共查询到20条相似文献,搜索用时 515 毫秒
1.
在核磁共振中,常规的正交检测技术采用两路相敏检波.因为两路相检波的相位和幅度存在不平衡而引起谱失真,所以必须用相位循环来消除.这增加了实验时间.本文提出并在MSL-300 NMR谱仪上实现了一种数字正交检波方法.这种方法使用单路相检波,避免了两路不平衡而引起的谱线失真,因此不需要相位循环技术 相似文献
2.
在核磁共振中,常规的正交检测技术采用两路相敏检波.因为两路相检波的相位和幅度存在不平衡而引起谱失真,所以必须用相位循环来消除.这增加了实验时间.本文提出并在MSL-300
NMR谱仪上实现了一种数字正交检波方法.这种方法使用单路相检波,避免了两路不平衡而引起的谱线失真,因此不需要相位循环技术. 相似文献
3.
从原理上分析了掩膜的光场成像特点,通过建立光场成像的计算机仿真模型,模拟四维光场的获取,并通过数字对焦算法获得离焦物体的清晰图像.同时利用采样定理分析了孔径采样密度对数字对焦图像的影响,计算出合适的采样间隔对仿真模型的复杂度进行优化. 相似文献
4.
5.
6.
7.
8.
本文介绍一种用场效应管制成的限幅再生式14N NQR谱仪。这种谱仪的频率范围为(1-5) MHz,射频幅度(0.5-4) VP-P,为了获得数字记录的NQR谱线,利用微处理器Z-80构成的数字相敏检波系统,把数字相敏检波系统接至信号处理通道,就构成一台带有微处理器的14N NQR谱仪。用它测定了乌洛托品(HMT)、亚硝酸钠和对位澳代苯胺等十多个含氯化合物在室温与77K时的14N NQR谱线。实验结果表明,用微处理器控制的NQR谱仪的信噪比是一般谱仪的两倍。此外,这种仪器也为进一步数据处理提供方便。 相似文献
9.
10.
11.
12.
提出了基于异构双核的低场核磁共振(Low-field Nuclear Magnetic Resonance,low-field NMR)接收机的设计,具有ARM(Adanced RISC Machines)和现场可编程门阵列(Field Programmable Gate Array,FPGA)先进的异构双核结构、高速的模数转换器(Analog to Digital Converter,ADC)采集、增益的可控以及可视化显示等特性,提高了整个系统的性能指标.设计中采用Xilinx公司的系统开发工具System Generator来实现内部信号处理功能.实验结果表明,数字接收机具有结构紧凑、可重构性强、采样速率高和成本低等特点,并且增益的可控使接收机获得了较大的动态范围,提高了重建图像的信噪比(Signal-to-Noise Ratio,SNR). 相似文献
13.
14.
15.
OPENCORE NMR: open-source core modules for implementing an integrated FPGA-based NMR spectrometer 总被引:1,自引:0,他引:1
Takeda K 《Journal of magnetic resonance (San Diego, Calif. : 1997)》2008,192(2):218-229
A tool kit for implementing an integrated FPGA-based NMR spectrometer [K. Takeda, A highly integrated FPGA-based nuclear magnetic resonance spectrometer, Rev. Sci. Instrum. 78 (2007) 033103], referred to as the OPENCORE NMR spectrometer, is open to public. The system is composed of an FPGA chip and several peripheral boards for USB communication, direct-digital synthesis (DDS), RF transmission, signal acquisition, etc. Inside the FPGA chip have been implemented a number of digital modules including three pulse programmers, the digital part of DDS, a digital quadrature demodulator, dual digital low-pass filters, and a PC interface. These FPGA core modules are written in VHDL, and their source codes are available on our website. This work aims at providing sufficient information with which one can, given some facility in circuit board manufacturing, reproduce the OPENCORE NMR spectrometer presented here. Also, the users are encouraged to modify the design of spectrometer according to their own specific needs. A home-built NMR spectrometer can serve complementary roles to a sophisticated commercial spectrometer, should one comes across such new ideas that require heavy modification to hardware inside the spectrometer. This work can lower the barrier of building a handmade NMR spectrometer in the laboratory, and promote novel and exciting NMR experiments. 相似文献
16.
Concerning many former liquid or hybrid liquid/solid NMR consoles, the built in Analog-to-Digital Converters (ADCs) are incapable of digitizing the fids at sampling rates in the MHz range. Regarding both strong anisotropic interactions in the solid state and wide chemical shift dispersion nuclei in solution phase such as 195Pt, 119Sn, 207Pb etc., the spectrum range of interest might be in the MHz range. As determining the informative tensor components of anisotropic NMR interactions requires nonlinear fitting over the whole spectrum including the asymptotic baseline, it is prohibited by low sampling rates of the ADCs. Wide spectrum width is also useful in solution NMR, since windowing of wide chemical shift ranges is avoidable. We built an external analog to digital converter with 10 MHz maximal sampling rate, which can work simultaneously with the built in ADC of the spectrometer. The ADC was tested on both Bruker DRX and Avance-I NMR consoles. In addition to the analog channels it only requires three external digital lines of the NMR console. The ADC sends data to PC via USB. The whole process is controlled by software written in JAVA which is implemented under TopSpin. 相似文献
17.
This work demonstrates that a significant improvement of the timing resolution, simultaneously keeping coincidence count rate high enough, can be achieved by use of the state-of-the-art ultra fast 8-bit digitizers which replace the traditional analog timing modules. Performance of the digital spectrometer in conditions of a routine measurement is compared with that of the same detectors connected to the analog setup. It was found that employment of the digital setup leads to an improvement of timing resolution from 169 ps for the traditional analog setup down to 146 ps for the digital setup. 相似文献
18.
The replacement of the commonly used analog phase-sensitive detection (PSD) by digital PSD for demodulation of electron paramagnetic
resonance (EPR) signals is suggested for upgrading of an out-of-date EPR spectrometer. Connection of the microwave bridge
output to a fast analog-digital converter (ADC) eliminates some of the spectrometer’s components: the electronics responsible
for analog PSD, ADC for sampling of demodulated signals, and a computer, as well as the usage of some of the spectrometer’s
settings. The spectrometer is reduced to a magnet, microwave bridge, and personal computer containing an ADC board. EPR signals
digitized for a set of magnetic field positions form a two-dimensional array which is stored in a personal computer. Demodulation
and filtering are done numerically to produce a conventional EPR spectrum. In comparison with analog PSD, this numerical approach
does not eliminate the out-of-phase component of the signal and the signals at the higher harmonics of the modulation frequency.
The details of modernizing the Bruker ER200E SRC EPR spectrometer are discussed to demonstrate these and other advantages
of digital demodulation. 相似文献
19.
In this work we propose an approach to reduce the digitization noise for a given dynamic range, i.e., the number of bits, of an analog to digital converter used in an NMR receiver. In this approach, the receiver gain is dynamically increased so that the free induction decay is recorded in such an emphasized way that the decaying signal is digitized using as many number of bits as possible, and at the stage of data processing, the original signal profile is restored by applying the apodization that compensates the effect of the preemphasis. This approach, which we call APodization after Receiver gain InCrement during Ongoing sequence with Time (APRICOT), is performed in a solid-state system containing a pair of (13)C spins, one of which is fully isotopically labeled and the other is naturally abundant. It is demonstrated that the exceedingly smaller peak buried in the digitization noise in the conventional approach can be revealed by employing APRICOT. 相似文献