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1.
扫描探针显微学中的云纹方法   总被引:2,自引:0,他引:2       下载免费PDF全文
在扫描探针显微镜(SPM)的扫描过程中,由SPM的扫描线与物质表面周期性晶格结构进行干 涉可以形成纳米云纹图像.采用高取向热解石墨(HOPG)和云母作为试件,分别对扫描隧道 显微镜(STM)和原子力显微镜(AFM)云纹进行了研究,实验结果与理论分析完全一致.SPM 纳米云纹法在纳米测量和表征方面具有较大的应用前景. 关键词: 云纹 SPM 晶格栅线 纳米测量  相似文献   

2.
纳米云纹法实验研究   总被引:8,自引:4,他引:4  
结合原子力显微镜技术提出了一种新型纳米云纹方法 ,并应用该方法进行纳米范围的变形。实验中选用原子力显微镜显示屏的扫描线做为参考栅 ,云母和高纯定向石墨的晶格结构做为试件。对纳米云纹形成原理及测量方法进行了详尽讨论。运用该方法对强脉冲激光辐照激光照射之后云母试样的剩余变形进行测量研究。成功的实验结果表明这种方法是可行性的 ,可望在纳米力学行为研究中获得广泛应用。  相似文献   

3.
纳米云纹法条纹倍增技术研究   总被引:4,自引:2,他引:2  
刘战伟  谢惠民  方岱  戴福隆  王卫  方炎 《光子学报》2005,34(9):1431-1433
提出了一种纳米云纹法的条纹倍增技术,可用于单晶材料纳米级变形测量.在测量中,单晶材料的晶格结构由透射电镜(TEM)采集并记录在感光胶片上作为试件栅,几何光栅作为参考栅.对纳米云纹条纹的形成原理,透射电镜放大倍数与试件栅的频率关系,条纹倍增技术,位移、应变测量方法等进行了详细讨论.该方法不仅能够测量连续力学参量,如应变和位移,而且能够表征纳观非连续参量,如位错、夹杂.  相似文献   

4.
在扫描探针纳米加工技术的基础上,提出了利用原子力显微镜(AFM)来制作高频光栅的新工艺。利用AFM硅制探针,在接触模式下对光盘(聚碳酸酯材料)进行刻划试验。对刻划光栅的工艺参数进行优化,得到了纳米量级光栅。并将刻划所得光栅应用于数字云纹法,与数字参考栅干涉形成微/纳米数字云纹。实验结果表明,该法所制得的光栅可以应用于实际变形的测量。  相似文献   

5.
介绍了近年来发展的纳米云纹法及其新的应用。这些方法是基于原子力显微镜、扫描隧道显微镜和透射电子显微镜的原理提出来的。纳米云纹法能够对物体的微/纳观变形提供定量的分析。详述了这些方法的测量原理和实验技术,并进行了新的应用研究。实验结果论证了这些方法的可行性,并证实了这些方法具有纳米级的位移测量灵敏度。  相似文献   

6.
提出了一种新的测量物质纳米级变形的云纹方法———数字纳米云纹法,在测量过程中,借助于各种电镜,采用具有周期结构的晶体物质的晶格或一些过渡金属、贵金属材料规则的表面原子重构作为试件栅。该试件栅的节距可达到亚纳米的量级,使得该方法可以在纳观范围内测量物体的面内位移,应变。参考栅采用计算机绘制的正弦型数字栅。详细地论述了该数字栅的制作方法,数字纳米云纹条纹的形成机理,及位移、应变的测量方法,云纹条纹的相移方法和倍增方法。  相似文献   

7.
原子力显微扫描云纹法的相移技术研究   总被引:3,自引:1,他引:2  
提出一种原子力显微镜扫描云纹法的相移新技术 ,运用原子力显微镜的压电扫描头作为相移元件 ,对所得云纹图像可进行 0 - 2 π范围内的四步相移。对该方法的测量原理和实验技术进行了详细的阐述。作为典型实验和应用实例 ,分别对由全息光栅和含热变形的电子封装试件栅形成的云纹进行相移分析。成功的实验结果表明 ,该方法是可行的 ,为微米云纹方法的条纹处理提供了一种新途径。该方法可望在微观变形的云纹法测量中发挥积极作用  相似文献   

8.
提出了透射电子显微镜(TEM)纳米云纹法的新技术,首次将该方法用于单根单壁碳纳米管的残余变形测量。纳米云纹由计算机显示器扫描线与碳纳米管束TEM图像干涉而成。该方法具有纳米级空间分辨率,可直接测量碳纳米管的力学性能。对TEM纳米云纹法的原理进行了详细的阐述,并利用不同管径的单壁碳管束产生了云纹。对直径为7.5nm的弯曲碳管束的残余变形进行测量,直接得到了其中一根直径为1.0nm的单壁碳管的残余变形场。实验结果证明了该方法的可行性。该方法为纳米尺度的碳管力学性能测量提供了新途径。  相似文献   

9.
将激光扫描共聚焦显微镜与实验力学中的云纹法相结合,提出了激光扫描共聚焦显微镜云纹法并对其进行了实验研究.实验中以激光扫描共聚焦显微镜的扫描线作为虚拟参考栅,以1 200 lines/mm的全息光栅作为试件栅,这两组栅线相干涉形成云纹条纹.对激光扫描共聚焦显微镜中云纹的形成原理和出现条件进行了讨论,对实验结果与理论分析进行了比较.结果表明,激光扫描共聚焦显微镜云纹法是真实可行的.由于该方法无需干涉系统且对测量环境无特殊要求,因此有望在待测物体表面微米量级变形观察和测量上得到应用.  相似文献   

10.
王林  Koned.L 《光学学报》2000,20(12):675-1679
X射线干涉仪以非常稳定的单晶硅晶格作为长度单位,可以实现亚纳米精度的微位移测量。提出了将X射线干涉仪和扫描隧道显微镜结合起来,利用单晶硅的晶格尺度测量扫描探针显微镜样板节距的技术方案,并进行了实验研究。  相似文献   

11.
双成象单元扫描隧道显微镜与原子尺纳米计量技术   总被引:3,自引:3,他引:0  
章海军  吴兰 《光子学报》1998,27(10):886-889
研制了双成象单元扫描隧道显微镜(STM),可同时对参考样品的原子晶格和被测样品扫描成象.计数原子晶格的数目,即可精确测定被测样品图象的尺度,以原子尺方式实现严格的纳米计量.本文介绍双成象单元的STM的原理和仪器系统,讨论原子尺纳米计量的可行性,给出被测样品图象的纳米计量结果.  相似文献   

12.
In this paper, a new nano-moiré method using scanning tunneling microscope (STM) is proposed. This method is capable of measuring nanoscopic deformation of matter. The formation mechanism of the STM moiré fringe and the phase shifting technique used in STM moiré fringes are explained in details. Typical experiments are conducted with the crystal lattices of freshly cleaved highly oriented pyrolytic graphite, are used as specimen grating, to generate STM moiré fringe patterns. Phase shifting is realized in four steps from 0 to 2π by controlling the PZT in the STM system to shift the specimen in the vertical direction. This method provides a new way for disposal of moiré fringes pattern in the nano-moiré measurement.  相似文献   

13.
A new method for studying of vibronic transitions by scanning tunneling microscope (“nitraresonator electron-vibronic scanning tunneling spectroscopy of adsorbates”) is proposed. Results of experiments carried out by STM “Omicron” where electron-vibronic series of field emission resonances were observed are presented. Frequencies of the resonances correspond to ones of local vibrations of titan oxide and adsorbed hydroxil particles.  相似文献   

14.
扫描隧道显微镜(STM)图象的解析,是STM应用的关键问题之一,STM的原始图象不能适应各种需要,而采用各种方法重构后,可以适应不同的应用。本文介绍了6种不同的重构方法。  相似文献   

15.
Bucky onions were fabricated by the DC discharge method and their behaviors and electric properties on Highly Oriented Pyrolytic Graphite (HOPG) were studied by using an atomic force microscope (AFM), a scanning tunneling microscope (STM) and a transmission electron microscope (TEM). Small-sized Bucky onions demonstrated the properties of semiconductors and as the size increased their metallicity became stronger. AFM and STM images revealed the tendency of Bucky onions to form dimers.  相似文献   

16.
We introduce a novel modular cell based scanning tunneling microscope with external piezoelectric actuators. A tip and a sample are contained in a closed interchangeable cell, consisting of a stiff top plate and a bottom part, fastened together by an elastic material. The bottom part, containing a scanning tip, is fastened to a base unit while the top plate, containing a sample, is capable of scanning motion by external piezoelectric actuators mounted in the same base unit. The actuators are pre-loaded by the deformation of the elastic material of the cell, giving an increased stability. This design is expected to simplify the scanning tunneling microscope (STM) operation in difficult environments greatly by enclosing only the tip and sample in a small cell-module, which is pluggable to a scanning mechanism and other supportive functionalities. A frequency characterization and an image scan showing atomic resolution of highly oriented graphite in air, at room temperature, is presented.  相似文献   

17.
Inelastically tunneled electrons from a scanning tunneling microscope (STM) were used to induce vibrationally mediated motion of a single cis-2-butene molecule among four equivalent orientations on Pd(110) at 4.8 K. The action spectrum obtained from the motion clearly detects more vibrational modes than inelastic electron tunneling spectroscopy with a STM. We demonstrate the usefulness of the action spectroscopy as a novel single molecule vibrational spectroscopic method. We also discuss its selection rules in terms of resonance tunneling.  相似文献   

18.
The structure of the Cu(410)-O surface is studied by a scanning tunneling microscope (STM) with atomic resolution. Tunneling is accomplished for various states of the tungsten STM probe, which allows oxygen and copper atoms to be visualized separately.  相似文献   

19.
We use scanning tunneling microscopy to measure magnetic field induced strains in highly oriented pyrolytic graphite. This is done by using a scanning tunneling microscope with some magnetic components, which however do not produce an observable response within our resolution in the case of pure (99.999%) paramagnetic or diamagnetic metals (at the low field strengths applied). We study also ferromagnetic metals with this method for comparison. We find a relatively large (similar to that of permalloy) magnetostrictive response of graphite for the low applied field. The data shows saturation of the strain and also that the strain observed is localized and is not the cumulative strain from the mounted edge of the sample to the position of measurement, implying that volume is not conserved with the strains. We believe that the observed strains correspond to a signal of a ferromagnetic material and in this case may be due to the defects observed on the graphite planes.Received: 25 May 2004, Published online: 24 September 2004PACS: 68.37.Ef Scanning tunneling microscopy (including chemistry induced with STM) - 75.80. + q Magnetomechanical and magnetoelectric effects, magnetostriction - 81.05.Uw Carbon, diamond, graphite  相似文献   

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