this paper. It is based on the absorption of light passing through a layer of dyed liquid and takes advantage of small sized diode laser sources and sensitive light sensors. The method is non-intrusive, easy to use and to calibrate and can be implemented at relatively low cost. Laboratory tests of the technique have yielded satisfactory accuracy and repeatability. Moreover, the technique allows measurements with a good spatial resolution. Flowing film thickness measurements made photometrically are compared directly to measurements taken simultaneously with a “parallel wire conductance probe”. Time-averaged film heights, RMS values and other statistical information have been obtained by analyzing these instantaneous film thickness records. With regard to the time-averaged values of liquid film thickness, there is a satisfactory agreement between the two measuring techniques. Received: 11 February 1999/Accepted: 30 May 1999     

Measurement of water falling film thickness to flat plate using confocal chromatic sensoring technique

An experimental investigation of wavy water film falling down a flat plate has been carried out using confocal chromatic sensoring technique to determine the instantaneous and statistical characteristics of the film. The experiments involved three parameters: liquid feed mode, Reynolds number and plate inclination angle. The present time–average film thickness data is compared with the previous experimental and theoretical results showing a good agreement. A new correlation for the average film thickness is suggested. Our results show that the liquid feed mode has a vital influence on the film thickness and that the film thickness increases with Reynolds number and decreased plate inclination angle. The root–mean–square value of the film thickness fluctuations depends non-monotonically on the film Reynolds number. The corresponding mechanisms are analyzed.     

PIV measurements of flow in drying polymer solutions during solvent casting

An experimental method based on confocal microscopy and particle image velocimetry (PIV) is used to characterize the flow in a polymer solution during solvent casting. The flow inside a 200-μm-thick film of a poly(vinyl alcohol) (PVA) solution is visualized near a vertical wall of a mold using confocal microscopy of seed particles during solvent evaporation at 25, 35, and 45°C, and the corresponding velocity vector fields are determined from projections of the confocal images. Flow toward the vertical wall is observed inside the film as well as a slower Marangoni-type counter flow at the film surface during the initial phase of solvent evaporation, resulting from a polymer concentration gradient along the film due to a local variation in evaporation rate. Total volume of the polymer solution in the observation volume as well as solvent evaporation rate are determined as a function of time, both revealing close correlation to average horizontal velocity data from PIV. The PIV measurements show significant differences in the flow velocity fields at different temperatures. The PIV measurements correlate with the solvent evaporation rates as well as the final polymer thicknesses on the vertical wall of the mold. Surface tension and viscosity measurements are taken for different concentrations of PVA solution.     

The accuracy of tomographic particle image velocimetry for measurements of a turbulent boundary layer

To investigate the accuracy of tomographic particle image velocimetry (Tomo-PIV) for turbulent boundary layer measurements, a series of synthetic image-based simulations and practical experiments are performed on a high Reynolds number turbulent boundary layer at Re_θ = 7,800. Two different approaches to Tomo-PIV are examined using a full-volume slab measurement and a thin-volume “fat” light sheet approach. Tomographic reconstruction is performed using both the standard MART technique and the more efficient MLOS-SMART approach, showing a 10-time increase in processing speed. Random and bias errors are quantified under the influence of the near-wall velocity gradient, reconstruction method, ghost particles, seeding density and volume thickness, using synthetic images. Experimental Tomo-PIV results are compared with hot-wire measurements and errors are examined in terms of the measured mean and fluctuating profiles, probability density functions of the fluctuations, distributions of fluctuating divergence through the volume and velocity power spectra. Velocity gradients have a large effect on errors near the wall and also increase the errors associated with ghost particles, which convect at mean velocities through the volume thickness. Tomo-PIV provides accurate experimental measurements at low wave numbers; however, reconstruction introduces high noise levels that reduces the effective spatial resolution. A thinner volume is shown to provide a higher measurement accuracy at the expense of the measurement domain, albeit still at a lower effective spatial resolution than planar and Stereo-PIV.     

Spall Characterization in Epoxy Via Laser Spallation

Background: The strength of materials under extreme dynamic loading conditions, such as in the case of shock wave loading, is assessed from their spallation characteristics. Under laboratory conditions, flyer plate impact, or sometimes laser-induced stress waves, is employed to instigate spall in a material. These methods are often combined with velocity interferometer system for any reflector (VISAR) technique for performing transient measurements. Although the VISAR can record the velocity of extremely fast-moving surfaces, it requires a complex optical setup and a specialized data reduction technique. Objective: In this study, a simpler approach is adopted by extending laser spallation method to determine the spall strength of epoxy, while performing in situ interferometric measurements, directly on top of thick epoxy films. Methods: The glass/epoxy test samples are prepared by transferring an aluminum coating on top of epoxy layers with different thicknesses. Laser-induced stress waves transmit across the substrate/film interface and induce subsurface failure in the epoxy at sufficiently high incident laser energy. The nature and magnitude of the waves are deciphered from the out-of-plane displacement histories of the top reflective sample surfaces, which are recorded by using a Michelson interferometer. Results: The interferometric data reveal the development of two (temporally) well-separated stress waves: an ablation-induced high-amplitude short-duration longitudinal pulse, which is referred to as the primary wave, and a secondary wave, which travels at a comparatively slower speed. The complex constructive interaction of the two waves develops a high-magnitude tensile stress region in the epoxy layer. The spall strength is quantified by superimposing the two stress wave histories associated with the critical energy fluence. Conclusions: The spall depths predicted from spatiotemporal wave travel analyses are in excellent agreement with the experimental observations. The newly adopted methodology estimates the spall strength of epoxy as 260?±?20 MPa.

     

Application of PIV to velocity measurements in a liquid film flowing down an inclined cylinder

PIV technique is applied for measurements of instant velocity distributions in a liquid film flowing down an inclined tube in the form of a wavy rivulet. An application of special optical calibration is applied to correct distortion effects caused by the curvature of the interface. A vortex flow of liquid is observed inside a wave hump in the reference system moving with wave phase velocity. Conditionally averaged profiles of longitudinal and transverse components of liquid velocity are obtained for different cross-sections of developed non-linear waves. It is shown that the increase in wave amplitude slightly changes the location of the vortex center. The analysis of modification of vortex motion character due to wavy flow conditions, such as tube inclination angle, film Reynolds number, wave excitation frequency, is fulfilled.     

Evaporation of pure liquids with increased viscosity in a falling film evaporator

The present study investigated fluid dynamics and heat transfer of viscous pure liquids in a falling film evaporator. This is of special benefit as it avoids mass transfer effects on the evaporation behaviour. Experiments at a single-tube glass falling film evaporator were conducted. It allowed a full-length optical film observation with a high-speed camera. Additionally the evaporator was equipped with a slotted weir distribution device. Test fluids provided viscosities ranging from μ = 0.3 to 41 mPa s. The Reynolds number was between 0.7 and 1,930. Surface evaporation and the transition to nucleate boiling were studied to gain information about the film stability at maximum wall superheat. A reliable database for laminar and laminar-wavy viscous single component films was created. The experimental results show a significant enhancement in the wave development due to the film distribution. A wavy flow with different wave velocities was superposed to the film in each liquid load configuration without causing a film breakdown or dry spots on the evaporator tube. It was found that nucleate boiling can be allowed without causing film instabilities over a significant range of wall superheat.     

Measurement of laser driven shock wave transit time through thin aluminium targets by optical shadowgraphy

Laser driven shock wave transit time in thin aluminium targets was experimentally estimated by determining the shock emergence time at the rear of thin aluminium foils of varying thickness from 5 to 35 μm. A 20 J, 5 ns Nd:glass laser was focused to produce laser intensity of 10¹² to 5 × 10¹³ W/cm² on the targets which were placed in vacuum. Target foil movement was measured to an accuracy of 10 μm using optical shadowgraphy technique. This technique was used to accurately measure the shock transit time by recording the optical shadowgrams at various instants of time and thus identify the instant at which the foil is just set into motion. Shock transit time measured in foils of different thickness can give the value of shock velocity at a given laser intensity. Target motion recorded by shadowgraphy can also give the target foil velocity from which shock pressure can be estimated. Experimental values of shock transit time, shock velocity and shock pressure were observed to agree well with the values using one-dimensional multi-group radiation hydrodynamic simulations. PACS 52.50Jm; 52.50Lp; 52.25 Communicated by K. Takayama     

μ-PIV measurements of the ensemble flow fields surrounding a migrating semi-infinite bubble

Microscale particle image velocimetry measurements of ensemble flow fields surrounding a steadily migrating semi-infinite bubble through the novel adaptation of a computer controlled linear motor flow control system. The system was programmed to generate a square wave velocity input in order to produce accurate constant bubble propagation repeatedly and effectively through a fused glass capillary tube. We present a novel technique for re-positioning of the coordinate axis to the bubble tip frame of reference in each instantaneous field through the analysis of the sudden change of standard deviation of centerline velocity profiles across the bubble interface. Ensemble averages were then computed in this bubble tip frame of reference. Combined fluid systems of water/air, glycerol/air, and glycerol/Si-oil were used to investigate flows comparable to computational simulations described in Smith and Gaver III (J Fluid Mech 601:1–23, 2008) and to past experimental observations of interfacial shape. Fluorescent particle images were also analyzed to measure the residual film thickness trailing behind the bubble. The flow fields and film thickness agree very well with the computational simulations as well as existing experimental and analytical results. Particle accumulation and migration associated with the flow patterns near the bubble tip after long experimental durations are discussed as potential sources of error in the experimental method.     

Experimental characterization of thin films,droplets and rivulets using LED fluorescence

Imaging based on fluorescence has been used in the past to investigate, mostly in a qualitative manner, liquid films occurring in various applications. In the present paper, a simple quantitative experimental setup and the associated calibration procedure are detailed for a configuration involving Rhodamin B or Rhodamin 101 excited with light-emitting diodes (LEDs). The measurement procedure has been first validated for an open-channel flow considering different Reynolds numbers around 550 and has then been applied to the characterization of thin films, isolated droplets and rivulets. Using this technique the film thickness, film velocity and contact angle have been evaluated accurately for a variety of flow conditions.     

Algebraic turbulence modeling in adiabatic gas–liquid annular two-phase flow

The study considers algebraic turbulence modeling in adiabatic gas–liquid annular two-phase flow. After reviewing the existing literature, two new algebraic turbulence models are proposed for both the liquid film and the droplet laden gas core of annular two-phase flow. Both turbulence models are calibrated with experimental data taken from the open literature and their performance critically assessed. Although the proposed turbulence models reproduce the key parameters of annular flow well (average liquid film thickness and pressure gradient) and the predicted velocity profiles for the core flow compare favorably with available core flow velocity measurements, a more accurate experimental database is required to further improve the models accuracy and range of applicability.     

An experimental study of the liquid film on a vertical wire under the action of an impinging annular jet

The liquid film remaining on a wire withdrawn from a liquid bath and forced through an annular jet is experimentally investigated on a dedicated facility. An optical laser-based technique recently introduced to study liquid-film instabilities on small-radius cylinders allows the measurement of the mean final thickness and wave characteristics. Experimental results are compared to analytical predictions obtained with a simple model specifically derived for this configuration and based on liquid-film properties (density, viscosity and surface tension) and operating parameters (wire speed, nozzle dimensions and stagnation pressure). Such a model relies on the knowledge of pressure-gradient and wall shear-stress distributions generated by the annular jet radially impinging on the cylinder. Different correlations providing the maxima of these profiles are employed and, after some improvements to the original “knife” model, the mean final thickness is correctly predicted. Successful results are obtained, also, using a simple expression derived from the LLD theory. The experimental measurement of surface-perturbation features (wave amplitude, wavelength and amplification factor) as a function of the operating parameters leads to some important conclusions that could have a remarkable and direct influence on the industrial process of wire coating.     

Simultaneous planar measurement of droplet velocity and size with gas phase velocities in a spray by combined ILIDS and PIV techniques

A new approach for simultaneous planar measurement of droplet velocity and size with gas phase velocities is reported, which combines the out-of-focus imaging technique ‘Interferometric Laser Imaging Droplet Sizing’ (ILIDS) for planar simultaneous droplet size and velocity measurements with the in-focus technique ‘Particle Image Velocimetry’ (PIV) for gas velocity measurements in the vicinity of individual droplets. Discrimination between the gas phase seeding and the droplets is achieved in the PIV images by removing the glare points of focused droplet images, using the droplet position obtained through ILIDS processing. Combination of the two optical arrangements can result in a discrepancy in the location of the centre of a droplet, when imaging through ILIDS and PIV techniques, of up to about 1 mm, which may lead to erroneous identification of the glare points from droplets on the PIV images. The magnitude of the discrepancy is a function of position of the droplet’s image on the CCD array and the degree of defocus, but almost independent of droplet size. Specifically, it varies approximately linearly across the image along the direction corresponding to the direction of propagation of the laser sheet for a given defocus setting in ILIDS. The experimental finding is supported by a theoretical analysis, which was based on geometrical optics for a simple optical configuration that replicates the essential features of the optical system. The discrepancy in the location was measured using a monodisperse droplet generator, and this was subtracted from the droplet centres identified in the ILIDS images of a polydisperse spray without ‘seeding’ particles. This reduced the discrepancy between PIV and ILIDS droplet centres from about 1 mm to about 0.1 mm and hence increased the probability of finding the corresponding fringe patterns on the ILIDS image and glare points on the PIV image. In conclusion, it is shown that the proposed combined method can discriminate between droplets and ‘seeding’ particles and is capable of two-phase measurements in polydisperse sprays.     

Experimental study of the falling film of liquid around a Taylor bubble

The present work reports an experimental study of the falling liquid film around single Taylor bubbles rising in vertical tubes filled with stagnant liquids by using a pulse-echo ultrasonic technique. The experiments were carried out in acrylic tubes 2.0  m long, with inner diameters of 0.019, 0.024 and 0.034  m, with five water-glycerin mixtures, corresponding to inverse viscosity number ranging from 15 to 22422. The rising bubble and the falling liquid film were measured by using ultrasonic transducers located at the one side of the tube. The velocity and profile of the Taylor bubble, and the development length and equilibrium thickness of the falling liquid film around the bubble were obtained by the ultrasonic signals processing. Based on the experimental results of the present study, several correlations available to estimate the equilibrium thicknesses of liquid films falling around Taylor bubbles were evaluated and new correlations were proposed to estimate the dimensionless equilibrium film thickness and the film development length respectively.     

Experimental study on surface wave and film breakdown of falling liquid film flow

In order to evaluate characteristics of the liquid film flow and their influences on heat and mass transfer, measurements of the instantaneous film thickness using a capacitance method and observation of film breakdown are performed. Experimental results are reported in the paper. Experiments are carried out at Re = 250–10000, T _in = 20–50°C and three axial positions of vertically falling liquid films for film thickness measurements. Instantaneous surface waveshapes are given by the interpretation of the test data using the cubic spline method. The correlation of the mean film thickness versus the film Reynolds number is also given by fitting the test data. It is revealed that the surface wave has nonlinear behavior. Observation of film breakdown is performed at Re = 1.40 × 10³–1.75 × 10⁴ and T _in = 85–95°C. From experimental results, the correlation of the film breakdown criterion can be obtained as follows: Bd = 1.567 × 10⁻⁶ Re ^1.183     

Experiments on the flow of a thin liquid film over a horizontal stationary and rotating disk surface

Experiments on characterization of thin liquid films flowing over stationary and rotating disk surfaces are described. The thin liquid film was created by introducing deionized water from a flow collar at the center of an aluminum disk with a known initial film thickness and uniform radial velocity. Radial film thickness distribution was measured using a non-intrusive laser light interface reflection technique that enabled the measurement of the instantaneous film thickness over a finite segment of the disk. Experiments were performed for a range of flow rates between 3.0 lpm and 15.0 lpm, corresponding to Reynolds numbers based on the liquid inlet gap height and velocity between 238 and 1,188. The angular speed of the disk was varied from 0 rpm to 300 rpm. When the disk was stationary, a circular hydraulic jump was present in the liquid film. The liquid-film thickness in the subcritical region (downstream of the hydraulic jump) was an order of magnitude greater than that in the supercritical region (upstream of the hydraulic jump) which was of the order of 0.3 mm. As the Reynolds number increased, the hydraulic jump migrated toward the edge of the disk. In the case of rotation, the liquid-film thickness exhibited a maximum on the disk surface. The liquid-film inertia and friction influenced the inner region where the film thickness progressively increased. The outer region where the film thickness decreased was primarily affected by the centrifugal forces. A flow visualization study of the thin film was also performed to determine the characteristics of the waves on the free surface. At high rotational speeds, spiral waves were observed on the liquid film. It was also determined that the angle of the waves which form on the liquid surface was a function of the ratio of local radial to tangential velocity.