影响纳米压入测试结果的因素

纳米硬度计 ,又称深度测量压入仪。该仪器在刚性压针上施加特定载荷 ,同时记录压入试样深度。此技术广泛应用于微纳米尺度力学性能的研究。以MTSNanoIndenter○RXP为测试手段 ,参考试样熔融硅为研究对象 ,进行了不同压入深度的测试。结果显示 ,硬度和模量有随压入深度减小而增大的趋势。分析了接触零点的确定、压针尖端缺陷、试样表面的吸湿和粗糙度、弹塑性转变等因素对测试结果的影响。在压入深度为微米和亚微米量级时 ,上述因素对测试结果无显著影响 ;而在纳米量级时 ,有显著影响。所以 ,当压入深度为几十纳米时 ,纳米压入测试结果的可靠性值得注意     

基于应变率阶跃测试的晶体铜压入应变率敏感性研究

纳米压入测试可以原位获取材料的诸多力学性能,包括弹性模量,硬度,屈服应力,应变率敏感指数等。本文利用应变率阶跃测试技术对多晶铜试样的应变率敏感性进行测试分析,硬度-位移曲线表明压头下方所存在的变形梯度对各阶跃应变率下的硬度值存在明显影响;采用基于晶体细观机制的塑性应变梯度理论对压入变形梯度效应予以修正,比较了修正与未修正数据所得的应变率敏感指数,在有效剔除压入变形梯度影响的基础上,应变率阶跃测试可实现单次压入下材料应变率敏感性的测试表征。     

基于微纳米压入法提取无铅焊料合金弹塑性力学参数的研究

本文通过微纳米压入法结合数值模拟研究了无铅焊料合金SnAg3.5 的弹塑性力学性能，分别采用圆柱形压头及两种不同锥角压头对无铅焊料合金进行压入测试：基于圆柱形压头测试过程中接触面积恒定的特点得到了无铅焊料的弹性模量，进一步采用塑性应变梯度理论对两种锥角压头的测试结果予以修正并通过数值模拟反分析得到相应的特征应力值，同时基于压入特征塑性应变与压头锥角的关系式得到两种不同锥角压头下的特征应变值，在此基础上经求解方程组得到焊料合金的初始屈服应力与应变强化因子，进而得到了焊料合金的幂强化弹塑性本构关系．该方法剔除了压入尺度效应的影响并保证了所得本构关系的唯一性，给出了一种通过原位压入测试表征金属材料弹塑性力学性能的有效方法．     

焊接接头局部塑性行为的循环压痕实验研究

基于纳米压痕技术,对转子钢焊接接头不同区域(母材、焊缝和热影响区)开展了压入位移控制的单向压痕实验和压入载荷控制的循环压痕实验研究.首先,通过压入位移控制的单向压痕实验,采用多次测试取平均值的方式获得了焊接接头各个区域的弹性模量和硬度分布特征,同时对各区域弹性模量中值点的载荷-压入深度曲线进行了分析;其次,对各个区域进行压入载荷控制的循环压痕实验,比较其压入深度随循环周次的演化特征.结果表明,焊接接头不同区域力学性能差异较大,热影响区的弹性模量、硬度、抗拉强度和抗循环变形能力最高,焊缝次之,母材最弱;三个区域在循环压痕载荷下的接触载荷-压入深度滞回环曲线均表现出类似棘轮变形的演化特征,且母材演化速度高于焊缝,高于热影响区.研究结果对汽轮机焊接转子的焊接工艺的优化、寿命预测和可靠性设计具有重要的借鉴意义.     

纳米压痕试验中压头尺寸效应的准连续介质法分析

采用准连续介质法模拟了单晶铝纳米压痕试验过程,分析了不同宽度的刚性矩形压头所引起的初始塑性变形特点,获得了载荷-压深、应变能-位移和硬度-压深曲线.从位错理论的角度分析了压头尺寸对纳米压痕测试结果的影响.研究发现:随着压头宽度的不断增大,压头下方位错形核所需要的载荷和压深程度增大,需要的应变能增加,应变能的变化速率递增,纳米硬度值减小,呈现出明显的尺寸效应.同时表明在一定的压入深度下,硬度与压头尺寸之间存在着一定的比例关系,不同尺寸压头获得的硬度值可以相互换算,但当矩形刚性压头宽度大于或等于120时这种尺寸效应消失.研究结果为纳米压痕实验过程中压头尺寸的选择提供了参考依据.     

轮轨滚动摩擦温升分析

利用有限元法,考虑轮轨间非稳态热传导、与环境的热对流以及热辐射的影响,建立了轮轨滚动接触热耦合计算模型来模拟轮轨滚滑摩擦温升;在模拟轮轨纯滑动条件下,计算分析了由磨损引起的滑动接触斑的尺寸增大对轮轨温度场的影响;在模拟轮轨接触斑部分滑动工况时,针对不同蠕滑率、摩擦系数以及轴重对轮轨温度场的影响进行了相应的计算分析.结果表明:接触斑材料的磨损速度只影响磨损过程中的温度场分布,其稳态温度场分布基本一致;热载荷随着纵向载荷、蠕滑率以及摩擦系数的增大而增大,进而影响轮轨滚动接触热疲劳.     

边坡岩体质量分级的模糊层次分析

基于深度测量压入方法，以材料试验机Instron 5848 Microtester作为加载平台，外接高分辨力位移传感器，设计专用夹具，开发出该材料试验 机的宏观压入功能. 研究发现：对于机架柔度，无需再进行修正；对于压针接触面积， 可用相关的方法计算. 采用Oliver-Pharr方法处理测试数据，可获得材料的 硬度和弹性模量. 为了验证试验的可靠性，选用5种典型金属材料，将宏观压入测试结果与 MTS Nano Indenter XP测试结果进行对比，二者基本一致，其分散性均在10{\%}以内. 显示了开发传统材料试 验机宏观压入测试功能的可行性.     

表面残余应力的仪器化压入检测方法研究进展

针对表面残余应力的仪器化压入检测方法, 阐释利用压入方式检测残余应力的基本原理及其力学机制, 梳理建立残余应力压入检测方法的常用技术路线, 结合残余应力压入检测方法的不同分类, 着重分析6种代表性压入检测方法的优势与局限, 讨论验证压入检测方法可靠性的常用方法, 最后总结残余应力压入检测方法的研究进展, 展望未来的发展趋势为建立无需参考试样一体化检测材料力学参数和非等轴残余应力的仪器化压入分析方法, 探讨建立方法的四个研究要领, 即机制清楚、分析可靠、技术可行、结果可信. 仪器化压入检测技术是郑哲敏先生晚年的研究兴趣之一, 作者在中科院力学所工作期间曾受到郑哲敏先生的热切关注和提问式激励, 谨以此文纪念郑哲敏先生逝世周年.      

刚性圆形压头作用下热电材料半平面的无摩擦接触问题

热电材料可以将热能转化为电能,反之亦然,这一优良的性质将有助于研发更具成本效益的设备和器件。本文研究了刚性圆形压头作用在热电材料半平面的无摩擦接触问题。假定压头为电导体、热导体,且压头压入深度及与材料的接触区域宽度未知。首先求解电场和温度场,利用傅里叶变换得到了电势函数、温度、电流密度和能量通量的解析表达式。然后求解弹性场,利用积分变换和边界条件,将该热弹性接触问题转化为第一类奇异积分方程并数值求解。数值结果讨论了压头半径和热电载荷对法向接触应力、电流强度因子和能量通量强度因子的影响。结果表明,对于圆压头,热电材料的法向电流密度、法向能量通量在接触边缘表现出奇异性,而表面法向接触应力在接触边缘为零。本文建立的研究模型有助于更深层次的了解热电材料的接触行为。     

两种不同形状压头与单晶铜基体间接触力和摩擦力的纳观分析

在考虑单晶铜基体弹塑性形变和晶体各向异性情况下,基于原子尺度,采用混合势函数(EAM和Morse)和Verlet算法动态模拟了半球形和圆锥形两种不同形状压头与单晶铜基体的黏着接触和滑动摩擦过程,分析了接触力和摩擦力对单晶铜基体内失效原子变化情况.研究表明:当压头下压位移为0.9 nm时,由于半球形压头比圆锥形压头底部表面积大,导致半球形压头与基体之间的引力更大而更易产生黏着接触现象.在下压接触过程中,与半球形压头相接触的基体内出现位错原子长大成位错环,而与圆锥形压头相接触的基体未出现此位错环现象,但位错原子数均随压深的增加而增多;在滑动过程中,因半球形压头对基体的摩擦力和法向力比圆锥形压头对基体的摩擦力和法向力大,使得半球形压头比圆锥形压头正前方堆积的位错原子数多,但均随滑动距离的增加而增多.     

Finite Element Simulation of Hot Nanoindentation in Vacuum

A finite element model is developed to investigate technical issues associated with hot nanoindentation measurements in vacuum, e.g. thermal expansion-induced drift and temperature variations at the contact region between the cold indenter tip and hot specimen. With heat conduction properly accounted for, the model is able to reasonably reproduce experimental indentation measurements on fused silica and copper—two materials with significantly different thermal and mechanical properties—at several temperatures. Temperature and loading rate effects on thermal drift are established using this model and an analytical expression for predicting thermal drift is numerically calibrated. The model also captures details of the indentation process that are not directly accessible experimentally, and reaffirms the need for operational refinements in order to acquire high temperature indentation data of high quality, especially in a vacuum environment. Such information can guide experiments aimed at understanding thermally-activated phenomena in materials.     

Determination of material properties using nanoindentation and multiple indenter tips

Nanoindentation is a useful method to probe the material properties of a solid. Its effective use lies in interpreting the data collected from a nanoindentation experiment with an associated analytical/numerical solution of the corresponding problem configuration. In this paper, a parametric finite element study has been performed to develop a new procedure for extracting elastic–plastic properties of a material through nanoindentation experiments with a substantially improved accuracy for the elastic properties of a elastic–plastic solid. The procedure involves data collected through the use of two, different, nanoindenter tips. Non-dimensional functions were constructed for two different indenter geometries to show that test results from multiple indenters, when appropriately manipulated, deliver superior results, compared to using one indenter. The material was assumed to be an isotropic elastic–plastic solid with power law hardening. Friction between the indenter and the material was included in the cases studied. The ratio of yield strength to elastic modulus was assumed to be in the range 0.0005–0.02 and the hardening coefficient was assumed to be between 0 and 0.4. Poisson’s ratio was fixed at 0.3.     

纳米压痕过程的三维有限元数值试验研究

采用有限元方法模拟了纳米压痕仪的加、卸载过程，三维有限元模型考虑了纳米压痕仪的标准Berkovich压头．介绍了有限元模型的几何参数、边界条件、材料特性与加载方式，讨论了摩擦、滑动机制、试件模型的大小对计算结果的影响，进行了计算结果与标准试样实验结果的比较，证实了模拟的可靠性．在此基础上，重点研究了压头尖端曲率半径对纳米压痕实验数据的影响．对比分析了尖端曲率半径r＝0与r＝100nm两种压头的材料压痕载荷—位移曲线．结果表明，当压头尖端曲率半径r≠0时，基于经典的均匀连续介质力学本构理论、传统的实验手段与数据处理方法，压痕硬度值会随着压痕深度的减小而升高．     

ANALYTICAL SOLUTION OF THERMAL CONSOLIDATION OF SATURATED SOILS WITH TWO PARALLEL CYLINDRICAL HEAT SOURCES1）

基于应力平衡条件、渗流连续方程、能量守恒方程,考虑土颗粒和孔隙水热膨胀系数的不同,建立考虑热水力耦合的饱和土体三维热固结控制方程。利用傅里叶变换和拉普拉斯变换导出变换域上的控制方程,解得点热源在变换域和实数域上的解析解,再利用区域积分给出两平行圆柱形热源热固结土体温度、孔压、位移的解析解,并对其进行分析,发现径距比增大会导致两热源温度相互影响程度减弱,热固结系数减小会导致孔压和位移的峰值增大。     

Thermoelastic instability of functionally graded materials with interaction of frictional heat and contact resistance

Both of the frictional heat and thermal contact resistance have a grave responsibility for the localized high temperature (hot spots) at the contact region, which is known as one of the most dangerous appearances in the brakes systems. In this paper, we study the thermoelastic instability (TEI) of a functionally graded material (FGM) half-plane sliding against a homogeneous half-plane at the in-plane direction. The interaction of the frictional heat and thermal contact resistance is taken into account in the TEI analysis. The material properties of the FGM half-plane are supposed to follow the exponential function along the thickness direction. The coupled TEI problem of FGMs is solved by using the perturbation method. The frictionally excited TEI of FGMs is also considered by neglecting the effect of the thermal contact resistance. The results show that the thermal contact resistance, sliding speed and gradient index have significant influence on the TEI. It is found that the variation of the gradient index of FGMs can increase the critical sliding speed and critical heat flux, and therefore improve the TEI of the sliding system.     

Effects of thickness on the largely-deformed JKR (Johnson–Kendall–Roberts) test of soft elastic layers

The paper aimed to study the effect of large deformation and material nonlinearity on the adhesive contact between a smooth rigid spherical indenter and a Neo-Hookean layer of finite thickness, for the cases of the layer thickness/indenter radius ratio between 1 and 2. Our analysis was based on the large-deformation JKR (LDJKR) theory, which models the adhesive contact of two elastic solids in large-deformation regime by knowing the solution of the corresponding non-adhesive contact problem. In this paper, the non-adhesive contact between a spherical indenter and a Neo-Hookean layer was solved by finite element analysis. Combined these numerical results and the LDJKR theory, approximate analytic expressions of the applied load and displacement of adhesive contact of Neo-Hookean layers were obtained. The effects of layer thickness were also discussed.     

The Influence of Indenter Tip Imperfection and Deformability on Analysing Instrumented Indentation Tests at Shallow Depths of Penetration on Stiff and Hard Materials

We report on the difficulties of extracting plastic parameters from constitutive equations derived by instrumented indentation tests on hard and stiff materials at shallow depths of penetration. As a general rule, we refer here to materials with an elastic stiffness more than 10 % of that of the indenter and a yield strain higher than 1 %, as well as to penetration depths less than ～ 5 times the characteristic tip defect length of the indenter. We experimentally tested such a material (an amorphous alloy) by nanoindentation. To describe the mechanical response of the test, namely the force-displacement curve, it is necessary to consider the combined effects of indenter tip imperfections and indenter deformability. For this purpose, an identification procedure has been carried out by performing numerical simulations (using Finite Element Analysis) with constitutive equations that are known to satisfactorily describe the behaviour of the tested material. We propose a straightforward procedure to address indenter tip imperfection and deformability, which consists of firstly taking account of a deformable indenter in the numerical simulations. This procedure also involves modifying the experimental curve by considering a truncated length to create artificially the material’s response to a perfectly sharp indentation. The truncated length is determined directly from the loading part of the force-displacement curve. We also show that ignoring one or both of these issues results in large errors in the plastic parameters extracted from the data.     

岩土介质非稳态热固结耦合问题的热源函数法

考虑耦合效应的饱和土体热固结问题控制方程,利用Fourier变换、Laplace变换给出其在变换域上的解,将初始温度场分布视为虚拟的热源或者将热源等价为特定的初始温度分布,利用热源函数法给出瞬时线热源非稳态温度场、应力场和位移场的解析求解方法,通过在时间域和空间域上进行积分,给出有初始温度场分布以及有分布内热源存在且热源强度随时间变化条件下的热固结问题计算方法。对一无限大物体内存在有平面矩形域热源情况下周围介质的温度、孔隙水压力以及位移等的变化特征进行分析。研究表明,热源函数法可有效地求解一系列复杂情况下的热固结问题。     

Experimental investigation of high temperature thermal contact resistance with interface material

Thermal contact resistance plays a very important role in heat transfer efficiency and thermomechanical coupling response between two materials, and a common method to reduce the thermal contact resistance is to fill a soft interface material between these two materials. A testing system of high temperature thermal contact resistance based on INSTRON 8874 is established in the present paper, which can achieve 600°C at the interface. Based on this system, the thermal contact resistance between superalloy GH600 material and three-dimensional braid C/C composite material is experimentally investigated, under different interface pressures, interface roughnesses and temperatures, respectively. At the same time, the mechanism of reducing the thermal contact resistance with carbon fiber sheet as interface material is experimentally investigated. Results show that the present testing system is feasible in the experimental research of high temperature thermal contact resistance.